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退火温度对CrFeCoNiTi1.5高熵合金微结构与性能的影响
引用本文:姜越,周广泰,程思梦,李秀明.退火温度对CrFeCoNiTi1.5高熵合金微结构与性能的影响[J].金属热处理,2020,45(3):108-113.
作者姓名:姜越  周广泰  程思梦  李秀明
作者单位:哈尔滨理工大学 理学院, 黑龙江 哈尔滨 150080
摘    要:为研究中低温热处理对CrFeCoNiTi1.5高熵合金性能的影响,分别在200、400及600 ℃下对高熵合金进行10 h退火处理。通过X射线衍射仪、扫描电镜(SEM)、能谱仪(EDS)、显微硬度计和电化学工作站对高熵合金的组织结构、表面形貌以及元素的偏析程度进行分析,并测试了高熵合金的动电位极化曲线以及维氏硬度。结果表明:退火温度的提高有利于CrFeCoNiTi1.5高熵合金中HCP结构相的析出;随着温度的升高Cr、Fe、Co和Ni逐渐向晶内聚集分布,Ti逐渐向晶间聚集。600 ℃中低温退火处理时合金耐腐蚀性能最好,硬度为914 HV0.5。

关 键 词:CrFeCoNiTi1.5高熵合金  退火处理  微结构  维氏硬度  耐腐蚀性  
收稿时间:2019-09-20

Effect of annealing temperature on microstructure and properties of CrFeCoNiTi1.5 high entropy alloy
Jiang Yue,Zhou Guangtai,Cheng Simeng,Li Xiuming.Effect of annealing temperature on microstructure and properties of CrFeCoNiTi1.5 high entropy alloy[J].Heat Treatment of Metals,2020,45(3):108-113.
Authors:Jiang Yue  Zhou Guangtai  Cheng Simeng  Li Xiuming
Affiliation:School of Science, Harbin University of Science and Technology, Harbin Heilongjiang 150080, China
Abstract:In order to study the effect of medium and low temperature heat treatment on properties of CrFeCoNiTi1.5 high entropy alloy,the high entropy alloy was annealed at 200,400 and 600℃for 10 h,respectively.The microstructure,surface morphology and segregation of the elements were analyzed by X-ray diffraction,scanning electron microscopy(SEM),energy dispersive spectroscopy(EDS).Simultaneously,the dynamic potential polarization curves and Vickers hardness of the high entropy alloy were also tested by microhardness tester and electrochemical workstation.The results show that the increase of annealing temperature is favorable to the precipitation of HCP structure phase of the CrFeCoNiTi1.5 high entropy alloy.With the increase of temperature,Cr,Fe,Co and Ni gradually aggregate into and distribute inside the grains,while Ti gradually aggregates to the intergranular region.When annealed at 600℃,the corrosion resistance of the CrFeCoNiTi1.5 high entropy alloy reaches the optimal value,and the Vickers hardness is 914 HV0.5.
Keywords:CrFeCoNiTi1  5 high entropy alloy  annealing  microstructure  Vickers hardness  corrosion resistance
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