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Porosity effect on microstructure,mechanical, and fluid dynamic properties of Ti2AlC by direct foaming and gel‐casting
Authors:Marek Potoczek  Anna Chmielarz  Murilo D de M Innocentini  Izabela C P da Silva  Paolo Colombo  Barbara Winiarska
Affiliation:1. Faculty of Chemistry, Rzeszow University of Technology, Rzeszów, Poland;2. Ceramic Department, Institute of Power Engineering, CEREL, Boguchwa?a, Poland;3. Course of Chemical Engineering, University of Ribeir?o Preto, UNAERP, Ribeir?o Preto, Brazil;4. Dipartimento di Ingegneria Industriale, Università di Padova, Padova, Italy;5. Department of Materials Science and Engineering, The Pennsylvania State University, State College, Pennsylvania;6. Faculty of Physics and Applied Computer Science, AGH University of Science and Technology, Kraków, Poland;7. The Henryk Niewodniczański Institute of Nuclear Physics, Polish Academy of Science, Kraków, Poland
Abstract:In this study, Ti2AlC foams were fabricated by direct foaming and gel‐casting using agarose as gelling agent. Slurry viscosity, determined by the agarose content (at a fixed solids loading), as well as surfactant concentration and foaming time were the key parameters employed for controlling the foaming yield, and hence the foam porosity after sintering process. Fabricated foams having total porosity in the 62.5‐84.4 vol% range were systematically characterized to determine their pore size and morphology. The effect of the foam porosity on the room‐temperature compression strength and elastic modulus was also determined. Depending on the amount of porosity, the compression strength and Young's modulus were found to be in the range of 9‐91 MPa and 7‐52 GPa, respectively. Permeability to air flow at temperatures up to 700°C was investigated. Darcian (k1) and non‐Darcian (k2) permeability coefficients displayed values in the range 0.30‐93.44 × 10?11 m2 and 0.39‐345.54 × 10?7 m, respectively. The amount of porosity is therefore a very useful microstructural parameter for tuning the mechanical and fluid dynamic properties of Ti2AlC foams.
Keywords:gel‐casting  MAX phases  morphology  permeability  pores/porosity
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