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FeCoCrNiMn高熵合金大形变冷轧板再结晶退火过程中的组织演变
引用本文:国春艳,刘玉宝,杨鹏飞,李园,吕卫东,高日增,张洋,侯复生.FeCoCrNiMn高熵合金大形变冷轧板再结晶退火过程中的组织演变[J].金属热处理,2022,47(7):163-167.
作者姓名:国春艳  刘玉宝  杨鹏飞  李园  吕卫东  高日增  张洋  侯复生
作者单位:1.包头铁道职业技术学院 机械与电气系, 内蒙古 包头 014000;2.包头稀土研究院 白云鄂博稀土资源研究与综合利用国家重点实验室, 内蒙古 包头 014030
基金项目:内蒙古自治区重大专项(ZDZX2018032)
摘    要:采用X射线衍射仪(XRD)、维氏硬度计、光学显微镜和电子背散射衍射(EBSD)研究了FeCoCrNiMn高熵合金经压下率为95%的大形变冷轧和550~800 ℃退火1 h后的晶体结构(fcc)、硬度变化、组织演变和再结晶行为。结果表明,冷轧-退火过程中FeCoCrNiMn高熵合金的晶体结构始终保持面心立方结构,再结晶开始温度为600 ℃,结束温度为750 ℃,随着退火温度的升高,试样的硬度先下降后逐渐趋于平缓,组织由纤维状的形变晶粒逐渐全部变为随机取向的再结晶晶粒。

关 键 词:FeCoCrNiMn高熵合金  大形变冷轧  退火  晶体结构  组织演变  
收稿时间:2022-01-30

Recrystallizing annealed microstructure evolution of severe cold rolled FeCoCrNiMn high entropy alloy
Guo Chunyan,Liu Yubao,Yang Pengfei,Li Yuan,Lü Weidong,Gao Rizeng,Zhang Yang,Hou Fusheng.Recrystallizing annealed microstructure evolution of severe cold rolled FeCoCrNiMn high entropy alloy[J].Heat Treatment of Metals,2022,47(7):163-167.
Authors:Guo Chunyan  Liu Yubao  Yang Pengfei  Li Yuan  Lü Weidong  Gao Rizeng  Zhang Yang  Hou Fusheng
Affiliation:1. Department of Mechanical and Electrical Engineering, Baotou Railway Vocational and Technical College, Baotou Inner Mongolia 014000, China;2. State Key Laboratory of Baiyunobo Rare Earth Resource Researches and Comprehensive Utilization, Baotou Research Institute of Rare Earths, Baotou Inner Mongolia 014030, China
Abstract:Crystal structure, hardness, microstructure evolution and recrystallization behavior of the FeCoCrNiMn high-entropy alloy after severe cold rolling with reduction ratio of 95% and then annealing at 550-800 ℃ for 1 h were studied by means of X-ray diffractometer (XRD), Vickers hardness tester, optical microscope and electron backscatter diffraction (EBSD). The results show that the crystal structure of the FeCoCrNiMn high-entropy alloy always maintains an fcc structure during the cold rolling-annealing process. The beginning temperature of recrystallization is 600 ℃, and the finishing temperature is 750 ℃. As the annealing temperature increases, the hardness of the high-entropy alloy decreases first and then tends to be gentle, and microstructure gradually changes from fibrous deformed grains to randomly oriented recrystallized grains.
Keywords:FeCoCrNiMn high-entropy alloy  severe cold rolling  annealing  crystal structure  microstructure evolution  
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