Effect of thermal ageing of CF8M on multi‐axial ductility and application to fracture toughness prediction

This paper proposes a method to predict the thermal ageing effect on fracture toughness of CF8M cast stainless steel. The proposed method is based on multi‐axial fracture strain combined with finite element damage analysis to simulate ductile tearing. Multi‐axial fracture strain loci of un‐aged and aged CF8M are determined by analyzing notched bar tensile test. It is shown that the thermal ageing effect on multi‐axial fracture strain loci can be characterized by one constant. It is further shown that J‐resistance curves of un‐aged and aged CF8M can be predicted well from finite element damage analysis using multi‐axial fracture strain loci. Implication of present results to practical application of crack assessment of aged cast stainless steels is discussed.     

AN EVALUATION OF THE FRACTURE RESISTANCE OF ENGINEERING MATERIALS FROM THE FRACTURE SURFACE MORPHOLOGY

Abstract— The following work examines the fracture morphology in relation to the COD R -curves of three stainless steels. Additional considerations are noted concerning crack growth behaviour based on simple, optical microscopic observations. Procedures for the determination of R -curves and initiation values are outlined when a multi-specimen technique is used and the crack growth is measured by a light microscope. The COD R -curves are obtained for different conditions which reduce fracture ductility in two 310S and one 304H stainless steels. These conditions include a sigma-phase in one 310S, and sensitization of the large grain size microstructure in the other 310S stainless steel.     

UNSTABLE FATIGUE CRACK PROPAGATION AND FATIGUE FRACTURE TOUGHNESS OF STEELS

This paper presents the results of fatigue crack growth and fatigue fracture toughness studies of a high-pressure vessel steel with particular emphasis on the influence of heat treatment, low temperatures, plastic prestraining, the stress ratio and specimen dimensions. It has been shown that steels in an embrittled state, caused primarily by thermal treatment and low-temperatures, exhibit unstable fatigue crack growth which is characterized by alternate crack jumps (cleavage zones) and zones of fatigue crack growth. The fatigue fracture toughness, which corresponds to the first crack jump, and final fracture can be appreciably lower (i.e. up to 50%) than the static fracture toughness under plane strain conditions at the corresponding temperature. An analysis has been performed of unstable and stable fatigue crack growth and a model of unstable crack propagation is proposed which accounts for the observed experimental behaviour.     

FRACTOGRAPHIC ANALYSIS IN THE UNDERSTANDING OF CORROSION FATIGUE MECHANISMS

Fractographic analyses have been used to explain the cyclic crack growth behaviour of A533-B, Ducol W30, a C-Mn steel and type 304 stainless steel in simulated light water reactor environments at ambient temperature. Fractographic observations have offered an explanation for anomalous crack growth behaviour and have also indicated where micro structural or environmental variables dominate in producing certain fracture modes and crack growth rates. An understanding of the operative corrosion fatigue mechanisms has been formulated through these fractographic analyses. Environmental crack growth in the ferritic steels has been described by a model involving both anodic dissolution and hydrogen embrittlement. Conditions where only one of these mechanisms would dominate have been identified and limits to their effect postulated. A crystallographic mode of failure observed in the austenitic type 304 stainless steel has also been explained by a selective dissolution process.     

Fatigue crack propagation in cast duplex stainless steels: thermal ageing and microstructural effects

The ferrite phase of cast duplex stainless steels becomes embrittled after thermal ageing, leading to a significant decrease in fracture properties. In the present paper, the influence of ageing and solidification structure on the fatigue crack growth rates (FCGRs) and on the fatigue crack growth mechanisms in a cast duplex stainless steel is studied. FCGRs measured at room temperature increase slightly after ageing at 400 °C, due to ferrite cleavage and to the resulting irregular shape of the crack front. The crack propagates without any preferential path by successive ruptures of ferrite and austenite phases. The macroscopic crack propagation plane depends on the crystallographic orientation of the ferrite grain. Secondary cracks can appear due to the complex solidification structure. This in turn influences the FCGR. The fatigue crack closure level decreases with increasing ageing. This can be explained by a decrease in the kinematic cyclic hardening of these materials.     

A model for predicting the influence of warm pre-stressing and strain ageing on the cleavage fracture toughness of ferritic steels

A micromechanistic model of warm pre-stressing is extended to predict the combined effects of warm pre-stressing and strain ageing on the cleavage fracture toughness of ferritic steels. The crack tip stress distribution after a cycle of pre-straining and strain ageing is estimated by superposition of the appropriate monotonic loading stress distributions. The Ritchie, Knott and Rice model of cleavage fracture and its associated fracture criterion are employed in conjunction with the crack tip stress distribution to predict the critical stress intensity factor after warm pre-stressing and strain ageing. Illustrative calculations are presented, based upon the published material's properties of a high nitrogen mild steel. Available experimental data for pressure vessel steels bear out the form of the predictions. At low temperatures, and after heavy pre-loads, the benefits of warm pre-stressing dominate strain ageing induced embrittlement and the toughness is apparently enhanced. At higher temperatures, or after small pre-loads, however, strain ageing dominates and the apparent toughness is reduced. Various assumptions and approximations inherent in the model are discussed. These generally tend to render the predictions conservative. Finally it is noted that the model should be equally applicable to the prediction of the combined effect of warm pre-stressing and neutron irradiation on the cleavage fracture toughness of ferritic steels.     

FATIGUE CRACK GROWTH RATE BEHAVIOUR OF STAINLESS STEEL CLADDINGS IN AIR AND UNDER VACUUM AT 300°C

CT type specimens containing two layers of 309L and 308L cladding stainless steels welded to A508 carbon steel and 316 stainless steel were specially devised to test the influence of R ratio and environment on the crack propagation rate behaviour of cladding materials at 300°C. Large effects are shown. The crack growth rate under vacuum can be smaller by more than one order of magnitude as compared to air. Large differences are also shown on the fracture surfaces, where it is observed than vacuum promotes the formation of large crystallographic {111} facets. The effect of environment is briefly discussed on the basis of existing gas adsorption models.     

CYCLIC LOADING AND FRACTURE TOUGHNESS OF STEELS

Abstract— The paper considers the effect of cyclic loading and loading rate upon fracture toughness characteristics of steels at room and low temperatures. It is shown that fracture toughness of a low-alloy ferrite-pearlite steel with 0·1% C (steel 1) and for 15G2AFDps steel of the same class (steel 2) are 2 to 2·5 times lower under cyclic loading (50 and 0·5 Hz) and dynamic loading (= 1·5 × 10⁶MPa √m s⁻¹) than under static loading (= 0·6 to 9 MPa √m s⁻¹). For quenched and low-tempered 45 steel at 293 K and for armco-iron at 77 K fracture toughness characteristics do not depend on the loading condition. Macro- and micro-fractographic investigations revealed a correlation between the plastic zone size and the length of brittle fracture areas which are formed in steels 1 and 2, and in armco-iron during unstable propagation of the fatigue crack. Dependence of the decrease of the critical stress intensity factor under cyclic loading on the number of load cycles are obtained for repeating ( R = 0) and alternating bending ( R =−1) of specimens with a crack. A model for the transition from stable to unstable crack propagation is proposed involving crack velocity in the zone ahead of the crack tip damaged by cyclic plastic deformation. A new approach is suggested to the classification of materials on the basis of the sensitivity of fracture toughness characteristics to cyclic conditions of loading.     

Effects of aging at 700°C on ductile fracture of AISI 316 stainless steel

Abstract

The micromechanisms of ductile fracture have been studied in a commercial AISI 316 austenitic stainless steel. Tensile, Charpy impact, and ductile fracture toughness testing have been performed on unaged material and samples aged at 700°C for times up to 4380 h. Examination of the specimens after testing has shown that the microstructural changes occurring at grain boundaries are responsible for the observed losses of ductility and crack growth resistance. The relative magnitude of the observed changes in mechanical properties has been explained using a simple model to describe the ductile fracture process.

MST/1001     

THE CRACK INITIATION TOUGHNESS FOR BRITTLE FRACTURE OF SUPER DUPLEX STAINLESS STEEL

Abstract— The occurrence of brittle stable crack growth before unstable fracture was demonstrated with the aid of heat-tinting, for a ferritic matrix super duplex stainless steel which had been age-hardened at 475°C. The critical crack tip opening displacement for stable crack growth, i.e. the crack initiation toughness, was measured using the direct-current-potential drop crack monitoring technique. A quantitative model for the effect of temperature and age-hardening on the brittle crack initiation toughness is described.     

THE INFLUENCE OF AGEING AT INTERMEDIATE TEMPERATURES ON THE MECHANICAL BEHAVIOUR OF A DUPLEX STAINLESS STEEL: Part II. FATIGUE LIFE AND FATIGUE CRACK GROWTH

Abstract— The mechanical behaviour of AISI 329 steel has been investigated for ageing times up to 20,000 h at temperatures of 475, 425, 375, 325 and 275°C. The study has concentrated on the changes in the response to cyclic strains, in the low-and the high-cycle fatigue regimes, and in the resistance to fatigue crack propagation as a function of temperature and time of ageing.
It is shown that ageing increases the fatigue resistance in the high-cycle fatigue regime, but the opposite occurs in the low-cycle fatigue regime. Ageing increases the LEFM threshold stress intensity factor range for fatigue crack propagation which reaches high values in these alloys, and is influenced by the fatigue load ratio. Crack closure contributes to the LEFM threshold stress intensity factor range for crack propagation only in the annealed condition of the AISI 329 steel.     

THE BRITTLE FRACTURE OF 475°C EMBRITTLED CAST DUPLEX STAINLESS STEEL

Abstract— The fracture behaviour of cast duplex stainless steels, heat treated to different ferrite contents and hardness was investigated using tensile and notched bend tests. The purpose was to identify the microstructural features which controlled the ductile-to-brittle fracture transition of 475°C embrittled duplex stainless steel. The results indicate that twin nucleated cleavage has a tensile stress fracture criteria and the brittle-to-ductile transition temperature depends on ferrite microhardness, ferrite grain size and constraint.     

Fracture toughness prediction of aged CF8M using small punch test

Following Ref. 1 , this technical note presents a method to predict the thermal ageing effect on fracture toughness of cast stainless steel CF8M from the small punch test using finite element (FE) damage analysis. A procedure is given to extract tensile properties and multi‐axial fracture strain locus of aged CF8M from the small punch test using FE analysis. It is further shown that fracture toughness of aged CF8M can be predicted from the small punch test using FE damage analysis. Comparison with experimental data shows good agreement.     

Effect of Layers Position on Fracture Toughness of Functionally Graded Steels in Crack Divider Configuration

In the present study, fracture toughness of functionally graded steels in crack divider configuration has been modeled. By utilizing plain carbon and austenitic stainless steels slices with various thicknesses and arrange- ments as electroslag remelting electrodes, functionally graded steels were produced. The fracture toughness of the functionally graded steels in crack divider configuration has been found to depend on the composites’ type together with the volume fraction and the position of the containing phases. According to the area under stress-strain curve of each layer in the functionally graded steels, a mathematical model has been presented for predicting fracture toughness of composites by using the rule of mixtures. The fracture toughness of each layer has been modified according to the position of that layer where for the edge layers, net plane stress condition was supposed and for the central layers, net plane strain condition was presumed. There is a good agreement between experimental results and those acquired from the analytical model.     

Fatigue, monotonic and fracture toughness properties of a Cr–Mn–N steel

The low-cycle fatigue, monotonic and fracture toughness behaviour of E3949, a Cr–Mn–N austenitic stainless steel, used for drillcollar connections was studied. Low-cycle fatigue tests were carried out at room temperature under total strain control in the range of 0.40 to 1.50% using Companion Specimens Test (CST) and Incremental Step Test (IST) methods. Cyclic softening without saturation was observed in all tests. Massing cyclic stress–strain behaviour was observed only with the IST method. The fatigue life behaviour obeyed Basquin and Coffin–Manson relationships and the high value obtained for ′_f imparts a significant improvement in fatigue resistance of this alloy compared to AISI 304LN. The J–R curves and J_IC values were obtained at room temperature and at 150°C by using single specimens and the elastic compliance technique for crack length measurement. The observed decrease in crack initiation fracture toughness at 150°C is proposed to be due to a dynamic strain ageing effect, which impairs ductility.     

A Gurson–Tvergaard based model to simulate the fracture of aged duplex stainless steels

In order to use duplex stainless steels for components designed to withstand temperatures up to 475 °C, the knowledge of the effect of ageing on the fracture mechanisms is required. For the unaged steel, the ductile fracture takes place due to the nucleation of microvoids initiated on precipitates and inclusions present in the austenitic phase. However, the ageing of the material leads to a global loss of ductility. The ferrite phase embrittlement causes it to break by cleavage at lower levels of plastic strain. These changes, both in mechanical properties and in fracture micromechanisms, can be simulated by means of variation in the parameters that govern the constitutive equation of the material. The local approach model developed by Gurson–Tvergaard has been used to simulate, by FE analysis, the elasto‐plastic behaviour and the fracture of these materials at various stages of ageing at 400 °C. An extensive experimental program has been undertaken in order to obtain the Gurson–Tvergaard model parameters needed for numerical simulations, which considers the effect of ageing conditions (time and temperature), the ferrite content of the steel that causes the global embrittlement and the geometry of the component from the stress triaxiality by using axisymmetric notched specimens. The numerical model developed allows predictions to be made for the damage constitutive parameters for duplex steels subjected to any ageing conditions and, as a consequence, can be directly used for designing components.     

Effect of aging on fracture behaviour of cast stainless steel and weldments

Abstract

An investigation has been undertaken to determine the magnitude of any reduction in properties that may occur in cast duplex stainless steels and weldments during long term exposure to reactor operating conditions. Test panels were fabricated in CF3 stainless steel using a manual metal arc (MMA) process and 19.9.L consumables. The mechanical properties of the parent material and weldments were measured following accelerated aging at 375 and 400°C for up to 20 000 h. Following aging at temperatures up to 400°C, reductions in both the Charpy impact and J integral–crack growth resistance R (J–R) fracture toughness of CF3 cast austenitic steel and 19.9.L austenitic weld metal were observed. For conditions equivalent to the proposed end of life for UK pressurised water reactors, the J–R fracture toughness at 300°C of both cast steel and MMA weld metal was reduced by ~30% for crack extensions of ≥1 mm. Hence, it is important that these reductions in weld metal toughness are taken into account during the development of safety cases and structural integrity assessments for any component in the primary loop that contains MMA stainless steel weldments.

MST/1198     

Static fracture toughness of ultra-fine grained steels processed by thermo-mechanical warm rolling

Ultra-fine grained steels were recently developed by thermo-mechanical warm rolling. Their low-temperature fracture toughness was evaluated in terms of crack tip opening displacement (CTOD) in this paper. Effect of temperature on CTOD and the correlation between CTOD and grain size were investigated, and the experimental results showed that refining ferrite grains can increase the fracture toughness of steel and lower the sensitivity of fracture toughness to temperature. The fracture toughness of the developed ultra-fine grained steels was superior to that of hot-rolled steel SM490B with similar chemical composition.     

Effect of aging on high temperature brittle intergranular fracture in austenitic stainless steels

Abstract

The present paper describes the effect of aging on crack growth at 550–750°C in a series of 316 and 347 based stainless steels. Crack initiation parameters and crack growth rates have been measured, and detailed fractography and microstructural characterisation carried out. The study shows that the high temperature brittle intergranular fracture mechanism operates in these alloys, as expected from incidences of cracking in austenitic stainless steels used in power plant. High temperature brittle intergranular fracture leads to lower crack tip opening displacements at initiation, and slightly higher crack growth rates than ductile intergranular failure. Susceptibility to high temperature brittle intergranular fracture is enhanced by aging. This increased susceptibility is explained in terms of the increased hardness, the reduction in dissolved C, and grain boundary precipitation. The effects of temperature, composition, and loading mode on the behaviour of the aged alloys are determined.

MST/3100     

Fracture toughness and crack growth resistance of pressure vessel plate and weld metal steels

Compact tension specimens were used to measure the initiation fracture toughness and crack growth resistance of pressure vessel steel plates and submerged are weld metal. Plate test specimens were manufactured from four different casts of steel comprising: aluminium killed C-Mn-Mo-Cu and C-Mn steel and two silicon killed C-Mn steels. Weld metal test specimens were extracted from five weld joints of Unionmelt No. 2 weld metal. The welds were of double V butt geometry having either the C-Mn-Mo-Cu steel (three weld joints) or one particular silicon killed C-Mn steel (two weld joints) as parent plate. On the upper shelf, a multiple specimen test technique was used to obtain crack growth data which were analysed by simple linear regression to determine the crack growth resistance lines and to derive the initiation fracture toughness values for each test temperature. These regression lines were highly scattered with respect to temperature and it was very difficult to determine precisely the temperature dependence of the initiation fracture toughness and crack growth resistance. The data were re-analysed, using a multiple linear regression method, to obtain a relationship between the materials' crack growth resistance and toughness, and the principal independent variables (temperature, crack growth, weld joint code and strain ageing).