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对某钙基膨润土进行物理提纯试验,确定湿法提纯有利于得到高纯度蒙脱石。车间采用二次旋流分力分级法提纯得到了蒙脱石含量≥95%的提纯精矿,通过物理化学性能测试、XRD、电镜等表征,该提纯土达到了医药蒙脱石要求。 相似文献
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工业酒精、食用酒精、无水酒精是酒精生产的三大方面.根据三者对酒精质量要求的不同,应采用不同的提纯方法.其中,食用酒精GB10343-2000新标准要求普级95.5%(v/v)以上,因此,食用酒精提纯技术能较合适地反映酒精提纯技术水平.着重阐述了食用酒精提纯的提纯等技术,并简要介绍了无水酒精提纯的传统技术和非传统技术. 相似文献
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采用酸处理法提纯隐晶质石墨(CG)可将其固定碳质量分数提高到0.94,但仍残留少量难以除去的石英。采用乳液共混法制备CG/炭黑/羧基丁腈橡胶复合材料,研究CG提纯对复合材料性能的影响。结果表明:未提纯CG和提纯CG在橡胶基体中分散都较为均匀,但提纯CG具有更高的补强效率和更为优异的润滑性;添加提纯CG的复合材料摩擦因数和比磨损率均小于添加未提纯CG的复合材料,这可能是由于提纯CG中硬质杂质(如晶质石英)含量降低,在摩擦过程中更容易形成连续润滑膜和转移膜的缘故。 相似文献
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对稳态强磁场装置水冷磁体中去离子水提纯系统的各项指标和提纯模式进行了分析,并对以往提纯模式的不足进行了改进,提出了一种新的提纯模式。改进后,基本上可以做到切换磁体后无需等待即刻实验,提纯速度得到大幅提升。 相似文献
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不同粒度红柱石对矾土基喷涂料性能的影响 总被引:1,自引:0,他引:1
以矾土为主要原料,铝酸钙水泥、硅微粉为结合系统,分别研究了不同粒度的红柱石对矾土基喷涂料性能的影响。试样自然干燥24h脱模,再经110℃烘干24h,分别于1000℃、1300℃和1500℃热处理3h。检测各温度热处理后试样的线变化率、体积密度、常温抗折强度、常温耐压强度以及试样的热膨胀系数、耐磨性能和抗热震性能。结果表明,添加粗粒度的红柱石并不能有效弥补矾土基喷涂料经高温热处理产生的收缩。矾土基喷涂料的体积密度随着红柱石粒度的增大而增大。不同粒度的红柱石未对矾土基喷涂料的中温强度产生明显影响,粗粒度的红柱石可以提高矾土基喷涂料的高温强度。矾土基喷涂料的耐磨性能随着红柱石粒度的增大而提高。细粒度的红柱石有利于改善矾土基喷涂料的抗热震性能。 相似文献
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Results are provided for comparative evaluation of the properties of pressed specimens of a matrix system and ceramic concrete
specimens prepared on the basis of bauxite with very fine quartz glass and quartz sand (VFQG and VFQS), and also the thermal
expansion of castings based on a suspension of quartz sand, bauxite and bauxite ceramic concrete. It is established that high-silica
molded and unmolded ceramic concretes prepared on a basis of bauxite VFQG (85%) and VFQS (15%) have improved physicomechanical
properties. After firing at 1150 and 1420°C their open porosity is 16 – 18% and the ultimate strength in compression is 95
– 125 MPa. Their temperature for the onset of softening is above 1570°C and higher than 1650°C (for compositions containing
SiC).
Part 1 was published in Novye Ogneupory, No. 1 (2009).
Translated from Novye Ogneupory, No. 3, pp. 34 – 40, March 2009. 相似文献
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Vijay Kumar Vinay Kumar Singh Abhinav Srivastava 《Journal of the American Ceramic Society》2013,96(7):2124-2131
In the present investigations nano size high alumina cements (HAC) were prepared by very effective co‐melt precursor sintering technique from their metal nitrate precursors. The prime cementing phases observed were CA, CA2, and C12A7. The addition of nano structured cements in refractory castables has improved the thermo‐chemical‐mechanical properties to a significant extent. Each batch of low cement castables (LCC) was prepared from calcined Chinese bauxite, HAC, and superfine additives. The effect of HAC in bauxite castable with the additives similar to Silicon Carbide, reactive alumina, and micro‐fine silica on the sinterability and properties of these castables was investigated. Physical properties such as apparent porosity and bulk density, mechanical properties such as hot modulus of rupture (HMOR), cold and hot modulus of rupture (CMOR), and cold crushing strength (CCS) of hydrated and sintered castables were studied. The sintered castables were also characterized for their solid phase compositions and microstructure using X‐ray diffraction (XRD) and FE‐SEM, respectively. In the castables new phases such as mullite, α‐alumina were formed at the expense of bauxite and silica. Solid solution of mullite formed at high temperature acts as a bonding phase and is accounted for high HMOR, CMOR, and CCS values. These excellent properties of such castables may enable their uses in various applications such as refractory lining for fabrication of steel, aluminium, copper, glass, cement, chemicals, and ceramics. 相似文献
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新一代矾土基耐火材料 总被引:5,自引:0,他引:5
可以期望在新世纪我国根据丰富的高铝矾土资源特点,新一代矾土基耐火材料将会兴起--优质合成原料和高效耐火新产品.优质合成原料包括:(1)Al2O3含量为50%~90%的均质矾土熟料(均质类);(2)矾土基烧结和电熔锆刚玉莫来石和锆刚玉尖晶石系合成料(改性类);(3)矾土基Sialon和Alon(转型类).利用这些合成料开发的矾土基高效新产品为:(1)高温性能优良的高品位高铝砖和浇注料,(2)矾土基刚玉系材料,(3)矾土基Al2O3-Sialon(Alon)复合材料. 相似文献
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The characteristics of bauxite tailing in China were reviewed,and the current utilization methods and the actuality were discussed.It is found that the bauxite tailing is mainly used for production of building materials and chemical products,and extraction of useful component,etc.Meanwhile,the shortages of these utilization methods were analyzed.In order to enlarge the bauxite tailing application,some new utilization paths were proposed,such as preparing zeolite 4A and corundum-mullite composite materials,which are high value added materials.The utilization ways of bauxite tailing were widened,the utilization ratio of resources and the economic benefit were improved. 相似文献
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为制备保温性能及机械性能均较优异的高温窑炉用隔热耐火材料,以多孔球形莫来石、矾土细粉、α-Al2O3微粉、硅微粉和Secar71水泥为主要原料,制备了多孔球形莫来石基浇注料,研究了矾土细粉掺量对多孔球形莫来石基浇注料机械性能、导热系数、抗侵蚀性能及热震稳定性的影响。结果表明,改变矾土细粉的掺量,可使多孔球形莫来石基浇注料在保持较高机械性能的基础上提高保温性、热震稳定性和抗侵蚀性能。随着矾土细粉掺量的增加,多孔球形莫来石基浇注料的机械性能变化不大,但导热系数小幅降低,抗侵蚀性能出现较大差异,热震稳定性先提高后降低。当矾土细粉掺量为28%(质量分数)时,多孔球形莫来石基浇注料的机械性能、热震稳定性及抗侵蚀性能良好,在1 000 ℃时导热系数为0.905 W·m-1·K-1。多孔球形莫来石基浇注料的导热系数低于中间包和钢包永久层用高铝浇注料,可替代中间包、钢包永久层用高铝浇注料以减少热损失。 相似文献
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采用煤矸石废料、劣质原料黑滑石和铝钒土为主要原料,通过原位生长法制备了堇青石质低膨胀高远红外瓷质卫生陶瓷。利用XRD、SEM和性能测试研究铝钒土含量对堇青石卫生陶瓷性能的影响。实验结果表明:铝钒土含量对吸水率、抗折强度和膨胀系数具有较明显的影响,而对远红外辐射率并未带来不利的影响,所有样品的远红外率均保持在0.93以上。当铝钒土含量为27%,煤矸石33wt.%,黑滑石37%时,陶瓷性能达到最优:吸水率为0.04%,热膨胀系数为2.74×10-6/℃,抗折强度为87.4 MPa。这主要是由于样品的主晶相堇青石含量最高,并且烧结致密化程度高,其中气孔分布更加均匀所致。相关研究结果对环境保护和工业废物的资源化利用有着积极意义。 相似文献
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以改性后铝土矿石为载体,采用两步浸渍法,制备Ni-Mn-K一氧化碳高温变换催化剂。采用活性评价、低温N2吸附、XRD和TPR等表征方法,考察催化剂的结构和性能。结果表明,改性后的铝土矿本身具有一定的变换活性,用该载体负载多组分制得的催化剂具有较好的变换活性。XRD和TPR结果表明,催化剂中具有明显的晶相NiO和K2CO3的特征衍射峰, MnO2与铝土矿载体中的Fe3O2和SiO2形成非晶态复合氧化物。比表面积和孔容减小主要因负载引起,负载活性组分后使耗氢量增大,还原峰温降低。 相似文献