共查询到20条相似文献,搜索用时 78 毫秒
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杨晓东;刘彦峰;高庆和;谢方明;王锐;陆雪峰;高善彬 《化工中间体》2013,(9):30-33
本文概括了近些年介-微孔复合分子筛的合成研究工作,从两种主要的复合方式入手,综述了原位合成方法和后合成法。原位合成法主要包括单模板合成法和双模板合成法,后合成法主要介绍了孔壁晶化法、附晶生长法和微孔沸石硅源法三种代表性的合成方法。文章并分别对归属每种合成方法的具体合成方法进行了介绍,最后对介-微孔复合分子筛的合成进行了综述展望。 相似文献
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介绍了国内外合成丁辛醇的工艺技术进展情况,包括戴维合成法、三菱化成合成法、巴斯夫合成法等。在比较不同生产工艺路线的同时,从现有技术成熟角度和应用情况对比,提出了低压羰基法合成丁辛醇的选择原则。同时阐述了未来丁辛醇合成技术的发展趋势。 相似文献
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概括了近几年微孔-介孔复合分子筛的合成研究工作,主要介绍了原位合成法、后合成法和纳米组装法。原位合成法主要包括单模板合成法与双模板合成法;后合成法主要包括孔壁晶化法、附晶生长法、水热重组法、碱处理法、机械混合法与包埋法。最后对微孔-介孔复合分子筛的发展远景进行了展望。 相似文献
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Drill cutting decontamination by microwave drying has been studied over the past few years and has proved to be a promising technology. This study aimed to investigate fundamental aspects of kinetics of heating and drying of drilling fluids and drill cuttings by microwaves. The microwave heating curve of cuttings free of fluid, drilling fluids, and pure organic compounds usually used in the formulation of these fluids was evaluated to understand the behavior of each component in microwave cutting decontamination. Furthermore, commercial software was used to describe the heating kinetics of the drilling fluids used in this study. The drying kinetics of cuttings contaminated with these drilling fluids was also studied at three temperatures of control. Some classic models of conventional drying of solids were used to describe the removal kinetics of the liquid components present in contaminated cuttings (water and organic compounds). Important aspects related to the interaction of these components in the drying operation and solid heating, water evaporation, and the drag of organic compounds were investigated. Both drilling fluids showed a very similar kinetic heating. Pure organic bases did not show a significant heating. For the same drying time, the removal of paraffin is more intense than the olefin. In respect to organic component removal from cuttings contaminated with both fluids, the kinetic drying curves are similar. The Page model was the one that best describes the drying operation of drill cuttings contaminated with both drilling fluids. The microwave drying model (MDM) model is proposed in this work as a simple modification in the Henderson–Pabis model: the addition of a third parameter. The incorporation of this parameter enabled a better fit of the experimental data. Computational simulations show an electric field with symmetrical patterns for the two BR-MUL fluids analyzed. 相似文献
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Feiyue Ren Zhihang Zhang Michael T. Gaffney Joseph P. Kerry Brijesh K. Tiwari 《Drying Technology》2018,36(4):435-447
The effects of four drying treatments (freeze-drying, hot air drying, oven drying, and vacuum oven drying) on the bioactive compounds (total phenolics, total flavonoids, and quercetins), color, and antioxidant capacity of organic and nonorganic onions of two varieties (Red Baron and Hyfort) subjected to two agronomic treatments (OSOP and CSCP) were investigated. The average final dry weight of the samples was 9.82?±?0.41%. After drying, there was a significant increase in total phenolics, total flavonoids, total quercetin, and antioxidant capacity in comparison with fresh onion samples, which suggested that drying can improve the extractability of phenols and accordingly the antioxidant activity of onions. Different drying techniques also resulted in different fractions of individual quercetins. Dried organic onions had higher levels of bioactive compounds and antioxidant capacity than dried nonorganic onions for a same variety. The highest antioxidant capacity displayed by freeze-dried and hot-air-dried organic Red Baron onion is in agreement with their higher phenolic and flavonoid contents compared to all other samples. 相似文献
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Drying kinetics of volatile organic solvents have been examined during the drying process of a pharmaceutical coating containing a multicomponent mixture of ethyl acetate, n-heptane, propanol-2, and toluene. A complete set of experiments was performed in two drying apparatuses, a laboratory air-dryer and an oven dryer, for a wide range of drying temperature, air velocity, initial coating thickness and drying time. An empirical kinetic model is used to predict the concentration of each organic solvent in the mixture during the drying process. The results show that both drying conditions and sample characteristics affect significantly the drying rate of solvents. 相似文献
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ABSTRACT Drying kinetics of volatile organic solvents have been examined during the drying process of a pharmaceutical coating containing a multicomponent mixture of ethyl acetate, n-heptane, propanol-2, and toluene. A complete set of experiments was performed in two drying apparatuses, a laboratory air-dryer and an oven dryer, for a wide range of drying temperature, air velocity, initial coating thickness and drying time. An empirical kinetic model is used to predict the concentration of each organic solvent in the mixture during the drying process. The results show that both drying conditions and sample characteristics affect significantly the drying rate of solvents. 相似文献
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Brendan C. O'Kelly 《Drying Technology》2004,22(7):1767-1776
The accuracy of moisture content values determined for organic soil using the oven drying method is dependent on the oven drying temperature. Some charring of the organic fraction occurs at the standard oven drying temperature of 110 ± 5°C; pore water remains in the soil when temperatures below 100°C are used. A new technique to determine the specific oven drying temperature that yields the correct value of the moisture content for organic soils is presented. Routine moisture content tests should be conducted at the standard oven drying temperature; moisture content values determined on the basis of the recommended oven drying temperature of 60°C include a larger error. A moisture content parameter is introduced to facilitate direct comparison of moisture content values calculated on the basis of different oven drying temperatures. 相似文献
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Requirements of organic gels for a successful ambient pressure drying preparation of carbon aerogels 总被引:1,自引:0,他引:1
In this paper, we investigated the requirements of organic gels for a successful ambient pressure drying by analyzing the
role of the strength, the pore size and the surfactant of organic gels in decreasing the drying shrinkage of organic aerogels.
Experimental results showed the effect of the decrease of the surface tension, resulting from the surfactant, on the drying
shrinkage was very small and negligible. The drying shrinkage depended strongly on the strength and the pore size. Subsequently,
the respective role of the strength and the pore size was evaluated. It can be found that the strength plays a greater role
than the pore size. 相似文献
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Microwave Drying of Wood Strands 总被引:2,自引:0,他引:2
Characteristics of microwave drying of wood strands with different initial moisture contents and geometries were investigated using a commercial small microwave oven under different power inputs. Temperature and moisture changes along with the drying efficiency were examined at different drying scenarios. Extractives were analyzed using gas chromatography/mass spectrometry (GC/MS). The results showed that the microwave drying process consisted of three distinct periods (warm-up period, evaporation period, and heating-up period) during which the temperature, moisture change, and drying efficiency could vary. Most of the extractives were remnant during microwave drying. It was observed that with proper selections of power input, weight of drying material, and drying time, microwave drying could increase the drying rate, save up to 50% of energy consumption, and decrease volatile organic compound (VOC) emissions when compared with the conventional drying method. 相似文献
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Response Surface Methodology (RSM) was used for optimizing the drying technology of sweet pepper under low-vacuum. It was found that pH value has greater influence on the organic Se index, while drying temperature has greater effect on the chlorophyll index. The optimized parameters of drying temperature, pH value and blanching time were obtained, respectively. 相似文献
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《Drying Technology》2013,31(7):1767-1776
Abstract The accuracy of moisture content values determined for organic soil using the oven drying method is dependent on the oven drying temperature. Some charring of the organic fraction occurs at the standard oven drying temperature of 110 ± 5°C; pore water remains in the soil when temperatures below 100°C are used. A new technique to determine the specific oven drying temperature that yields the correct value of the moisture content for organic soils is presented. Routine moisture content tests should be conducted at the standard oven drying temperature; moisture content values determined on the basis of the recommended oven drying temperature of 60°C include a larger error. A moisture content parameter is introduced to facilitate direct comparison of moisture content values calculated on the basis of different oven drying temperatures. 相似文献
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Abstract Characteristics of microwave drying of wood strands with different initial moisture contents and geometries were investigated using a commercial small microwave oven under different power inputs. Temperature and moisture changes along with the drying efficiency were examined at different drying scenarios. Extractives were analyzed using gas chromatography/mass spectrometry (GC/MS). The results showed that the microwave drying process consisted of three distinct periods (warm-up period, evaporation period, and heating-up period) during which the temperature, moisture change, and drying efficiency could vary. Most of the extractives were remnant during microwave drying. It was observed that with proper selections of power input, weight of drying material, and drying time, microwave drying could increase the drying rate, save up to 50% of energy consumption, and decrease volatile organic compound (VOC) emissions when compared with the conventional drying method. 相似文献