石油钻杆材料G105在不同条件下的疲劳断裂

采用国产PQ-6型旋转弯曲疲劳试验机研究钻杆管体材料G105的弯曲疲劳性能以及H_2S腐蚀和缺口对试样弯曲疲劳性能的影响,利用金相显微镜和扫描电子显微镜对光滑试样断口、缺口试样断口以及H_2S腐蚀后试样断口进行微观形貌分析。结果表明:在光滑试样的疲劳极限载荷作用下,经过H_2S腐蚀后的光滑试样的疲劳寿命和缺口试样的疲劳寿命相当,材料的疲劳寿命都从106降低至104;缺口试样在缺口的高应力集中效应下,加快疲劳裂纹形核过程。H_2S腐蚀对钻杆疲劳性能影响的主要作用在于氢原子在材料内缺陷处聚集引起材料疲劳性能降低,缺口和H_2S腐蚀都会加快疲劳裂纹的扩展。材料疲劳断裂主要是因为试样在交变应力的作用下上产生滑移最后致使位错塞积而导致的。     

TNM-Ti Al合金室温高周疲劳性能研究

采用升降法与成组法对TNM-TiAl合金试样进行了应力比R=-1的室温拉压疲劳和R=0.1的室温拉伸疲劳试验，得到TNM-TiAl合金的P-S-N曲线，并对断口进行了分析。结果表明:TNM-TiAl合金对应力十分敏感，R=-1和R=0.1时的曲线整体呈较为平直的斜线，R=-1时的疲劳极限为414.7 MPa,R=0.1时的疲劳极限为285.6 MPa。R=0.1的S-N曲线远低于R=-1的S-N曲线;R=-1时，应力幅与疲劳寿命的关系满足Basquin方程。疲劳试件宏观断口较为粗糙，静态拉伸宏观断口平整，两者差异较大。拉伸断口整体分为裂纹萌生区与扩展区，其中起裂源均位于试样表面或板状试件的边角棱线处，起裂源区域包括γ相的解理断裂面、片层团的沿层解理面以及β₀相平整的穿晶断裂平面等特征。疲劳断口整体分为裂纹萌生区、扩展区与瞬断区，其中裂纹萌生区分为表面沿层起裂和γ相起裂。TNM-TiAl合金的疲劳断裂为脆性断裂，主要体现在扩展区上大量的片层团穿层断裂、扭折撕裂、γ相解理断裂和β₀相穿晶断裂。同寿命量级下，R=-1的断口与R=0.1的断口断裂类型...     

缺口对7A85铝合金拉伸性能和疲劳性能的影响

在光滑试样表面预制深度为0.1 mm和0.2 mm的环状缺口，研究了不同缺口尺寸对7A85铝合金拉伸性能和疲劳性能的影响，并分析了7A85铝合金含缺口试样的疲劳断裂机理。结果表明，随着缺口深度由0 mm增加至0.2 mm, 7A85铝合金试样的抗拉强度、断后伸长率和疲劳强度分别下降了6%、47.5%、44.4%。缺口对7A85铝合金塑性的影响远大于拉伸强度，且其抗拉强度与疲劳强度呈线性关系。试样疲劳缺口系数随着缺口尺寸和循环次数的增加而增大。7A85铝合金试样的疲劳裂纹源通常是富铁的第二相颗粒，环状缺口根部应力集中促进了多疲劳裂纹源萌生，多个裂纹源同时扩展使得试样有效承载面积快速减少，导致疲劳寿命急剧缩短。     

Ti—15—3钛合金的疲劳断裂行为研究

研究了Ｔｉ－１５－３合金板材光滑和缺口疲劳及疲劳裂纹萌和方式，发现光滑疲劳试样裂纹多起源于板材原始表面，形成面源；面具有中心孔和边缺口试样的疲劳裂纹多起源于缺口处的机加工端面，形成角源的线源。而且５２０℃时效后所获得的板材的拉伸强度是比５４０℃时效的高７３ＭＰａ，但疲劳极限差别不大。     

TC21合金315℃高周疲劳光滑和缺口试样断口分析

开展了TC21研究合金光滑和缺口试样的315℃高周疲劳实验,并对疲劳断口进行详细观察,研究了缺口对TC21合金疲劳寿命的影响.结果表明,光滑和缺口试样的疲劳强度比值随循环寿命降低而降低;光滑试样的失稳疲劳裂纹长度随循环应力升高而降低;瞬断区所承受的断裂应力随循环应力升高而降低;这说明裂纹失稳决定试样的断裂,缺口试样断口有多个裂纹源,以缺口试样名义应力乘以应力集中因子与光滑试样的应力相等作为比较时,缺口试样主裂纹长度大于光滑试样的裂纹长度,缺口试样的裂纹扩展寿命更长.     

镍基单晶合金中温疲劳性能应力集中敏感性

疲劳是涡轮叶片的一种主要失效模式.本文开展了DD11单晶合金在650℃中温条件下2种应力集中系数(K_t=1(光滑状态)、K_t=3(缺口状态))的旋转弯曲疲劳性能研究,对比了2种应力集中系数下的疲劳强度,并开展了相关断口分析.结果表明:应力集中系数由K_t=1增大到K_t=3时,疲劳极限由446 MPa降低为311 MPa,说明DD11单晶合金疲劳性能存在应力集中敏感性;疲劳寿命由10~5提高到10~7时,光滑状态由600 MPa降低为420 MPa,疲劳强度降低幅度为180 MPa,而缺口状态由370 MPa降低为290 MPa,降低幅度为80 MPa,说明应力集中条件下DD11单晶合金的疲劳寿命对于外载变化较敏感.断口分析表明,光滑试样断口(应力500 MPa/疲劳寿命9.7×10~5)由几个相交的光滑晶体学平面组成,疲劳源萌生在距表面100μm左右的铸造孔洞;缺口试样断口(应力340 MPa/疲劳寿命8.1×10~5试样)呈平面状,与应力轴垂直,为多源疲劳模式,疲劳源观察到小刻面,在加工刀痕不连续位置萌生.     

残余压应力场中疲劳裂纹的止裂

20Cr钢在不同缺口尖锐度下滚压后疲劳试验结果表明,滚压强化明显提高缺口试样的疲劳极限,其作用高于光滑试样,缺口越尖锐强化效果越显著。在缺口滚压试样疲劳断口上出现裂纹扩展速率快—慢—快的变化。缺口试样滚压后在疲劳极限下运行出现非扩展裂纹。     

LC9CGS3铝合金光滑与缺口疲劳试样在不同载荷条件下的断裂行为

用ＳＥＭ电镜观察分析了ＬＣ９ＣＧＳ３铝合金在不同载荷下光滑与缺口疲劳试样的断裂行为。结果表明：两种试样的疲劳裂纹均为两阶段扩方式，而且疲劳裂纹Ⅰ阶段扩民菜区面积随应降低而增大。     

返回料添加比例对K44合金热疲劳性能的影响

研究了返回料添加比例对新型抗热腐蚀高温合金K44热疲劳性能的影响.结果表明:新料和返回料合金试样V型缺口尖端主裂纹扩展长度与热循环次数之间遵循L=bNa规律.新料合金热疲劳裂纹萌生和扩展速率最低,随着合金中返回料比例的增大,热疲劳裂纹萌生速率和扩展速率也增大.热疲劳裂纹萌生于V型缺口尖端附近区域,沿枝晶间、晶界和开裂的碳化物扩展,主裂纹扩展以裂纹尖端连续开裂的形式进行.返回料合金由于氮含量增加导致共晶和夹杂物增多,碳化物聚集块化,加速了热疲劳裂纹的萌生与扩展.合金经热疲劳实验后,裂纹两侧产生氧化带和γ'相贫化带.     

应力幅对退火态Mg-3Al-2Sc合金疲劳行为的影响

在不同应力幅下对退火处理后的Mg-3Al-2Sc合金进行应力控制的疲劳实验,研究应力幅对合金的裂纹扩展行为和断裂机制的影响。结果表明:在12～75MPa应力范围内,当控制应力比为0.2,随着应力幅增加,裂纹扩展速率增加,Mg-3Al-2Sc合金的疲劳断裂寿命降低。在裂纹萌生区合金主要表现为解理断裂机制,进入裂纹稳定扩展阶段的疲劳断裂主要为准解理断裂。而在瞬断区,低应力幅时主要表现为准解理断裂,高应力幅时主要表现为微孔聚合断裂。     

2219铝合金TIG和FSW接头力学及疲劳性能

目的 研究钨极氩弧焊(TIG)和搅拌摩擦焊(FSW)对2219铝合金(母材)力学及疲劳性能的影响。方法 通过拉伸试验,得到了母材、TIG和FSW接头的抗拉强度和伸长率;通过疲劳性能试验测试了母材、TIG和FSW接头在不同应力下相应的疲劳寿命,根据疲劳试验结果绘制了其试样的S-N曲线;使用扫描电子显微镜观察并分析了疲劳断口的形貌特征。结果 未焊接的铝合金母材抗拉强度和伸长率最高,分别为506 MPa和15.92%;TIG接头抗拉强度和伸长率分别为330 MPa和7.65%,FSW接头抗拉强度和伸长率分别为310 MPa和8.74%。母材、TIG和FSW接头等3种疲劳试样在2×10⁶次循环下的疲劳强度分别为129、108、115 MPa,其疲劳断口均可分为裂纹源区、裂纹扩展区和瞬间断裂区,疲劳裂纹分别起始于试样表面的局部变形区、第二相夹杂物和“吻接”缺陷。疲劳裂纹扩展区的主要形貌为疲劳辉纹和二次裂纹,瞬间断裂区以脆性断裂为主。结论 TIG和FSW等2种焊接工艺均导致了2219铝合金的强度、塑韧性和疲劳性能降低,其接头表面的第二相夹杂物和“吻接”缺陷促进了疲劳裂纹的萌生。     

MB8镁合金高周疲劳实验研究

采用升降法对MB8镁合金室温高周疲劳行为进行实验研究。结果表明:利用升降法计算出MB8镁合金在应力比R=0.1,循环基数为107条件下的疲劳强度为90.2MPa,相当于其抗拉强度的34%左右;合金的疲劳裂纹萌生于试样表面,裂纹扩展区由小的平面状断面组成,没有明显的疲劳辉纹存在,合金疲劳断口呈现韧性断裂特征。     

ZTC4（Ti-6Al-4V）铸造钛合金的室温低周疲劳行为

研究了ZTC4钛合金应变控制的室温低周疲劳行为,对循环应力-应变和应变疲劳寿命数据进行了分析,通过双对数线性回归处理,得出了Manson-Coffin处理模型的疲劳参数。结果表明：ZTC4钛合金总应变幅在0.6%～0.8%时,材料存在轻度循环软化的现象;总应变幅为0.4%～0.5%时,循环初期表现出循环硬化的现象,而后循环软化。合金的疲劳裂纹萌生于试样表面,裂纹扩展区存在明显的疲劳条带,合金疲劳断口呈现韧性断裂特征。     

Tensile and fatigue behaviour of wrought magnesium alloys AZ31 and AZ61

The mechanical behaviour of two hot rolled magnesium alloys, namely the AZ31 and AZ61, has been evaluated experimentally under both monotonic and cyclic loading. Both longitudinal (L) and long transverse (LT) directions were evaluated. The tensile behaviour of the L and LT directions is similar and differs only in the offset 0.2% yield strength for both materials. This difference is attributed to the angular spread of basal poles toward the rolling direction and is more pronounced for the case of AZ31. A distinct hardening response is obvious in both directions. Twinning formation was observed; it is more pronounced in the longitudinal direction while the fracture mode is intergranular and equiaxed facets are present in the fracture surfaces of the specimens. The S–N curves exhibit a smooth transition from the low to high cycle fatigue regime. AZ61 exhibits an overall better fatigue behaviour compared to AZ31. A transgranular crack initiation mode is observed in all tested specimens while the propagation of the cracks is characterized as intergranular.     

U75V重轨钢弯曲疲劳裂纹扩展行为EI北大核心

为明确珠光体钢轨的疲劳裂纹扩展行为,测定U75V重轨钢轧态和热处理态两种条件下的三点弯曲疲劳裂纹扩展速率,采用光学显微镜、扫描电镜、EBSD对钢轨的微观组织、片层、断口形貌及裂纹扩展轨迹进行观察。结果表明:轧态和热处理态钢轨的疲劳辉纹平均间距分别为253,215 nm,轧态钢轨的疲劳断口呈现解理台阶与河流花样形貌,且河流花样趋于合并,而热处理态钢轨的疲劳断口呈现大量的解理台阶及较多的微裂纹和撕裂棱,河流花样以支流为主;热处理态钢轨的疲劳裂纹扩展速率远低于轧态,到达裂纹失稳阶段也较滞后;轧态和热处理态钢轨的疲劳裂纹扩展都是以穿晶断裂为主的穿晶断裂和沿晶断裂混合扩展方式进行,轧态和热处理态钢轨的珠光体片层间距分别为272,148 nm,其中热处理态钢轨的珠光体片层细密且方向多样,存在显著的珠光体团簇,裂纹扩展轨迹中出现较多的分支裂纹和裂纹桥接现象,对扩展起到阻碍作用,是热处理态钢轨抗疲劳裂纹扩展能力优于轧态的重要原因。     

Crack-healing behaviour and resultant high-temperature fatigue strength of machined Si3N4/SiC composite ceramic

The crack‐healing behaviour of machining cracks in Si₃N₄/20 wt% SiC composite was investigated. The machining cracks were introduced by a heavy machining process, during the creation of a semicircular groove. The machined specimens were healed at various temperatures and times in air. The optimized crack‐healing condition of the machined specimens was found to be a temperature of 1673 K and a time of 10 h. The specimens healed by this condition exhibited almost the same strength as the smooth specimens healed. Moreover, the bending strengths and the fatigue limits of the machined specimens healed were systematically investigated at temperatures from room temperature to 1673 K. The machined specimens healed at the optimized condition exhibited an almost constant bending strength (～700 MPa) up to 1673 K. Also, the specimens exhibited considerably high cyclic and static fatigue limits at temperatures from 1073 to 1573 K. These results demonstrated that the crack‐healing could be an effective method for improving the structural integrity and reducing machining costs of the Si₃N₄/SiC composite ceramic.     

Three-point bending fatigue behavior of WC–Co cemented carbides

WC–Co cemented carbides with different WC grain sizes and Co binder contents were sintered and fabricated. The three-point bending specimens with a single edge notch were prepared for tests. In the experiments, the mechanical properties of materials were investigated under static and cyclic loads (20 Hz) in air at room temperature. The fatigue behaviors of the materials under the same applied loading conditions are presented and discussed. Optical microscope and scanning electron microscopy were used to investigate the micro-mechanisms of damage during fatigue, and the results were used to correlate with the mechanical fatigue behavior of WC–Co cemented carbides. Experimental results indicated that the fatigue fracture surfaces exhibited more fracture origins and diversification of crack propagation paths than the static strength fracture surfaces. The fatigue fracture typically originates from inhomogeneities or defects such as micropores or aggregates of WC grains near the notch tip. Moreover, due to the diversity and complexity of the fatigue mechanisms, together with the evolution of the crack tip and the ductile deformation zone, the fatigue properties of WC–Co cemented carbides were largely relevant with the combination of transverse rupture strength and fracture toughness, rather than only one of them. Transverse rupture strength dominated the fatigue behavior of carbides with low Co content, whilst the fatigue behavior of carbides with high Co content was determined by fracture toughness.     

EFFECT OF BIAXIAL MEAN STRESS ON CYCLIC STRESS-STRAIN RESPONSE AND BEHAVIOUR OF SHORT FATIGUE CRACKS IN A HIGH STRENGTH SPRING STEEL

Abstract— Biaxial fatigue tests were conducted on a high strength spring steel using hour-glass shaped smooth specimens. Four types of loading system were employed, i.e. (a) fully reversed cyclic torsion, (b) uniaxial push—pull, (c) fully reversed torsion with a superimposed axial static tension or compression stress, and (d) uniaxial push—pull with a superimposed static torque, to evaluate the effects of mean stress on the cyclic stress—strain response and short fatigue crack growth behaviour. Experimental results indicate that a biaxial mean stress has no apparent influence on the stress—strain response in torsion, however a superimposed tensile mean stress was detrimental to torsional fatigue strength. Similarly a superimposed static shear stress reduced the push—pull fatigue lifetime. A compressive mean stress was seen to be beneficial to torsion fatigue life. The role of mean stress on fatigue lifetime, under mixed mode loading, was investigated through experimental observations and theoretical analyses of short crack initiation and propagation. Using a plastic replication technique the effects of biaxial mean stress on both Stage I (mode II) and Stage II (mode I) short cracks were evaluated and analysed in detail. A two stage biaxial short fatigue crack growth model incorporating the influence of mean stress was subsequently developed and applied to correlate data of crack growth rate and fatigue life.     

航空铝合金原位腐蚀疲劳性能及断裂机理EI北大核心CSCD

为了研究不同腐蚀条件下2024铝合金的疲劳性能,首先设计搭建原位腐蚀疲劳平台,然后分别进行无腐蚀疲劳、预腐蚀疲劳和原位腐蚀疲劳实验,分析不同腐蚀疲劳条件下2024铝合金的疲劳断裂行为,最后利用扫描电镜(SEM)表征宏、微观断口特征,探究失效机理。结果表明:相同腐蚀环境和时间下,预腐蚀和原位腐蚀疲劳寿命分别为无腐蚀疲劳寿命的92%和42%;在原位腐蚀疲劳条件下,滑移带挤入、挤出导致表面粗糙度增加,吸附较多腐蚀介质,加剧蚀坑演化,易于裂纹萌生并形成多个裂纹源。裂纹的连通形成更大尺寸的损伤,并在材料内部快速扩展。预腐蚀和原位腐蚀疲劳试件断口观察到大量脆性疲劳条带,并且原位腐蚀疲劳条带平均间距约为无腐蚀疲劳条带间距的2倍,说明原位腐蚀疲劳条件下裂纹扩展速率更快。     

The effect of cerium on high-cycle fatigue properties of die-cast magnesium alloy

The effect of cerium (Ce) on high‐cycle fatigue behaviour of die‐cast magnesium alloy AZ91D was investigated. Mechanical fatigue tests were conducted at the stress ratio, R= 0.1 on specimens of AZ91D alloys with different Ce additions. The microstructure and fatigue fracture surfaces of specimens were examined using a scanning electron microscope (SEM) to reveal the micromechanisms of fatigue crack initiation and propagation. The results show that the grain size of AZ91D is refined, and the amount of porosity decreases and evenly distributes with the addition of Ce. The fatigue strength of AZ91D evaluated by the up‐and‐down load method increases from 96.7 MPa to 116.3 MPa (1% Ce) and 105.5 MPa (2% Ce), respectively. The fatigue cracking of AZ91D alloy initiates at porosities and inclusions of the alloy's interior, and propagates along the grain boundaries. The fatigue fracture surface of test specimens shows the mixed fracture characteristics of quasi‐cleavage and dimple.