织构与晶粒对挤锻复合成形AZ61镁合金力学性能的影响

采用AZ61镁合金挤压态预成形坯材,通过不同变形程度的模锻成形试验制备AZ61镁合金拉伸试样,运用金相观察、电子背散射衍射(EBSD)取向成像技术,分析了AZ61镁合金在挤锻复合成形过程中晶粒尺寸与织构对其室温力学性能的影响。结果表明,挤压态预成形试样存在强烈的基面织构,晶粒处于硬取向,基面滑移难以启动,AZ61镁合金具有较高的屈服强度。在基面织构强度相似的情况下,晶粒细化可提高试样的屈服强度和伸长率,但不能通过变形的无限增加改善合金的组织与性能。     

AZ31-0.4Nd挤压管材变形织构及力学各向异性EI北大核心CSCD

采用高温挤压的方法制备AZ31-0.4Nd合金管材,分析添加少量稀土元素Nd对AZ31合金挤压管材织构特征及力学性能的影响。结果表明:添加Nd有利于管材动态再结晶的发生,再结晶晶粒细小且分布均匀;添加Nd改变了合金的织构类型,弱化了基面织构;挤压管材纵向拉伸抗拉强度达236 MPa,伸长率达10.5%;管材力学性能呈各向异性,其主要原因是沿TD方向拉伸时可开动的基面滑移少、且利于{1012}孪晶形成,从而使得沿TD方向拉伸时的抗拉强度较高而伸长率较低。     

挤压ZAT522镁合金的组织与力学性能研究

研究了均匀化态与挤压态Mg-5Zn-2Al-2Sn(ZAT522)合金的微观结构、织构和力学性能。结果表明:挤压合金为完全动态再结晶结构,具有双峰晶粒尺寸。挤压合金的平均晶粒尺寸为11.2μm,在晶界与晶粒内部析出了大量细小Mg2Sn相,析出相的不均匀分布是导致双峰晶粒结构的主要原因;挤压合金中形成强的基面织构。此外,与均匀化合金相比,挤压的ZAT522合金具有优异的力学性能,其抗拉强度255 MPa、屈服强度114 MPa、伸长率32%。挤压合金强度显著增加主要归因于晶粒细化、沉淀强化和织构强化。     

Mg?RE挤压合金晶体学织构与力学性能各向异性分析

本论文研究了热挤压加工对Mg-1Gd-1Nd (wt.%)合金显微组织、织构及力学性能的影响。研究结果表明,铸态合金呈现典型的共晶显微组织,包含α-Mg基体及半连续状的共晶化合物。经过固溶热处理后,这些共晶化合物已基本固溶入α-Mg基体中。采用电子背散射衍射(EBSD)技术分析了挤压合金的显微组织与织构。结果表明,挤压合金显示出了完全再结晶的显微组织与弱的基面织构。合金中的晶粒基面同时朝向挤压板材的挤压方向与垂直方向偏移,尤其在挤压方向上晶粒的取向更加分散。这种分散的取向可以有效地激活合金中的基面滑移使得合金在断裂前能够承受更大的塑性变形。另一方面,织构也影响了合金力学性能的各向异性。     

Mg-RE挤压合金晶体学织构与力学性能各向异性分析（英文）

研究了热挤压加工对Mg-1Gd-1Nd(质量分数,%)合金显微组织、织构及力学性能的影响。结果表明,铸态合金呈现典型的共晶显微组织,包含α-Mg基体及半连续状的共晶化合物。经固溶热处理后,这些共晶化合物已基本固溶入α-Mg基体中。采用电子背散射衍射(EBSD)技术分析了挤压合金的显微组织与织构。结果表明,挤压合金显示出了完全再结晶的显微组织与弱的基面织构。合金中的晶粒基面同时朝向挤压板材的挤压方向与垂直方向偏移,尤其在挤压方向上晶粒的取向更加分散。这种分散的取向可以有效地激活合金中的基面滑移使得合金在断裂前能够承受更大的塑性变形。另一方面,织构也影响了合金力学性能的各向异性。     

不同轧制工艺对AZ31镁合金薄板室温成形性能的影响

采用常规轧制(NR)、异步轧制(DSR)和交叉轧制(CR)3种不同工艺来获得AZ31镁合金板材并进行室温成形性能的研究。结果表明:AZ31镁合金板材的综合力学性能不仅与晶粒尺寸有关,还与晶粒取向有关。基面织构的减弱可明显提高板材的胀形性能。异步轧制明显降低板材基面织构强度,使板材室温冲压性能得到提高。交叉轧制使晶粒显著细化,基面织构增强,提高了板材的力学性能,却降低其冲压成形性能;同时交叉轧制可以减弱板材各向异性。研究结果为改善镁合金室温塑性与成形性能提供了理论依据和新思路。     

温轧及退火对挤压AZ31B镁板室温各向异性的影响

以挤压AZ31B镁合金板为原料，通过温轧与退火制备了弱各向异性的镁薄板。研究了在温轧及随后退火过程中挤压镁板组织及各向异性的变化，获得在室温下具有较高综合力学性能与成形性(屈服强度>250 MPa,抗拉强度>300 MPa,伸长率>15%,杯突IE=2.8 mm),且各向异性低的板材。挤压镁板中的非基面织构将完全或部分中和后续轧制过程中的基面织构，是获得低各向异性的关键，随后的退火将进一步弱化板材的基面织构和各向异性。相比于伸长率，各向异性与成形性的相关性更大。     

织构和晶粒尺寸对AZ31镁合金薄板成形性能的影响

采用不同的轧制工艺,制备4种晶粒尺寸为7~18μm和不同强度基面织构的AZ31镁合金板材,通过单向拉伸试验和室温Erichsen试验,探讨晶粒尺寸与织构对镁合金板材室温成形性能的影响。结果表明:晶粒细化虽然增强了板材的力学性能,但不利于提高板材的胀形性能;基面织构的减弱使板材沿厚度方向变形能力增强,具有较好的胀形性能,但另一方面使板材的屈服强度降低。     

日本关于镁合金板材力学性能和成形性的最新研究

阐述了日本国内镁合金板材的应用和生产状况,在与其他合金相比较的基础上,综述了日本关于镁合金板材力学性能(拉伸强度和伸长率)和二次成形性(埃里克森值,拉伸极限和塑性应变比等参数)的最近研究结果,并且从机理上分析了微观组织对力学性能和成形性的影响。结果表明,晶粒细化和织构控制是提高镁合金力学性能和成形性的两个重要因素,当基面织构弱化到一定程度时,织构对力学性能和成形性的影响甚至会超过细化晶粒的效果。     

热轧AZ31镁合金薄板室温成形性能

针对AZ31镁合金板材室温冲压成形较差的特点,采用在不同轧制温度下获得的镁合金板材对其进行拉伸、埃里克森和锥杯试验,并通过光学电镜和X射线衍射仪对其显微组织、织构和成形性能等进行研究。结果表明,AZ31镁合金板材的综合力学性能不仅与晶粒尺寸有关,还与晶粒取向有关;基面织构的减弱可明显提高板材的胀形性能,在基面织构强度相似的强况下,晶粒大小对板材的成形性能起决定性影响。     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

THERMODYNAMICS STUDY ON THE DECOMPOSITION OF CHROMITE WITH KOH

Institute of Process Engineering, Chinese Academy of Sciences, China, has proposed a method for oxidative leaching of chromite with potassium hydroxide. Understanding the mechanism of chromite decomposition, especially in the potassium hydroxide fusion, is important for the optimization of the operating parameters of the oxidative leaching process. A traditional thermodynamic method is proposed and the thermal decomposition and the reaction decomposition during the oxidative leaching of chromite with KOH and oxygen is discussed, which suggests that chromite is mainly destroyed by reactions with KOH and oxygen. Meanwhile, equilibrium of the main reactions of the above process was calculated at different temperatures and oxygen partial pressures. The stable zones of productions, namely, K2CrO4 and Fe2O3, increase with the decrease of temperature, which indicates that higher temperature is not beneficial to thermodynamic reactions. In addition, a comparison of the general alkali methods is carried out, and it is concluded that the KOH leaching process is thermodynamically superior to the conventional chromate production process.     

INFLUENCE OF HEAT TREATMENT ON DAMPING BEHAVIOUR OF THE MAGNESIUM WROUGHT ALLOY AZ61

The effect of isochronal heat treatments for 1h on variation of damping, hardness and microstructural change of the magnesium wrought alloy AZ61 was investigated. Damping and hardness behaviour could be attributed to the evolution of precipitation process. The influence of precipitation on damping behaviour was explained in the framework of the dislocation string model of Granato and Lücke.     

Theoretical Analysis for the Motion and Temperature of Melt Droplets in Spray Degassing Process

The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results.     

Growth Kinetics of Single Inclusion Particle in Molten Melts

On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes＇ collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process.     

Three-Dimensional Growth of Coherent Ferrite in Austenite: A Molecular Dynamics Study

Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.     

An Easy Way to Quantify the Adhesion Energy of Nanostructured Cu/X(X=Cr,Ta,Mo,Nb,Zr) Multilayer Films Adherent to Polyimide Substrates

An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models.     

High-Speed Friction Stir Welding of SiC_p/Al–Mg–Si–Cu Composite

A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency.