Fatigue fracture of embedded copper conductors in multifunctional composite structures

The fatigue failure mechanisms of copper strips embedded into glass/epoxy were investigated. This combination of materials composes a multifunctional electrical-composite load bearing structure that is essential for systems such as large antennas integrated into aircraft skins. In smart structures applications, bulky and heavy wiring harnesses associated with densely deployed sensors, actuators, and devices can be avoided by using embedded electrical interconnects in a manner analogous to printed circuit boards. Since metals generally exhibit lower fatigue life relative to composites, understanding the failure mechanisms associated with embedded metal conductors is necessary for improving operational life. Specimens having 0.127 mm thick embedded copper strips were used to measure fatigue life as a function of copper strain amplitude. Fracture of the conductor was observed for loading below 75% of the composite ultimate strength, without failure of the composite. The fracture surface morphology was composed of a combination of fatigue crack growth and ductile fracture, with a higher percentage of the latter existing for greater load amplitude. Crack growth in the copper was found to be strongly coupled with debonding between the copper and composite. Prevention of debonding directly influences the fatigue life of the embedded copper strip, much in the same way as composite patches retard crack growth in repaired metal structures.     

Interfacial fatigue crack propagation in microscopic model composite using bifiber shear specimens

Interfacial fatigue crack growth behavior in GF/epoxy model composites was investigated using bifiber shear (BFS) specimens in a scanning electron microscope. The specimen is composed of two E-glass filaments with diameters of 23 and 40 μm, and bisphenol A type epoxy is impregnated between the filaments. The crack growth behavior under different stress ratios was investigated to clarify the fatigue crack growth mechanism. The change in the crack growth rate, da/dN, was not monotonic with crack length, suggesting a variation in the resistance to fatigue crack growth along a single filament. The resistance to fatigue crack growth of the interface is much smaller than that of composite laminates. The fatigue crack growth mechanism of the glass fiber/epoxy interface under different stress ratios is controlled by the maximum energy release rate, G_max, which is completely different from that of composite laminates.     

Surface and sub-surface degradation of unidirectional carbon fiber reinforced epoxy composites under dry and wet reciprocating sliding

The role of water on the sub-surface degradation of unidirectional carbon fiber reinforced epoxy composite is examined. The correlation between the debonding of carbon fibers at the fiber–epoxy interface, and the wear behavior of the carbon fiber composite are discussed based on an in-depth analysis of the worn surfaces. We demonstrate that a reciprocating sliding performed along an anti-parallel direction to the fiber orientation under dry conditions results in a large degradation by debonding and breaking of the carbon fibers compared to sliding in parallel and perpendicular directions. Immersion in water has a harmful effect on the wear resistance of the carbon fiber composite. The competition between crack growth and the wear rate of epoxy matrix and/or carbon fibers in the sliding track determines the level of material loss of the composite in both test environments.     

Evolution of damage during the fatigue of 3D woven glass-fibre reinforced composites subjected to tension–tension loading observed by time-lapse X-ray tomography

The development of fatigue damage in a glass fibre modified layer-to-layer three dimensional (3D) woven composite has been followed by time-lapse X-ray computed tomography (CT). The damage was found to be distributed regularly throughout the composite according to the repeating unit, even at large fractions of the total life. This suggests that the through-thickness constraint provides a high level of stress redistribution and damage tolerance. The different types of damage have been segmented, allowing a quantitative analysis of damage evolution as a function of the number of fatigue cycles. Transverse cracks were found to initiate within the weft after just 0.1% of life, followed soon after (by 1% of life) by longitudinal debonding cracks. The number and extent of these multiplied steadily over the fatigue life, whereas the spacing of transverse cracks along with weft/binder debonding saturated at 60% of life and damage in the resin pockets occurred only just before final failure.     

The tensile fatigue behaviour of a silica nanoparticle-modified glass fibre reinforced epoxy composite

An anhydride-cured thermosetting epoxy polymer was modified by incorporating 10 wt.% of well-dispersed silica nanoparticles. The stress-controlled tensile fatigue behaviour at a stress ratio of R = 0.1 was investigated for bulk specimens of the neat and the nanoparticle-modified epoxy. The addition of the silica nanoparticles increased the fatigue life by about three to four times. The neat and the nanoparticle-modified epoxy resins were used to fabricate glass fibre reinforced plastic (GFRP) composite laminates by resin infusion under flexible tooling (RIFT) technique. Tensile fatigue tests were performed on these composites, during which the matrix cracking and stiffness degradation was monitored. The fatigue life of the GFRP composite was increased by about three to four times due to the silica nanoparticles. Suppressed matrix cracking and reduced crack propagation rate in the nanoparticle-modified matrix were observed to contribute towards the enhanced fatigue life of the GFRP composite employing silica nanoparticle-modified epoxy matrix.     

Hybrid nanoreinforced carbon/epoxy composites for enhanced damage tolerance and fatigue life

Hybrid nano/microcomposites with a nanoparticle reinforced matrix were developed, manufactured, and tested showing significant enhancements in damage tolerance properties. A woven carbon fiber reinforced polymer composite, with the polymer (epoxy) matrix reinforced with well dispersed carbon nanotubes, was produced using dispersant-and-sonication based methods and a wet lay-up process. Various interlaminar damage tolerance properties of this composite, including static strength, fracture toughness, fatigue life, and crack growth rates were examined experimentally and compared with similarly-processed reference material produced without nanoreinforcement. Significant improvements were obtained in interlaminar shear strength (20%), fracture toughness (180%), shear fatigue life (order of magnitude), and fatigue crack growth rate (factor of 2). Observations by scanning electron microscopy of failed specimens showed significant differences in fracture surface morphology between the two materials, related to the differences in properties and providing context for understanding of the enhancement mechanisms.     

Experimental determination of the mode I delamination fracture and fatigue properties of thin 3D woven composites

The mode I delamination fracture toughness and fatigue strength of thin-section three-dimensional (3D) woven composite materials is experimentally determined. The non-crimp 3D orthogonally woven carbon–epoxy composites were thin (2 mm) and consequently their through-thickness z-binder yarns were inclined at a very steep angle (about 70°) from the orthogonal direction. The steep z-binder angle has a marked effect on the delamination toughening and fatigue strengthening mechanisms. Experimental testing revealed that the fracture toughness and fatigue resistance increased progressively with the volume content of z-binders. However, the steep angle caused the z-binder yarns bridging the delamination crack to deform and fail in shear and through-thickness tension, rather than in-plane tension which usually occurs in thick 3D woven composites. Mode I pull-off tests on a single woven z-binder yarn embedded within the composite revealed that the crack bridging traction load, strain energy absorption and failure mechanism were strongly affected by the steep angle.     

Fatigue behaviour of glass fibre reinforced epoxy composites enhanced with nanoparticles

Nanoparticle reinforcement of the matrix in laminates has been recently explored to improve mechanical properties, particularly the interlaminar strength. This study analyses the fatigue behaviour of nanoclay and multiwalled carbon nanotubes enhanced glass/epoxy laminates. The matrix used was the epoxy resin Biresin® CR120, combined with the hardener CH120-3. Multiwalled carbon nanotubes (MWCNTs) 98% and organo-montmorillonite Nanomer I30 E nanoclay were used. Composites plates were manufactured by moulding in vacuum. Fatigue tests were performed under constant amplitude, both under tension–tension and three points bending loadings. The fatigue results show that composites with small amounts of nanoparticles addition into the matrix have bending fatigue strength similar to the obtained for the neat glass fibre reinforced epoxy matrix composite. On the contrary, for higher percentages of nanoclays or carbon nanotubes addition the fatigue strength tend to decrease caused by poor nanoparticles dispersion and formation of agglomerates. Tensile fatigue strength is only marginally affected by the addition of small amount of particles. The fatigue ratio in tension–tension loading increases with the addition of nanoclays and multi-walled carbon nanotubes, suggesting that both nanoparticles can act as barriers to fatigue crack propagation.     

Assessment of the mechanical behaviour of glass fibre composites with a tough polydicyclopentadiene (PDCPD) matrix

The use of a tough thermoset polydicyclopentadiene (PDCPD) as a matrix material for composites was explored. A PDCPD–glass fibre composite and an equivalent epoxy composite were compared. Fibre–matrix adhesion quality was assessed by transverse bending tests. The materials were subjected to compression tests, impact tests, static tensile tests and tensile fatigue tests. The results indicate that the tough behaviour of the PDCPD matrix markedly influences the composite damage resistance. The size of the impact damage in the PDCPD composite was half of that in the epoxy composite. The tensile tests indicated no significant difference in tensile strength, but the damage before failure was found to be much more severe in the epoxy samples. The fatigue results showed a much lower variation in fatigue life for the PDCPD material than for the epoxy material, as well as clear differences in damage development for the two materials.     

Experimental and numerical studies in model composites Part I: Experimental results

Results on strength, apparent toughness, fatigue crack growth and fiber debonding on specially made composite materials are reported. The compact tension composite specimen used consisted of an epoxy matrix and layers of long aligned glass or kevlar fibers that were equally spaced. The experimental data on crack initiation strength showed that for a range of fiber spacing , the composite's strength _A , scaled with the fiber spacing in the form of % MathType!MTEF!2!1!+-% feaafiart1ev1aaatCvAUfeBSjuyZL2yd9gzLbvyNv2CaerbuLwBLn% hiov2DGi1BTfMBaeXatLxBI9gBaerbd9wDYLwzYbItLDharqqtubsr% 4rNCHbGeaGak0dh9WrFfpC0xh9vqqj-hEeeu0xXdbba9frFj0-OqFf% ea0dXdd9vqaq-JfrVkFHe9pgea0dXdar-Jb9hs0dXdbPYxe9vr0-vr% 0-vqpWqaaeaabaGaciaacaqabeaadaqaaqaaaOqaaiabeo8aZnaaBa% aaleaaieGacaWFbbaabeaakmaakaaabaGaeq4UdWgaleqaaOGaeyyp% a0JaeqOUdSgaaa!3EB5!\[\sigma _A \sqrt \lambda = \kappa \]. The apparent toughness of the composite specimens increased with a decrease in fiber spacing. Two sets of fatigue crack propagation experiments were performed. The first one was on specimens with the same fiber spacing and under different applied loads. The second set was on specimens with different fiber diameter and the same loading conditions. While crack arrest was observed in the first set, crack arrest was seen in the second set for the relatively large diameter fibers and specimen fracture for the relatively thin fibers. A method, based on fracture mechanics principles and crack opening displacements, for evaluating bridging tractions is outlined. Using this method, simulations for the bridging tractions and stress intensity factor were carried out using a linear crack opening profile. The total stress intensity factor was found to decrease with crack length. The debonding in the bridging zone, on specimens with different fiber spacing, was evaluated using a one dimensional debonding analysis. The model was calibrated with the debonding on the first fiber and consequently used to describe debonding on the bridging zone of specimens with different fiber spacing. In spite of the assumptions adopted in the present studies, the model seems to describe debonding well.     

Influence of load ratio on the biaxial fatigue behaviour and damage evolution in glass/epoxy tubes under tension–torsion loading

An extensive experimental campaign was carried out to understand the influence of the multiaxial stress state and load ratio on the matrix-dominated damage initiation and evolution in composite laminates under fatigue. Tubular glass/epoxy specimens were tested under combined tension–torsion loadings with different values of the load ratio and biaxiality ratio (shear to transverse stress ratio). Results are reported in terms of S–N curves for the first crack initiation and Paris-like diagrams for crack propagation, showing a strong influence of both parameters. Fracture surfaces were also analysed to identify the damage mechanisms at the microscopic scale responsible for the initiation and propagation of transverse cracks. Eventually, a crack initiation criterion presented by the authors in a previous work is applied to the experimental data showing a good agreement.     

颗粒和微观结构对Cu/WCp复合材料疲劳裂纹萌生和扩展行为的影响

通过原位扫描电子显微镜(SEM)研究了粉末冶金制备的Cu/WCp复合材料的疲劳裂纹萌生和扩展行为,分析了颗粒和微观结构对Cu/WCp复合材料疲劳裂纹萌生和早期扩展行为的影响。结果表明:疲劳微裂纹萌生于WCp颗粒和基体Cu的界面;微裂纹之间相互连接并形成主裂纹,当主裂纹和颗粒相遇时裂纹沿着颗粒界面扩展。在低应力强度因子幅ΔK区域疲劳小裂纹具有明显的"异常现象",并占据了全寿命的71%左右。疲劳小裂纹的早期扩展阶段易受局部微观结构和颗粒WCp的影响,扩展速率波动性较大,随机性较强;当小裂纹长度超过150μm时,裂纹扩展加快直至试样快速断裂。裂纹偏折、分叉和塑性尾迹降低了疲劳裂纹扩展速率,而颗粒界面脱粘则提高了复合材料的疲劳裂纹扩展速率。通过数值模拟也可以发现颗粒脱粘增大了材料的疲劳扩展驱动力,从而提高了疲劳裂纹扩展速率。     

Fractographic study of transverse cracks in a fibre composite

Transverse fracture of unidirectional fibre composites was studied in a model glass/epoxy composite in which 1 mm-diameter rods had been used in place of fibres. The fracture surface resulting from transverse cracking in this model system was studied by scanning electron microscopy (SEM). The interaction of the crack with the epoxy matrix resin and the glass rods was the following: Cracks in the resin appeared to have effected a debonding at the glassmatrix interface before reaching the glass. The debonding then propagated along the interface and induced secondary cracks ahead of the primary debonding crack. The confluence of the secondary and primary cracks resulted in sharp ridges being formed on the matrix resin surface, produced by plastic deformation of the rigid epoxy resin. These appeared as a field of parabolic marks. Considering the brittleness of the resin, the amount of plastic deformation indicated by the ridges was astonishing. As the debonding continued around the glass rod, a transverse corrugated texture developed on the resin surface, again produced by plastic deformation. Finally, the cracks reentered the matrix from small patches of polymer adhering especially strongly to the glass surface. The overall fracture energy of transverse cracking of unidirectional fibre composites is suggested to consist, therefore, of the following elements in addition to crack propagation in the matrix resin: (a) the glass-resin debonding before the incoming cracks reach the glass, (b) the initiation of secondary cracks or debonds at the interface, (c) the plastic deformation in generating the ridges on the rigid resin surface, appearing both as the paraboloids and the transverse corrugation, and (d) cracking of the matrix reinitiated at the opposite side of the glass. The use of an enlarged glass reinforcement in this study provided a more direct observation of the properties of transverse crack propagation in composite materials than would have been possible with the small, roughly 10m fibres.     

The influence of subzero temperatures on fatigue behavior of composite sandwich structures

The fatigue lives and failure modes of foam core carbon/epoxy and glass/epoxy composite sandwich beams in 4-point bending were characterized from room temperature (22 °C) down to −60 °C. Similar previous investigations had focused on elevated temperatures only, but the low temperature fatigue behavior must be understood so that these materials may be evaluated for possible use in the hull structures of ships, which operate in cold regions. Core shear was found to be the dominant fatigue failure mode for the test specimens over the entire temperature range from 22 °C down to −60 °C. Significant increases in the useful fatigue life with brittle type core shear failure were observed at low temperatures by comparison with the corresponding room temperature behavior. Fatigue failure at the low temperatures was catastrophic and without any significant early warning, but the corresponding failures at room temperature were preceded by relatively slow but steadily increasing losses of stiffness. Two different approaches were used to investigate stiffness reductions during fatigue tests, and both approaches led to the same conclusions. Experimental observations regarding the location of fatigue crack initiation were confirmed by static finite element analyses for both materials.     

Deformation micromechanics of a model cellulose/glass fibre hybrid composite

Interfacial stress transfer in a model hybrid composite has been investigated. An Sm³⁺ doped glass fibre and a high-modulus regenerated cellulose fibre were embedded in close proximity to each other in an epoxy resin matrix dumbbell-shaped model composite. This model composite was then deformed until the glass fibre fragmented. Shifts of the absolute positions of a Raman band from the cellulose fibre, located at 1095 cm⁻¹, and a luminescence band from a doped glass fibre, located at 648 nm, were recorded simultaneously. A calibration of these shifts, for both fibres deformed in air, was used to determine the point-to-point distribution of strain in the fibres around the breaks in the glass fibre. Each break that occurred in the glass fibre during fragmentation was shown to generate a local stress concentration in the cellulose fibre, which was quantified using Raman spectroscopy. Using theoretical model fits to the data it is shown that the interfacial shear stress between both fibres and the resin can be determined. A stress concentration factor (SCF) was also determined for the regenerated cellulose fibre, showing how the presence of debonding reduces this factor. This study offers a new approach for following the micromechanics of the interfaces within hybrid composite materials, in particular where plant fibres are used to replace glass fibres.     

Mode I interfacial toughening through discontinuous interleaves for damage suppression and control

An investigation is described concerning the interaction of propagating interlaminar cracks with embedded strips of interleaved materials in E-glass fibre reinforced epoxy composites. The approach deploys interlayer strips of a thermoplastic film, thermoplastic particles, chopped fibres, glass/epoxy prepreg, thermoset adhesive film and thermoset adhesive particles ahead of the crack path on mid-plane of Double Cantilever Beam (DCB) specimens. During these mode I tests, the interlayers were observed to confer an apparent increase in the toughness of the host material. The crack arrest performance of individual inclusion types are discussed and the underlying mechanisms for energy absorption and the behaviour of the crack at the interaction point of the interleave edge were analysed using scanning electron microscopy.     

Fatigue crack growth in thin notched woven glass composites under tensile loading. Part I: Experimental

Helicopter blades are made of composite materials mainly loaded in fatigue and have normally relatively thin skins. A through-the-thickness crack could appear in these skins. The aim of this study is to characterize the through-the-thickness crack propagation due to fatigue in thin woven glass fabric laminates. A technological test specimen is developed to get closer to the real loading conditions acting on these structures. An experimental campaign is undertaken which allows evaluating crack growth rates in several laminates. The crack path is linked through microscopic investigations to specify damage in woven plies. Crack initiation duration influence on experimental results is also underlined.     

Acoustic Emission-Based Methodology to Evaluate Delamination Crack Growth Under Quasi-static and Fatigue Loading Conditions

The aim of this study was to investigate the applicability of acoustic emission (AE) technique to evaluate delamination crack in glass/epoxy composite laminates under quasi-static and fatigue loading. To this aim, double cantilever beam specimens were subjected to mode I quasi-static and fatigue loading conditions and the generated AE signals were recorded during the tests. By analyzing the mechanical and AE results, an analytical correlation between the AE energy with the released strain energy and the crack growth was established. It was found that there is a 3rd degree polynomial correlation between the crack growth and the cumulative AE energy. Using this correlation the delamination crack growth was predicted under both the static and fatigue loading conditions. The predicted crack growth values was were in a good agreement with the visually recorded data during the tests. The results indicated that the proposed AE-based method has good applicability to evaluate the delamination crack growth under quasi-static and fatigue loading conditions, especially when the crack is embedded within the structure and could not be seen visually.     

Finite fracture mechanics analysis of crack onset at a stress concentration in a UD glass/epoxy composite in off-axis tension

The presence of stress concentrations at holes and notches is known to reduce the strength of composite materials. Due to complexity of the damage processes at a stress raiser in a composite, different modeling approaches have been developed, ranging from empirical point and average stress criteria to involved damage mechanics or cohesive zone-based models of failure. Finite fracture mechanics approach with a coupled stress and energy failure criterion, recently developed and applied mainly to cracking in homogeneous isotropic materials, allows predicting the appearance and propagation of a crack using material strength and toughness characteristics obtained from independent tests. The present study concerns application of the finite fracture mechanics to the analysis of cracking at a notch in a UD glass/epoxy composite subjected to tensile off-axis loading. Based on UD composite strength and intralaminar toughness characterized by separate tests, finite fracture mechanics analysis provided conservative estimates of crack onset stress at the notch.     

Experimental investigations on fatigue crack growth of repaired thick aluminium panels in mixed-mode conditions

In this paper, experimental fatigue crack growth of thick aluminium panels containing a central inclined crack of 45° repaired with single-side glass/epoxy composite patch are performed. It is shown that, the technique of single-side repair using glass/epoxy composite patch is effective in the crack growth life extension of the thick panels in mixed-mode conditions. It is also shown that the crack-front of the propagated cracks of the repaired panels has a curvilinear shape which is the effect of the existed out-of-plane bending due to the asymmetry conditions in the single-side repaired panels. It is indicated that the crack propagation path at patched surface is different from the un-patched surface of the panels. In the primary stages of the crack growth, the crack surfaces through the thickness, in the vicinity of the mid-plane propagate without surface twisting. There are considerable differences between the obtained crack growth path at patched and un-patched surfaces of the panels which mean that the crack propagation surfaces have three-dimensional patterns. Using the various thin patch lay-ups has minor effects on the crack re-initiation life of the repaired thick panels. It is shown that using various four layers patch lay-up configurations, the crack propagation life of the cracked panels may increase by the order of 30–85%. The most fatigue crack growth life extension belongs to the repaired panel with the patch lay-up of [90]₄.