Effect of Cold-rolling on Hardness of SiCw／Al Composite

A SiCw|A| compostie was fabricated through a squeeze cast route and cold rolled to about 30%,50% and 70% reduction in thickness.respectively.The length of whiskers in the composite before and after rolling was examined using SEM.Some of the rolled composites were annealed by recrystallizing to remove the work hardening of the matrix alloy.The hardness of the rolled and annealed SiC A SiCw|A| composites was examined and then associated with the change of the whisker length and the work hardening of the matrix alloy.It was found that the hardness was a function of the degree of cold rolling .For the cold rolled composites .with the increase in the degree of cold rolling .the hardness increases at first,and decreases when the degree of cold rolling excecds 50%.For the annealed ones .however,the hardness monotonously with the increase in rolling degree.The different changes in hardness beticeen the rolled and annealed composites coukl be attributed to a result of the competition benceen the work hardening of the matrix resulting from the cold rolling and the work softening arising from the change of whisker length.     

氮对Ti-6Al合金的铸态组织与性能的影响

采用熔铸工艺制备了w(N)=0.045~0.27%的原位自生氮化物增强钛铝基复合材料.分析测试了该材料的铸态组织和合金的力学性能.研究结果表明:在Ti-6A l的合金中,当w(N)=0.045~0.27%时,随着氮质量分数的增加,增强体的体积分数有所增加.Ti-6A l-xN中的氮化物较为细小.复合材料的硬度、抗压强度和弹性模量均高于Ti-6A l合金.随着氮质量分数增加材料的抗压强度、硬度和弹性模量增加.由压缩断口分析可知,基体为韧性断裂.随着氮质量分数增加,合金由韧窝 解理断口向具有解理特征的脆性断裂转变.     

Effects of Matrix on Tensile Strength of SiCw/Al Composites

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The hot compressive deformation behavior of the metal matrix composites with the large whisker orientation

Metal matrix composites are often subjected to ahot compressive plastic forming.During the thermome-chanical process the reinforcements are misaligned fromthe loading axis and rotate toward a more stable posi-tion.Meanwhile,the strain softening can be observedduring the hot compression of the metal matrix compos-ites reinforced with discontinuous reinforcements suchas the randomly oriented whiskers[1-3],the whiskersparallel to the applied loading[4-5]and the whiskerstilted away from the applie…     

氧化SiCp增强ZL101铝基复合材料的显微结构

利用光学和电子显微镜研究了液态金属搅拌法处理后金属型铸造和连续铸造ＳｉＣｐ／ＺＬ１０１ 铝基复合材料的显微组织与界面结构特征．结果表明,ＳｉＣｐ 高温氧化后表面生成的ＳｉＯ２ 晶体在复合材料复合与铸造期间与铝合金熔液中的Ｍｇ 、Ａｌ 元素发生界面反应,生成ＭｇＡｌ２ Ｏ４ 和Ｓｉ,促使ＳｉＣｐ 与铝合金润湿,并提高ＳｉＣｐ 的分散性．与普通金属型铸造相比,连续铸造ＳｉＣｐ／ＺＬ１０１ 复合材料的晶粒细小,ＳｉＣｐ 分布十分均匀,ＳｉＣｐ／Ａｌ 界面反应层较薄．     

Effect of homogenization treatment on microstrucmre and properties of Al-Mg-Mn-Sc-Zr alloy

The effect of homogenization on the hardness, tensile properties, electrical conductivity and microstructure of as-cast Al-6Mg-0.4Mn-0.25Sc-0.12Zr alloy was studied. The results show that during homogenization as-cast studied alloy has obviously hardening effect that is similar to aging hardening behavior in traditional Al alloys. The precipitates are mainly Al3（Sc,Zr） and Al6Mn When homogenization temperature increases the hardness peak value is declined and the time corresponding to hardness peak value is shortened. The electrical conductivity of the alloy monotonously increases with increasing homogenization temperature and time. The decomposition of the supersaturated solid solution containing Sc and Zr which is formed during direct chilling casting and the precipitation of Al3（Sc, Zr） cause hardness increasing. The depletion of the matrix solid solubility decreases the ability of electron scattering in the alloy, resulting in the electrical conductivity increased. Tensile property result at hot rolling state shows that the optimal homogenization treatment processing is holding at 300-350℃ for 6-8 h.     

界面性能对晶须增强树脂基复合材料力学行为的影响

用碳化硅晶须、光敏树脂合成了光固化用树脂基复合材料,并对材料进行了拉伸测试,测试结果表明复合材料的实测拉伸强度与理论值相差较大;在实验的基础上进一步建立了复合材料的界面相模型,采用有限元方法分析了界面性能对晶须增强树脂基复合材料力学行为的影响.结果表明:界面性能对晶须承受轴向应力的影响远大于对树脂基体的影响,晶须界面剪切应力与界面结合强度成正比,晶须端面应力集中系数随界面结合性能的增强而递增.     

基于单颗磨粒划切试验的SiCp/Al复合材料表面去除机理研究

碳化硅颗粒增强铝基（SiCp/Al）复合材料中含有不规则碳化硅颗粒使得材料内部形成大量非理想截面,为材料表面的有效去除带来困难. 为了揭示材料去除机理,进行SiCp/Al 复合材料单颗磨粒变切深划切的表面去除仿真分析和试验验证. 研究结果表明,界面破坏对表面创成有重要影响,存在铝合金基体撕裂、界面分离,碳化硅颗粒裸露、裂纹扩展、破碎脱落、压入铝合金基体、碎片滑擦材料表面等去除过程,碳化硅颗粒中部大面积破碎脱落形成凹坑,并在刀具推挤作用下对材料进行二次切削,使铝合金基体表面形成非连续裂纹. SiCp/Al复合材料中由于铝合金基体的存在,实际划切深度小于名义切削深度. 研究可以为SiCp/Al复合材料去除机理与加工研究提供一定借鉴.     

(TiB_2+SiC_p)/ZL101复合材料组份优化及其力学性能

为了确定(TiB2+SiCp)/ZL101复合材料的最佳成分,通过采用正交实验分析方法,研究复合材料的制备工艺,测试了复合材料的力学性能,并对该材料进行了显微金相分析和透射电子显微分析.结果表明,复合材料经过热处理后,抗拉强度、布氏硬度分别较基体合金ZL101提高了21.4%、49.3%;热膨胀系数较基体合金降低了14.1%;热处理后,复合材料中的共晶硅以粒状形态均匀分布于基体中;复合材料中增强相TiB2为粒状,SiC粒子为多边形尖角块状,两相较均匀分布于基体晶粒内部,且与-αAl的界面结合良好.     

Reactive processing and mechanical properties of Al/SiCP composite

The reactive process for Al/SiC_P composite was studied. SiC particles were in-situ coated by the exothermal reaction of SiC-Ti powder compact in Al melt bath, and easily incorporated into Al melt. The detailed study was carried out to understand the microstructures of the reacted SiC particles. During the reaction and consequent mixing, the successive processes include in-situ coating on the reacted SiC particles, coat dissolution and SiC_P splitting. The tensile mechanical properties of 6013Al/SiC_P composite processed by the present technology showed that the reacted SiC_P considerably reinforced the 6013 matrix. Foundation item: The Key Program of the 9th Five-year Plan of China(No. 95-YS-005) Biography of the first author: CHEN Kang-hua, professor, born on Aug. 30, 1962, received Ph. D degree in 1991, majoring in Al alloy, Al matrix composite and powder metallurgy.     

轧制对Zr（60）Al（15）Ni（25）块体非晶合金晶化动力学的影响

通过线性DSC实验研究了轧制对Zr60Al15Ni25大块非晶合金晶化动力学的影响。实验结果表明,Zr60Al15Ni25非晶合金在轧制塑性变形过程中,随着变形量的增加,热稳定性降低。Zr60Al15Ni25块体非晶合金轧制后原子组态的变化主要影响晶化的形核阶段,变形量较低时（20%）合金原子组态向无序方向发展,导致晶化速率变慢,晶化变得比较困难。随着轧制的进一步增加,合金原子的无序性降低,晶化速率又逐渐提高,从而使其在随后加热过程中的晶化变得比较容易。     

硼酸铝晶须增强铝复合材料的电化学腐蚀行为

通过对不同扫描速率下电化学极化曲线的测试,研究了3种晶须体积分数的硼酸铝晶须增强纯铝基复合材料在3.5%NaCl溶液中的电化学腐蚀行为,并利用扫描电子显微镜观察了经极化处理后,复合材料表面的微观组织形貌.研究结果表明,随晶须体积分数的增加,复合材料阳极钝化区域逐渐减小,且相应复合材料表面被腐蚀程度也显著增加,即随体积分数的增加,复合材料发生腐蚀的敏感性逐渐增加.对同种晶须体积分数的复合材料而言,随扫描速率的提高,复合材料阳极极化曲线中钝化区域明显增大,从而表明在较高的腐蚀速率下,复合材料更易于钝化.     

Nb微合金化冷轧双相钢DP980的试制研究

采用C-Si-Mn-Cr-Nb合金系,采取两种热轧、退火工艺,在实验室试制Nb微合金化冷轧双相钢DP980。结果表明,两种试制钢的抗拉强度分别为1034 MPa和1048 MPa,屈服强度分别为534 MPa和499 MPa,伸长率分别为11.2%和11.3%,n值分别为0.28和0.27,屈强比分别为0.52和0.48;试制钢的热轧组织为F＋P,连续退火后的组织为F＋M,退火后的应力应变曲线表现出连续屈服的特点。     

颗粒增强复合材料的动态压缩力学性能研究

首先采用Instron2300材料试验机和Hopk inson压杆冲击试验测试了10%(vo l)S iC/A l陶瓷颗粒增强金属基复合材料在不同应变率范围的应力应变曲线.结果表明,该复合材料存在明显的应变率强化效应,随应变率的增加,其流动应力也迅速增加.在不相同的应变率下,随应变的增加,复合材料的流动应力与准静态流动应力的比值趋于一常数,表明复合材料在不同的应变率下具有相同的应变硬化规律.最后用R am berg-O sgood材料模型结合应变率强化模型拟合了复合材料的动态应力应变曲线,得到了与实验结果相吻合的结果.     

铸造颗粒增强铝基复合材料的研究

利用机械搅拌方法,制备了SiC/ZL101;Al2O3/ZL101;SiC,Al2O3/ZL101复合材料,研究了SiC/ZL101,Al2O3/ZL101复合材料组织.结果表明,制备工艺对SiC/ZL101,SiC-Al2O3/ZL101组织及硬度有重要的影响.该研究为颗粒增强铝基复合材料的制备提供了理论与实验基础.     

一种新型冷轧变形钢筋的力学性能试验分析

对一种新型冷轧变形钢筋进行金相分析和力学性能试验。结果与热轧圆盘母材和I型冷轧扭钢筋作了比较，表明其抗拉强度，表面强度比热轧圆盘母材提高了20％以上，而伸长率δ5大于9．05％，与I型冷轧扭钢筋相比，其塑性性能获得提高。     

SiCp／Al复合材料的压铸法制造工艺的研究

采用先制预制块然后加压铸造的方法制得了致密均匀的ＳｉＣｐ／Ａｌ复全材料，与基体铝合金相比，其屈服强度提高４６％，抗拉强度提高２４％，弹性模量提高８７％。     

包覆法制备Gp/SiC复合材料的显微结构和性能

以不同粒径的石墨颗粒和SiC粉体为原料,采用SiC粉体包覆石墨颗粒的方法,于2000℃热压制备了石墨/碳化硅（Gp/SiC）复合材料.利用扫描电子显微镜（SEM,EDS）分析了材料的金相和断口显微结构.研究表明,石墨粒径较小且质量分数较少的复合材料比石墨粒径较大且质量分数较多的复合材料在热压工艺中更致密.石墨颗粒呈岛状紧密地镶嵌在SiC基体中,石墨与SiC界面处C和Si的扩散不明显.复合材料的相对密度、抗折强度,断裂韧性和硬度随石墨粒径和质量分数的减少而增加.断口形貌表明SiC陶瓷基体为脆性,石墨为韧性断裂.当石墨粒径为125μm、SiC与石墨的质量比为3.5时,复合材料的综合性能最佳,开口气孔率为0.3%,相对密度为97.9%,抗折强度为75±15 MPa,断裂韧性为5.4±0.5 MPa.m1/2,硬度为26.8±3GPa.     

IF钢生产过程中的织构演变

对IF钢生产过程中热轧、冷轧及退火试样的织构演变进行研究。分别借助EBSD和XRD测定和计算了热轧、退火及冷轧试样的取向分布函数及相关织构组分的体积分数。结果发现,热轧板在变形过程中发生了动态再结晶,晶粒为细小的等轴晶,为后续组织发展提供了基础;热轧后试样中的织构很弱,不会影响冷轧织构组分及含量。冷轧过程是织构形成的主要过程,试样中含有4种主要的织构组分：{001}〈110〉、{111}〈110〉、{111}〈112〉和{112}〈110〉。退火过程中发生再结晶,4种冷轧织构组分在退火过程中均分别转变为{111}面织构。     

Effect of pressure on the solidification behavior and mechanical properties of SiCp/Al-Mg composites

SiCp/Al-Mg metal matrix composites were manufactured by semi-solid stirring technique. The composites were remelted and then solidified under different pressures to study the solidification behavior of composites by differential thermal analysis, scanning electron microscopy, and transmission electron microscopy. The experimental results show that SiCp reinforcements can not act as heterogeneous nucleation sites for α(Al), and an interfacial layer composed of MgAl2O4 spinel and Si-rich phase existed at Al/SiCp interface. The undercooling of the matrix alloy was improved by the pressure applied, resulting in the grain of matrix alloy refining. The X-ray diffraction pattern of composites testified that the matrix alloy exhibited a certain preferred orientation during solidification. In addition, with increasing the pressure for solidification, the pored defects in the composites decreased, while the relative density, hardness and compressive strength increased. Therefore, the microstructure and mechanical properties of the composites were improved by pressure placed during the solidification of SiCp/Al-Mg composites.