共查询到18条相似文献,搜索用时 218 毫秒
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印楝素的快速提取法研究 总被引:4,自引:0,他引:4
采用微波辐射、超声波强化和快速搅拌三种辅助方法从印楝种仁粉中提取印楝油和印楝素。研究结果表明,快速搅拌法印楝油、二氯甲烷粗提物、印楝素A和印楝素B的提取率均高于微波辐射法和超声波强化法,具有明显的提取优势。 相似文献
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印楝素(azadirachtin)是第一个从印楝Azadirachtaindica种子中分离出来的、目前世界公认的活性最强的植物源昆虫拒食剂,对害虫具有显著的拒食和生长发育抑制作用,印楝素主要存在于印楝种子中,印楝种子中含印楝素可达0.1%~0.9%(w),为了从印楝种子中充分提取印楝素,本文建立了用超临界流体从印楝种子中萃取印楝素的方法,用正交试验优化设计选择萃取条件,最佳萃取条件为:温度35℃,压力30MPa,夹带剂用量每克印楝种子干粉1.5mL甲醇,提取率明显优于溶剂法。 相似文献
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正交实验优化长春碱微波辅助提取工艺 总被引:2,自引:0,他引:2
采用微波辅助提取法提取长春花中的长春碱,通过微波提取时间、乙醇体积分数、微波功率、固液质量体积比(g/mL)、浸泡时间5个因素对长春碱提取率的影响进行了正交实验,确定微波提取最佳工艺条件为A2B1C1D4E3,即提取时间2 m in、体积分数为80%的乙醇、微波功率为低火、固液质量体积比1∶20(g/mL)、浸泡时间为1 h。微波提取长春花叶片中长春碱的提取率为0.011 427%,是回流提取的1.24倍,是超声提取的1.16倍。结果表明:微波提取长春花中长春碱具有提取时间短、速度快、提取率高等特点。 相似文献
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Organic solvents of diethyl ether and pentane were tested against ethanol for the extraction of terpenoids and cannabinoids from hemp inflorescence. It is not well known how pretreatment of grinding and extraction conditions, that is, number of extractions, temperature, and solvent residence time affect extraction yield and product compositional profiles, so these were examined in this study. As a general trend, diethyl ether and pentane had better selectivity towards the terpenoids and cannabinoids compared to ethanol. It was found that even though grinding to reduce the particle size of the inflorescence did not dramatically increase the total extraction yield, it increased the yield of the first extraction as well as the content of terpenoids and cannabinoids in the extract. Extraction residence time trial revealed the benefit of shorter time and the different behavior of the two classes of compounds. Increasing the extraction temperature from 4 to 21°C improved the total extraction yield by all three solvents, however, no additional improvement was seen at 30°C. To achieve high concentration of the bioactive compounds in the extract, multiple extraction at 21°C with short residence time, such as 15 min, are preferred for the solvents tested, and an extract having about 6% terpenoids and 59% main cannabinoids was obtained using pentane. This systematic study provides a guide to commercial processing optimization and directions for further investigation. 相似文献
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提取条件对苦参中总生物碱提取率的影响 总被引:2,自引:0,他引:2
为了选出苦参中生物碱的最佳提取条件,本研究通过对比不同提取溶剂、不同提取方法对苦参中总生物碱出膏率、总生物碱含量的影响,并用酸性染料比色法测定药膏中总生物碱的含量。结果表明,氨水-氯仿提取,出膏率最高、总生物碱含量最高;超声提取高效、省时、省能源,是比较好的提取方法。 相似文献
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The effect of juice extraction conditions on the quality of haskap berries (Lonicera caerulea L.) dried at different temperatures (60, 100, and 140°C) was investigated. The conventional juice extraction (process A) consisted of a two-press process, where thawed berries were pressed, and osmotic treatment was applied before pressing again. This was compared with a modified extraction (process B), which applied osmotic treatment during fruit thawing and only one press was used for extraction. The quality parameters investigated included moisture content, pressed berry yield, extraction loss, drying yield, total anthocyanin content (TAC), vitamin C content, and the rehydration characteristics of the final dried berries. Pressing the berries to 70% juice yield resulted in a higher pressed berry yield and better physicochemical quality in the pressed product. The yield was 26.39 and 28.92% in the conventional and modified extraction, with moisture contents of 70.32 and 77.75%, respectively. The TACs of pressed berries from extraction processes A and B were 24.62 and 33.03?mg C-3-G g?1 DW and the vitamin C contents were 14.14 and 36.18?mg/100?g, respectively. Drying at 60°C until 25% moisture content was better than at higher temperatures, resulting in a better quality dried product. It revealed drying yields of 45.32 and 52.75%, TACs of 4.00 and 4.30?mg C-3-G g?1 DW, vitamin C contents of 2.97 and 4.91?mg /100?g, and rehydration ratios of 2.22 and 2.37 from processes A and B, respectively. Process B with the one-step extraction is recommended for higher pressed berry yield, higher drying yield, and enhanced quality of the pressed and dried products. It is also a more efficient process, in terms of time, cost, and energy. 相似文献
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《Food and Bioproducts Processing》2014,92(4):393-401
An increasing demand for natural flavonoids necessitates the development of new technologies to improve the extraction of phytochemicals whilst retaining their bioactivity. Extracts from rooibos (Aspalathus linearis), well known as an herbal tea and food and beverage supplement, have shown significant potential for the treatment of various lifestyle conditions, but poor extraction of soluble matter limits its potential value and put limited supplies under pressure. This study demonstrates that pre-treatment with food-grade cellulase, ferulic acid esterase and/or pectinase increased the soluble solid yield from green and fermented rooibos when preparing an infusion, whereas ferulic acid esterase and β-glucanase/β-xylanase increased the total polyphenol yield. A combination of β-glucanase/β-xylanase and pectinase increased the yield of soluble solids from fermented rooibos in industrial evaluations by 33%. Although the total polyphenol and antioxidant content was reduced due to the extraction of ‘inactive’ sugar moieties, the extract exceeded industry benchmarks for both quality parameters. Furthermore, a clear extract was produced with no detrimental impact on its sensory attributes. Although the enzyme treatment reduced the aspalathin content of the extract, there was a concomitant increase in its flavone counterpart, isoorientin, which has significant pharmaceutical value for the treatment of both types of diabetes mellitus. 相似文献
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广西灵香草提取物的化学成分研究及香气评价 总被引:3,自引:0,他引:3
目的 :研究广西金秀灵香草提取物的化学成分及香气。方法 :采用超临界CO2 萃取法和溶剂法提取的广西灵香草提取物 ,用气相色谱 /质谱进行分离测定 ,结合计算机检索技术对分离的化合物进行结构鉴定 ,应用色谱峰归一化法确定各成分的相对含量。结果 :超临界CO2 萃取灵香草提取物得率 1.5 % ,鉴定出 2 7个化学成分 ,溶剂法得率 1.2 % ,鉴定出 2 0个化学成分 ;经评定 ,超临界CO2 萃取法得到的提取物气味更接近灵香草天然香气。结论 :用超临界CO2 萃取法可以生产出最接近自然香气的天然香料 相似文献
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《分离科学与技术》2012,47(12):1851-1858
Experiments were performed to evaluate an extraction process developed in our laboratory called the instantaneous controlled pressure drop process (“Détente Instantanée Contrôlée” or (DIC)) for extracting volatile compounds from oak wood. This process involves subjecting oak chips for a short time (10 s to 12 min) under a steam pressure (1 to 6 bars or from 100 to 165°C). This first step is followed by a rapid decompression toward vacuum (up to 50 mbar). Some parameters were evaluated: steam pressure level, processing time, initial moisture content, chips thickness and velocity of the rapid decompression. A preliminary experimental design allowed optimizing the processing pressure and processing time: 6 bar and 5 minutes. Under these conditions, the optimal conditions were as follows: 20% for initial moisture content, 0.5 mm for the chips thickness. The number of decompressions towards vacuum was also investigated and it appeared that extraction yield can be enhanced by repeating the decompressions cycles for a same processing time. Moreover, GC-MS analysis indicated that DIC extract included the same molecules that obtained by steam distillation with almost the same percentages. 相似文献