镁合金AZ31B搅拌摩擦焊研究

研究了镁合金AZ31B搅拌摩擦焊接工艺参数（搅拌头转速n、焊接速度v、焊接压力P）及搅拌头材料和形状对焊接头的影响。结果表明，采用高速钢制圆台带凹面形的搅拌头效果较好；其合适的工艺参数范围是n=950～1500r／min，v=37．5～60mm／min,P=3kN；最优工艺参数为：n；1500r／min，v=47．5mm／min，P=3kN。     

镁合金AZ31B搅拌摩擦焊研究

研究了镁合金AZ31B搅拌摩擦焊接工艺参数(搅拌头转速n、焊接速度v、焊接压力P)及搅拌头材料和形状对焊接头的影响。结果表明,采用高速钢制圆台带凹面形的搅拌头效果较好;其合适的工艺参数范围是n=950～1500r/min,v=37.5～60mm/min,P=3kN;最优工艺参数为:n=1500r/min,v=47.5mm/min,P=3kN。     

MB3镁合金固态塑性连接组织性能研究

研究了MB3镁合金的搅拌摩擦焊技术。对其塑性连接时的焊缝成形，焊缝组织形态及接头的力学性能进行了分析。结果表明，用搅拌摩擦焊方法焊接MB3镁合金，当工艺参数合适时，可获得外观成形美观、内部无缺陷，几乎无变形的平板对接接头。接头力学性能试验表明，其抗拉强度可达母材的97．2％，高于熔焊接头的强度，断裂位置大多位于热影响区。     

AZ91镁合金的半固态搅拌摩擦焊接连接形成机理

半固态连接被认为是一种连接合金的可能的方法。研究了AZ91镁合金半固态搅拌摩擦焊接的机理。将2块7.5 mm厚的AZ91镁合金试件和1块2 mm厚的 Mg?25%Zn中间层放在加热板上,加热到所需温度并保温3 min后,采用旋转搅拌头搅拌焊缝。将加热板在台车上以4.6 cm/min的恒定速度运动。同时,对一个样品进行无中间层焊接。使用扫描电子显微镜和光学显微镜研究焊接过程中搅拌速度、搅拌头形状和温度的影响。结果表明,中间层降低了焊接温度;升高温度、加快搅拌速度、采用圆形搅拌头代替槽形搅拌头都能增大搅拌区的宽度。在焊接过程中,可能存在某些机理,从而有助于获得良好的的冶金结合,例如氧化层消失、液相混合、液球连接、液体渗入基体、从大量液球基体金属进入焊缝区。     

基于钻铣床的搅拌摩擦焊设备设计

以ZX50CA钻铣床为研究对象,采用液压技术对其压下装置进行设计,设计出一台适用于镁合金薄板搅拌摩擦焊的设备,选用3 mm厚的AZ31镁合金板材进行对接焊接实验。结果表明:当搅拌头转速为1400 r/min、焊接速度为15 mm/min、压紧力为1500 N时,焊接接头表面成形良好。通过实验证明,该设备能够满足搅拌摩擦焊的工艺参数要求,适用于搅拌摩擦焊的实验研究,而且相对于大型专用搅拌摩擦焊设备,成本低,使用灵活、方便,为镁合金薄板搅拌摩擦焊设备的开发提供了很好的参考价值。     

镁合金搅拌摩擦焊接技术

对5mm厚镁合金AZ31B板材的摩擦焊接技术进行了试验研究，结果表明：适合其板材的搅拌摩擦焊接的搅拌头，材料为W6MoSCr4V2高速钢，结构为凹面圆台形，根部直径5．5mm，端部直径为2．5mm，轴肩尺寸为12mm，长度为4．7mm。镁合金搅拌摩擦焊接头的抗拉强度可达母材的90％，延伸率可达母材的50％。搅拌摩擦焊接头焊合区为动态再结晶组织，在接头前进边焊合区与母材有明显的分界线，返回边过渡区有金属微熔的迹象。     

搅拌头形貌对AZ31镁合金板材FSW接头力学性能的影响

采用不同形貌的搅拌头对6.2 mm厚AZ31镁合金板材进行搅拌摩擦焊接试验,研究了搅拌头形貌对接头力学性能的影响。结果表明,旋转速度为1500 r/min,焊接速度为80 mm/min时,使用T1双圆环搅拌头得到的接头力学性能最好,焊缝在材料厚度方向上的尺寸变化呈均匀过渡趋势,焊缝表面比较美观。接头的硬度基本上与母材相当,只有热影响区硬度略有下降。     

AZ91D薄板搅拌摩擦焊

实现了厚度为2.2 mm铸造镁合金AZ91D薄板的搅拌摩擦焊和钨极氩弧焊,分析了搅拌摩擦焊工艺参数对焊接接头成形的影响和接头组织变化,考察了搅拌摩擦焊接头的力学性能.在搅拌头旋转速度为1 380 r/min时得到了比较理想的焊接接头,而1 960 r/min的转速过大.接头不同区域所受的机械力和热量不同,显微组织明显不同.搅拌区晶粒细小,显微硬度和强度都有所提高.搅拌摩擦焊接头力学性能与热输入有关;与氩弧焊接头相比,搅拌摩擦焊接接头的性能更好.     

工艺参数对铝镁搅拌摩擦焊焊缝成形质量的影响

工艺参数对铝镁异种材料搅拌摩擦焊接头质量有着重要影响,研究了焊接速度,搅拌头旋转频率,材料放置位置,搅拌头正反转及偏移等工艺参数对7075铝合金与AZ31B热挤压态镁合金异种材料搅拌摩擦焊对接接头成形质量的影响.结果表明,在搅拌针旋转频率为13 r/s,焊接速度为30 mm/min下可获得较好的焊缝成形质量;另外,要获...     

搅拌头转速对AZ31镁合金厚板搅拌摩擦焊接头力学性能的影响

选用9.8 mm厚AZ31镁合金进行搅拌摩擦焊对接试验,探究搅拌头转速对焊接接头力学性能和表面成型的影响。结果表明,接头的力学性能随搅拌头转速的增加呈先增大后减小的趋势。过低的搅拌头转速会造成热输入不足,产生隧道缺陷,降低接头力学性能;搅拌头转速过高会造成热输入过大,也会降低接头的力学性能。当选择转速800r/min,焊接速度180 mm/min时,接头力学性能最好,拉伸断口呈韧性断裂,无缺陷。     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

THERMODYNAMICS STUDY ON THE DECOMPOSITION OF CHROMITE WITH KOH

Institute of Process Engineering, Chinese Academy of Sciences, China, has proposed a method for oxidative leaching of chromite with potassium hydroxide. Understanding the mechanism of chromite decomposition, especially in the potassium hydroxide fusion, is important for the optimization of the operating parameters of the oxidative leaching process. A traditional thermodynamic method is proposed and the thermal decomposition and the reaction decomposition during the oxidative leaching of chromite with KOH and oxygen is discussed, which suggests that chromite is mainly destroyed by reactions with KOH and oxygen. Meanwhile, equilibrium of the main reactions of the above process was calculated at different temperatures and oxygen partial pressures. The stable zones of productions, namely, K2CrO4 and Fe2O3, increase with the decrease of temperature, which indicates that higher temperature is not beneficial to thermodynamic reactions. In addition, a comparison of the general alkali methods is carried out, and it is concluded that the KOH leaching process is thermodynamically superior to the conventional chromate production process.     

INFLUENCE OF HEAT TREATMENT ON DAMPING BEHAVIOUR OF THE MAGNESIUM WROUGHT ALLOY AZ61

The effect of isochronal heat treatments for 1h on variation of damping, hardness and microstructural change of the magnesium wrought alloy AZ61 was investigated. Damping and hardness behaviour could be attributed to the evolution of precipitation process. The influence of precipitation on damping behaviour was explained in the framework of the dislocation string model of Granato and Lücke.     

Theoretical Analysis for the Motion and Temperature of Melt Droplets in Spray Degassing Process

The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results.     

Growth Kinetics of Single Inclusion Particle in Molten Melts

On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes＇ collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process.     

An Easy Way to Quantify the Adhesion Energy of Nanostructured Cu/X(X=Cr,Ta,Mo,Nb,Zr) Multilayer Films Adherent to Polyimide Substrates

An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models.     

High-Speed Friction Stir Welding of SiC_p/Al–Mg–Si–Cu Composite

A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

A STUDY OF TEMPERATURE-DEPENDENT VALENCE BOND STRUCTURE OF TITANIUM

On the basis of energy and shape method for the determination of the valence bond (VB) structures of crystal, the valence bond structure of titanium is redetermined at room temperature and calculated in the whole temperature range of 0-1943K. The outer shell electronic distribution of Ti is e_c~(2.9907) · (s_c~(0.4980) d_c~(2.4927)) ef1.0093 in crystal. The temperature dependences of the VB structures of hcp and bcc phases are the same. The VB structures of hcp and bcc phases monotonically increase or decrease with the increase in temperature, but show discontinuous changes at the phase-transformation temperature 1155K.