硼微合金化SS400B热轧板卷卷取工艺优化

针对通化钢铁股份有限公司试制的SS400B厚规格热轧板卷强度偏高、伸长率较低的问题,分析了卷取温度、冷却模式对板卷性能的影响。结果表明,卷取温度对SS400B热轧板卷力学性能影响明显,随卷取温度的提高,板卷晶粒尺寸增大,屈服强度、抗拉强度显著降低;层流冷却模式能够改善板卷组织性能,延长冷却时间、适当降低冷却速率可以一定程度降低其强度并提高其塑性;在目前成分设计下,采用650～670℃卷取温度和均匀冷却工艺可以保证SS400B板卷获得最佳性能,其屈服强度为340MPa,抗拉强度为500MPa,伸长率为23%。     

卷取温度对Q960热轧薄钢板组织与性能的影响

研究了中低温卷取温度对Q960热轧薄板钢显微组织和力学性能的影响。结果表明,随着卷取温度从562℃降至359℃,Q960热轧板的显微组织由粒状贝氏体+少量的珠光体转变为下贝氏体;渗碳体含量明显增加而MC相略有下降。低温或超低温卷取可以减轻或消除Q960热轧板的带状组织。采用非再结晶轧制和约350℃低温卷取可以使Q960热轧卷板获得1000 MPa以上的非比例延伸强度,同时冲击性能良好。     

成分和卷取温度对热轧铌微合金钢组织和性能的影响

研究了化学成分,特别是铌含量的增加对铌微含金钢热轧板组织性能的影响;分析了不同的卷取温度对相同铌含量的热轧板组织性能的影响,同时分析比较了卷取温度对低碳钢组织性能的影响.结果表明.铌含量由0.017%增加到0.03%,沉淀强化作用相对于晶粒细化作用更为显著;550℃、600℃、650℃的卷取温度对铌含量0.017%的热轧板组织性能影响不大,同样750℃、550℃卷取温度对成分相近的低碳钢组织性能影响也不大,这对热轧板生产具有一定参考意义.     

C-Si-Mn-Cr双相钢组织与性能的柔性控制技术

以C-Si-Mn-Cr成分体系双相钢为研究对象,采用金相显微镜、扫描电镜、拉伸试验等方法,对终轧温度、卷取温度、退火温度等工艺参数对C-Si-Mn-Cr系双相钢组织和性能的影响进行了研究。结果表明,降低终轧和卷取温度,热轧板组织由铁素体+珠光体转变为铁素体+珠光体+贝氏体,同时热轧板的屈服强度和抗拉强度都有所提高;当冷轧和退火工艺相同时,对采用低温终轧和低温卷取生产的双相钢来说,其抗拉强度由472 MPa增加到524 MPa,而屈服强度则变化不大,此时伸长率和n值略有降低;通过采用低温卷取+中温退火工艺,可以实现一种成分体系生产CR260/450DP和CR290/490DP两种强度级别双相钢的柔性化生产目标。     

卷取温度对540 MPa级热轧酸洗板组织性能的影响

对不同卷取温度下540MPa级热轧酸洗板的组织性能进行了研究。结果表明,卷取温度为380℃时,540 MPa级热轧酸洗板组织为铁素体+粒状贝氏体,R_(eL)≥440MPa、R_m≥550MPa,A≥28%,扩孔率达100%;当卷取温度为290℃时,钢板组织中出现了马氏体,其屈服强度和抗拉强度明显提升,扩孔性能和伸长率下降;当卷取温度降至220℃时,钢板组织中出现了大量马氏体。因此,为获得理想的强度、塑性及扩孔性能,卷取温度不宜过低。     

卷取温度对1000MPa级低碳贝氏体高强钢的影响

设计了一种低碳抗拉强度为1000 MPa级的工程结构钢,通过使用扫描电子显微镜(SEM)和拉伸试验机等仪器研究了卷取温度对低碳合金钢的组织性能影响。结果表明:终卷取温度对实验钢组织和性能有较大影响,卷取等温温度较高时实验钢的组织以粒状贝氏体为主,卷取等温温度较低时以板条贝氏体为主。随着等温温度的上升,抗拉强度和屈服强度均呈先上升后下降的趋势,卷取温度控制在350℃时,获得最佳的力学性能,屈服强度和抗拉强度分别达到1026 MPa和1118 MPa,伸长率为12.1%。     

卷取温度对低合金高强度钢组织与性能的影响

研究卷取温度对低合金高强度钢组织与性能的影响。结果表明,钢的屈服强度、硬度和抗拉强度随卷取温度的升高而降低,伸长率随卷取温度的升高而有所增加。当卷取温度为580℃时,钢的组织为铁素体+粒状贝氏体,屈服强度为731.52 MPa,抗拉强度为840.67 MPa,显微硬度为231.6 HV,伸长率为20.2%,强韧匹配性较佳。     

卷取温度对Ti-V-Mo复合微合金化超高强度钢组织及力学性能的影响

利用OM,EBSD,TEM,XRD及物理化学相分析法,对不同卷取温度下Ti-V-Mo复合微合金化热轧高强钢的强化增量进行了估算和分析,分别讨论了卷取温度对屈服强度和MC相粒子对均匀塑性的影响规律.结果表明,在600℃卷取时具有最佳的综合力学性能:抗拉强度为1134 MPa,屈服强度为1080 MPa,延伸率为13.2%,均匀延伸率为6.8%,其析出强化增量sp在444~487 MPa范围内,甚至更高,主要是由质量分数高达72.6%的10 nm以下的(Ti,V,Mo)C粒子提供的.析出强化和细晶强化是主要的强化方式,sp的改变是导致不同卷取温度下屈服强度变化的主要因素.随着卷取温度由500℃升高至600℃,抗拉强度和屈服强度均不断增加,均匀延伸率不但没有降低,反而呈线性缓慢增加.其主要原因是sp对屈服强度的贡献量不断提高,在提高强度的同时改善了均匀塑性.     

Ti微合金化700MPa级汽车大梁钢的研究

通过实验,采用低成本Ti微合金元素进行强化,获得了抗拉强度745～760MPa,下屈服强度640～655MPa,伸长率为23. 0%～23. 5%的热轧钢板。同时,通过调整热轧工艺,获得了终冷温度与热轧板强度的关系。此外,研究了轧制过程不同阶段析出相的种类、分布以及析出量的变化情况。结果表明,钢板屈服强度、抗拉强度与其终冷温度基本呈线性关系,随终冷温度的降低,屈服强度和抗拉强度均明显提高。析出相的定量分析结果表明,在粗轧结束时,Ti的析出率接近50%,在精轧结束时,Ti的析出率接近60%。在700℃等温卷取后,Ti的析出率超过95%。降低卷取温度到650、600℃时,Ti的析出率分别降低到87. 5%、75. 2%。如果700℃终冷后采用空冷方式冷却,Ti的析出率最低,降低到只有63. 3%,与精轧结束时析出量相近。     

冷却工艺对微合金化高强度钢板组织与力学性能的影响

以550MPa级微合金化高强度钢为研究对象,研究了冷却模式和卷取温度对钢板力学性能与显微组织的影响。结果表明,冷却方式对钢板的组织与性能影响较小。卷取温度为605℃时,抗拉强度达到702 MPa,-20℃冲击功为63.4 J。     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

THERMODYNAMICS STUDY ON THE DECOMPOSITION OF CHROMITE WITH KOH

Institute of Process Engineering, Chinese Academy of Sciences, China, has proposed a method for oxidative leaching of chromite with potassium hydroxide. Understanding the mechanism of chromite decomposition, especially in the potassium hydroxide fusion, is important for the optimization of the operating parameters of the oxidative leaching process. A traditional thermodynamic method is proposed and the thermal decomposition and the reaction decomposition during the oxidative leaching of chromite with KOH and oxygen is discussed, which suggests that chromite is mainly destroyed by reactions with KOH and oxygen. Meanwhile, equilibrium of the main reactions of the above process was calculated at different temperatures and oxygen partial pressures. The stable zones of productions, namely, K2CrO4 and Fe2O3, increase with the decrease of temperature, which indicates that higher temperature is not beneficial to thermodynamic reactions. In addition, a comparison of the general alkali methods is carried out, and it is concluded that the KOH leaching process is thermodynamically superior to the conventional chromate production process.     

INFLUENCE OF HEAT TREATMENT ON DAMPING BEHAVIOUR OF THE MAGNESIUM WROUGHT ALLOY AZ61

The effect of isochronal heat treatments for 1h on variation of damping, hardness and microstructural change of the magnesium wrought alloy AZ61 was investigated. Damping and hardness behaviour could be attributed to the evolution of precipitation process. The influence of precipitation on damping behaviour was explained in the framework of the dislocation string model of Granato and Lücke.     

Theoretical Analysis for the Motion and Temperature of Melt Droplets in Spray Degassing Process

The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results.     

Growth Kinetics of Single Inclusion Particle in Molten Melts

On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes＇ collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process.     

An Easy Way to Quantify the Adhesion Energy of Nanostructured Cu/X(X=Cr,Ta,Mo,Nb,Zr) Multilayer Films Adherent to Polyimide Substrates

An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models.     

High-Speed Friction Stir Welding of SiC_p/Al–Mg–Si–Cu Composite

A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency.     

Three-Dimensional Growth of Coherent Ferrite in Austenite: A Molecular Dynamics Study

Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.