7A52铝合金搅拌摩擦焊的焊缝成形

针对7．6mm厚的7A52铝合金，研究了搅拌头的形状和焊接工艺参数对焊缝成形的影响，分析了搅拌摩擦焊缺陷产生的原因。结果表明，搅拌头的形状决定了焊接时焊缝成形的旋转速度范围；搅拌头旋转速度、焊接移动速度、焊接倾角、搅拌头轴肩压入被焊接件表面深度等都对搅拌摩擦焊焊缝成形有重要影响，只有合适的工艺匹配才能保证焊缝成形良好。     

搅拌摩擦焊接工艺参数对AA6061-B4C焊接接头抗拉强度的影响（英文）

搅拌摩擦焊(FSW)是一种固态连接技术,可用来连接高强度铝合金及多种陶瓷颗粒增强金属基复合材料(MMCs)。搅拌摩擦焊获得的陶瓷增强金属基复合材料焊缝优良,在增强体与基体间没有发生有害反应。对搅拌摩擦焊接工艺参数对AA6061-B4C焊接接头抗拉强度的影响进行研究。采用4因素5水平的中心复合设计来控制实验的次数。构建一数学模型来分析搅拌摩擦焊工艺参数对接头抗拉强度的影响。结果表明,在旋转速度1000r/min、焊接速度1.3mm/s、轴向力10kN、增强相含量12%的条件下,搅拌摩擦焊得到的焊接接头的抗拉强度最大。根据构建的模型采用广义简约梯度算法进行优化以得到最大的抗拉强度。金相分析表明,在焊接接头中出现了多种区域,如焊合区、热力影响区和热影响区。在焊合区观察到大量的被细化的铝基体晶粒以及粒径明显减小的B4C颗粒。在热力影响区出现塑性变形、热影响和被拉长的铝晶粒。     

焊接参数对5A06铝合金搅拌摩擦焊接头性能的影响

采用搅拌摩擦焊工艺对10 mm厚的5A06铝合金板进行焊接,研究了搅拌头转速(150～400 r/min)、焊接速度(50～200 mm/min)对接头显微组织、拉伸性能和硬度的影响。结果表明:在试验参数范围内焊接均可获得无宏观缺陷且成形良好的搅拌摩擦焊接头;接头焊核区晶粒细小、组织均匀,热机影响区晶粒相比焊核区的粗大,当搅拌头转速为400 r/min、焊接速度为50 mm/min时,接头焊核区和热机影响区的组织明显粗大;当焊接热输入特征值,即焊接速度与搅拌头转速的比值在0.3～0.5 mm/r时,焊接接头的拉伸性能与母材相当,其抗拉强度最高可达381 MPa,断后伸长率可达25.4%;接头焊核区硬度最高,热影响区硬度最低,当搅拌头转速为250 r/min、焊接速度为100 mm/min时,焊核区硬度较高。     

工艺参数对搅拌摩擦焊洋葱圆环形成的影响

搅拌摩擦焊中焊缝材料的流动对焊件性能有很大影响，洋葱圆环是搅拌摩擦焊焊焊核区中材料流动的集中体现，文中对5mm厚的1060、3003铝合金板材进行了搅拌摩擦焊连接，通过对其焊核区腐蚀后的形貌观察分析研究了不同工艺参数下材料的流动形态，结果表明，工艺参数对搅拌摩擦焊焊核区洋葱圆环的形成有很大影响，采用较高的搅拌头转速和合适的焊接速度可获得稳定，质量良好的搅拌摩擦焊接头。     

AA5083铝合金的搅拌摩擦焊接工艺参数对搅拌头受力和热输入的影响(英文)

采用系统实验设计方法研究AA5083铝合金搅拌摩擦焊接工艺参数对搅拌头受力和热量输入的影响,得到了用来设计搅拌摩擦焊搅拌头和焊机的经验模型。当采用计算机来控制搅拌摩擦焊接时,这些模型可用来确定AA5083这类铝合金的摩擦焊接工艺参数、编制焊接程序及工艺参数控制。结果表明:影响轴向力和热量输入的重要参数是搅拌头转速、焊接速度和搅拌头轴肩直径,而影响纵向应力的重要参数是焊接速度和探头直径。     

LF21板搅拌摩擦焊接头组织与焊接工艺关系的研究

利用搅拌摩擦焊方法对LF21铝合金板进行了焊接实验。分析了接头组织分区情况，探讨了搅拌头尺寸及焊接工艺参数对其接头组织的影响。经过实验得知：焊接时，搅拌头旋转速度为950～1500r／min，焊接速度为23．5-375mm／min，皆可获得接头性能尚可的焊接接头。同时发现，搅拌头旋转速度与焊接速度越小焊缝组织越细小：当两焊板间留有间隙时对焊缝孔洞的形成有一定的影响。     

搅拌摩擦焊概述（一）

搅拌摩擦焊专栏是《现代焊接》杂志与中国搅拌摩擦焊中心合作开辟的搅拌摩擦焊技术的科普专栏，包括以下专题——搅拌摩擦焊概述，搅拌摩擦焊优点。搅拌摩擦焊原理，搅拌摩擦焊历史，搅拌摩擦焊应用，搅拌摩擦焊设备，搅拌头设计和材料，搅拌摩擦焊可控参数和过程控制，搅拌摩擦焊匙孔去除技术，搅拌摩擦焊工艺改进，搅拌摩擦焊接头性能，搅拌摩擦焊点焊，铜、镁、钛、钢的搅拌摩擦焊，搅拌摩擦焊接头及夹具设计，搅拌摩擦焊检测技术，搅拌摩擦焊质量控制等。敬请关注![编者按]     

搅拌摩擦焊工艺对AZ31合金组织性能的影响

研究了焊接速度、搅拌头转速对AZ31合金搅拌摩擦焊接头显微组织和力学性能的影响,分析了焊接工艺参数的作用机理。结果表明,焊接速度过低(250 mm/min)或者搅拌头转速过高(650、700 r/min),焊核区的条带区中都会产生孔洞缺陷。随着焊接速度的增加,焊核区和热影响区的晶粒尺寸都呈现逐渐减小的趋势,合金的抗拉强度和断后伸长率都表现为先升高后降低的趋势。随着搅拌头转速的增加,焊核区和热影响区的晶粒尺寸都呈现逐渐增加的趋势,合金的抗拉强度和断后伸长率呈现先增加后减小的趋势。AZ31合金适宜的搅拌摩擦焊工艺为焊接速度400 r/min、搅拌头转速550 r/min,此时搅拌摩擦焊接头的抗拉强度和断后伸长率分别为202 MPa和5.0%,断裂位置位于后退侧热影响区。     

搅拌工具尺寸和工艺参数对塑料搅拌摩擦焊焊缝质量的影响

用不同尺寸的搅拌工具对聚氯乙烯(PVC)板材进行了搅拌摩擦对接焊工艺试验.试验证明,在搅拌工具肩部直径为30 mm,搅拌头直径为10 mm,搅拌头旋转速度为1 660 r/min,焊接速度为25 mm/min的情况下,可以得到焊缝饱满、成形美观的焊接接头.提高搅拌头的旋转速度可以成比例地提高焊接温度;焊接速度的影响较复杂,增大焊接速度一方面会降低焊接热输入,一方面又会间接地增大搅拌头的进给阻力,从而增大摩擦发热功率,提高焊接温度;搅拌工具肩部直径直接影响肩部与被焊材料表面的摩擦发热功率,增大肩部直径可以提高焊接温度,还有利于阻止焊缝材料的飞溅和外溢;而搅拌头直径的影响较复杂,增大它既可以提高搅拌头侧面与被焊材料之间的相对运动线速度,从而提高焊接温度,又会增加被焊材料的吸热功率和传热面积,从而降低焊接温度.     

2A12厚板铝合金搅拌摩擦焊接头组织性能研究

本文通过对航空航天结构件常用的2A12@g合金的搅拌摩擦焊实验，研究了在不同焊接工艺下焊缝组织及接头的力学性能。研究结果表明，用搅拌摩擦焊方法焊接板厚12mm的2A12铝合金，当工艺参数合适时，可获得成形美观、内部无缺陷、几乎无变形的平板对接接头。从显微组织角度，焊接接头可分为不同区域。力学性能实验表明，接头的抗拉强度可达母材的86％，高于熔焊接头的强度，断裂位置大多位于热影响区。     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

THERMODYNAMICS STUDY ON THE DECOMPOSITION OF CHROMITE WITH KOH

Institute of Process Engineering, Chinese Academy of Sciences, China, has proposed a method for oxidative leaching of chromite with potassium hydroxide. Understanding the mechanism of chromite decomposition, especially in the potassium hydroxide fusion, is important for the optimization of the operating parameters of the oxidative leaching process. A traditional thermodynamic method is proposed and the thermal decomposition and the reaction decomposition during the oxidative leaching of chromite with KOH and oxygen is discussed, which suggests that chromite is mainly destroyed by reactions with KOH and oxygen. Meanwhile, equilibrium of the main reactions of the above process was calculated at different temperatures and oxygen partial pressures. The stable zones of productions, namely, K2CrO4 and Fe2O3, increase with the decrease of temperature, which indicates that higher temperature is not beneficial to thermodynamic reactions. In addition, a comparison of the general alkali methods is carried out, and it is concluded that the KOH leaching process is thermodynamically superior to the conventional chromate production process.     

INFLUENCE OF HEAT TREATMENT ON DAMPING BEHAVIOUR OF THE MAGNESIUM WROUGHT ALLOY AZ61

The effect of isochronal heat treatments for 1h on variation of damping, hardness and microstructural change of the magnesium wrought alloy AZ61 was investigated. Damping and hardness behaviour could be attributed to the evolution of precipitation process. The influence of precipitation on damping behaviour was explained in the framework of the dislocation string model of Granato and Lücke.     

Theoretical Analysis for the Motion and Temperature of Melt Droplets in Spray Degassing Process

The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results.     

Growth Kinetics of Single Inclusion Particle in Molten Melts

On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes＇ collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process.     

An Easy Way to Quantify the Adhesion Energy of Nanostructured Cu/X(X=Cr,Ta,Mo,Nb,Zr) Multilayer Films Adherent to Polyimide Substrates

An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models.     

High-Speed Friction Stir Welding of SiC_p/Al–Mg–Si–Cu Composite

A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

A STUDY OF TEMPERATURE-DEPENDENT VALENCE BOND STRUCTURE OF TITANIUM

On the basis of energy and shape method for the determination of the valence bond (VB) structures of crystal, the valence bond structure of titanium is redetermined at room temperature and calculated in the whole temperature range of 0-1943K. The outer shell electronic distribution of Ti is e_c~(2.9907) · (s_c~(0.4980) d_c~(2.4927)) ef1.0093 in crystal. The temperature dependences of the VB structures of hcp and bcc phases are the same. The VB structures of hcp and bcc phases monotonically increase or decrease with the increase in temperature, but show discontinuous changes at the phase-transformation temperature 1155K.