共查询到19条相似文献,搜索用时 93 毫秒
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超临界CO2萃取的研究进展 总被引:2,自引:0,他引:2
超临界CO2流体萃取技术是近年来兴起的一项具有精馏和萃取两过程的高新物质分离精制技术,文章主要通过对各类超临界CO2流体萃取实验的文献报道和实验操作进行分析,对超临界CO2流体革取技术的原理、特点和超临界CO2流体萃取的主要影响因素及其优化方法和经验模型进行了综述。 相似文献
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超临界CO2流体萃取中的在线检测技术 总被引:3,自引:1,他引:2
综述了超临界CO2流体萃取中的在线检测技术,介绍了超临界CO2流体萃取与超临界流体色谱、气相色谱、高效液相色谱、核磁共振、近红外光谱等技术的联用在线检测,阐述了在线检测技术的优越性,提出了如何发展超临界CO2流体萃取中的在线检测技术。 相似文献
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针对超临界CO2流体萃取装置的工艺特点,分析了超临界CO2流体萃取装置中主要污染物的组成种类及其主要来源,指出噪声是超临界CO2流体萃取装置的主要污染物,同时提出从污染源着手,控制和减少超临界CO2流体萃取装置污染的一些措施。 相似文献
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超临界CO2萃取的研究进展 总被引:3,自引:0,他引:3
通过对各类超临界CO2流体萃取实验的文献报道和实验操作进行分析,对超临界CO2流体萃取技术的原理、特点和超临界CO2流体萃取的主要影响因素及其优化方法和经验模型进行了综述. 相似文献
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针对超临界CO2流体萃取装置的工艺特点,分析了超临界CO2流体萃取装置中主要污染物的组成种类及其主要来源,指出噪声是超临界CO2流体萃取装置的主要污染物,同时提出从污染源着手,控制和减少超临界CO2流体萃取装置污染的一些措施. 相似文献
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本文论述了超临界萃取中药提取在中药产业化形势及应用新技术的意义,超临界CO2流体萃取新技术在中药提取分离中的应用及其优越性。同时阐述了超临界CO2流体萃取技术在中药提取分离及中药现代化中的应用方式及前景。 相似文献
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超临界CO2流体萃取技术已成为一种新兴分离技术,具有操作简单、快速、效率高、无毒、无污染等优点使其广泛应用于各个领域。文章主要介绍了超临界CO2流体萃取技术的原理及优点,综述了近年来超临界流体萃取技术在食品工业、天然香料工业及中草药开发中的应用,并进行了展望,指出了存在的问题和今后发展的趋势。 相似文献
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超临界萃取技术及其应用 总被引:3,自引:0,他引:3
方立 《化学推进剂与高分子材料》2009,7(4):34-36,48
回顾了超临界流体(SCF)的研究历史,介绍了超临界流体的特性,分析了一元和三元体系的高压相图,简述了超临界流体萃取技术的原理、萃取过程和技术特点,并举例说明了CO2超临界流体在天然药物成分提取中的应用。 相似文献
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随着化工工程的发展,超临界技术得以发展并被广泛的应用到了各个领域之中,尤其是石油化工行业。二氧化碳、乙醇、丙烯等气体都可作为流体萃取的溶剂,而在石油工业中,二氧化碳萃取具有独特的优势。对以二氧化碳为溶剂的超临界流体萃取技术在石油工业中的应用情况进行分析与探究。 相似文献
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超临界二氧化碳萃取蛋黄油实验研究 总被引:4,自引:2,他引:2
介绍了超临界二氧化碳萃取技术提取蛋黄洫的工作原理及工艺流程。设计了正交实验.考察萃取压力、萃取温度、萃取时间等参数对萃取率的影响,确定了最佳工艺条件。 相似文献
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The extraction of L-proline from the fermentation broth filtrate with the supercritical fluid was studied. It has been proved that L-proline and most amino acids are hardly dissolved in the pure supercritical carbon dioxide fluid. When the methyl alcohol was added as an entrainer in L-proline solution or carbon dioxide fluid, the solubility of L-proline in the supercritical fluid would be greatly increased, but ethyl alcohol was unsatisfactory as an entrainer.The influences of extraction pressure, temperature, time, flow rate of fluid, concentrations of L-proline and entrainer on the yield of L-proline have been investigated for searching the optimal extraction conditions. 相似文献
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Eduardo Vyhmeister Humberto Estay Julio Romero Francisco Cubillos 《Chemical Engineering Communications》2013,200(5):644-657
Supercritical fluid and membrane technology coupling is a relatively new concept applicable to solvent separation and solute extraction. In these processes a hydrophobic or hydrophilic macroporous membrane is used as a two-different-nature solutions contactor. This methodology is an alternative to conventional liquid solution supercritical fluid extraction processes, which are associated with high investment costs. In the present work, a membrane-based supercritical fluid extraction module is modeled, simulated, and optimized as an independent industrial-scale operational unit. UniSim design suite R390 software from Honeywell was used as the platform for the simulation. Acetone and ethanol literature extraction results and methanol experimental extraction results (27.6% to 14.5% with a 10 wt.% aqueous solution; 7.1% to 5.9% with a 500 ppm aqueous solution) were used for validation of the model and definition of the semi-empirical equation parameters. The generated industrial-scale system optimization, which used a modular membrane arrangement, was strongly dependent on thermodynamic, economic, and energetic variables (higher mass transfer resistance in the carbon dioxide phase increased the number of membranes needed; process feasibility was affected by the number of membrane units, carbon dioxide flow rate, and product added value; compression energy requirements affected the optimization result). The modeled system proved to be an important aid in the design, scaling, and optimization of systems that use membranes as phase contactors in liquid solution supercritical carbon dioxide extraction. 相似文献
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Senka Vidović Ibrahim Mujić Zoran Zeković Žika Lepojević Svetlana Milošević Stela Jokić 《Journal of the American Oil Chemists' Society》2011,88(8):1189-1196
Mushrooms contain many valuable compounds such as fatty acids, carbohydrates, lycopene, lovastatin, trace elements etc. As
they are currently valued for biologically active substances, and as high pressure carbon dioxide fluid extraction has been
documented as an effective method for preparing bioactive products from plant materials, subcritical and supercritical carbon
dioxide extraction of Boletus edulis mushroom was performed. In the extracts obtained, the fatty acids were determined. Response surface methodology (RSM) was
applied to investigate the effect of pressure and extraction time on the extraction yield. The analysis of variance showed
that pressure and extraction time had a significant effect on the extraction yield in both investigated process. The interaction
between pressure and extraction time had a significant effect only in supercritical extraction process of B. edulis. Higher extraction yields have been obtained by subcritical carbon dioxide, and higher linoleic acid content has been determined
in extracts obtained by supercritical carbon dioxide. 相似文献