Effect of natural stitched composites on the crashworthiness of box structures

In the present paper the effects of stitching on the energy absorption and crashworthy behaviour of composite box structures will be studied. The combination of unidirectional carbon fibre-reinforced polymer (CFRP) and glass fibre-reinforced polymer (GFRP) composite materials are used to laminate the composite boxes. Delamination study in Mode-I with the same lay-up was carried out to investigate the effect of stitching on delamination crack growth on energy absorption of stitched and non-stitched composite box structures. The double cantilever beam (DCB) standard test method was chosen for delamination studies. For non-stitched and stitched composite boxes the lamina bending and brittle fracture crushing modes were observed. It was found that the stitched composite boxes which show higher fracture toughness in Mode-I delamination tests, are not necessarily able to absorb more crushing energy in comparison with non-stitched composite boxes. It was also observed that the position of stitched area can affect the crushing mode and consequently energy absorption capability of composite box structures. The main reason can be related to other mechanisms such as bending, friction and bundle fracture which significantly contribute to energy absorption. The analytical model based on energy balance approach is proposed to estimate the mean crushing force, F_m, in axial crushing of square composite box.     

Progressive crushing of stitched glass/polyester composite cylindrical shells

This paper examines the effect of mode I interlaminar fracture toughness (G_Ic) on the specific energy absorption of stitched glass/polyester composite cylindrical shells under axial compression. The laminated composite cylindrical shells used as energy absorbers, absorb large amount of impact energy during collision. Since mode I delamination in the thin wall of axially collapsed shell is one of the major energy absorbing modes, contribution of G_Ic to specific energy absorption (SEA) of tubes is significant during collision. The G_Ic values are determined through double cantilever beam (DCB) test with stitched and unstitched planar specimens. The four and six-layered cylindrical tubes of D/t ratios 29.27 and 20, respectively, with G_Ic values ranging from 1.68 to 8.09 kJ/m² are prepared by stitching and are subjected to quasi-static axial compression. Increasing G_Ic up to certain value leads to controlled progressive crushing, which is a good energy absorbing mechanism, beyond which failure is uncontrolled. Cylindrical tubes having G_Ic up to 6.34 kJ/m² leads to 40% increase in SEA for four-layered tubes and 6.6% for six-layered tubes comparing with the corresponding unstitched tubes. When the tubes have G_Ic of 8.09 kJ/m², four-layered tubes undergo unstable failure, but six-layered tubes undergo stable progressive crushing with 22% increase in SEA. Transition from stable to unstable failure depends upon the thickness of tubes. An analytical model is developed based on energy approach to predetermine the steady state mean crush load of cylindrical composite shells under axial compression. The model results are validated by experimental results, and show good agreement.     

Interlaminar fracture properties of weft-knitted/woven fabric interply hybrid composite materials

An experimental study has been undertaken to characterize the delamination behavior and tensile properties of interply hybrid laminated composites reinforced by interlock weft-knitted and woven glass fiber preform fabrics. The hybrid composites, comprising the alternate layers of interlock and uniweave fabrics, were compared to interlock knitted (only) and uniweave (only) composites with respect to delamination and tensile performances. Mode-I double cantilever beam and mode-II end-notched flexure tests were carried out to assess the interlaminar fracture toughness using aluminum-strip stiffened specimens. The mode-I and mode-II interlaminar fracture toughness values, G _IC and G _IIC, for the hybrid composite were about three and two times higher than that for the uniweave composite, respectively. The tensile strength and modulus of the hybrid composite were 315 MPa and 12.8 GPa in the wale direction, respectively, demonstrating that the strength and modulus were found to be slightly lower than those of the uniweave composite, and significantly improved in comparison with the interlock knitted composites.     

Improvement of interlaminar mechanical properties of CFRP laminates using VGCF

In order to improve the interlaminar mechanical properties of CFRP laminates, hybrid CFRP/VGCF laminates have been fabricated by using a newly-developed method, i.e., powder method, where the powder of vapor grown carbon fiber (VGCF) is added at the mid-plane of [0°/0°]₁₄ CFRP laminates. Experimental results of double cantilever beam (DCB) tests indicate the improvement on the interlaminar mechanical properties of Mode-I fracture behavior with much higher critical load P_C and fracture toughness G_IC with VGCF interlayer. Crack propagation and fracture surface have also been observed to interpret this improvement mechanism. Moreover, based on experimental G_IC, numerical simulations using finite element method (FEM) with cohesive elements have been carried out to analyze the delamination propagation. The interlaminar tensile strength of hybrid CFRP/VGCF laminates, which is obtained by matching the numerical load–COD (crack opening displacement) curves to experimental ones, is higher than that of base CFRP laminates.     

Fracture and fatigue study of unidirectional glass/epoxy laminate under different mode of loading

Interlaminar fracture is the dominant failure mechanism in most advanced composite materials. The delaminating behaviour of materials is quantified in terms of the strain energy release rate G. In this paper, the experimental measurements of the fatigue delaminating growth for some combinations of energy release rate mode ratio have been carried out on unidirectional glass/epoxy laminates. On this base the constants in the Paris equation have been determined for each G_II/G_T considered modal ratio. The fatigue threshold strain energy release rate Δ G_Tth , below which delaminating doesn't occur, were measured. Three type specimens were tested, namely: double cantilever beam (DCB), end‐loaded split (ELS) and mixed‐mode bending (MMB) under mode I, mode II and mixed‐mode (I + II) loading, respectively. Scanning electron microscopy techniques were used to identify the fatigue delamination growth mechanisms and to define the differences between the various modes of fracture.     

Interlaminar fracture toughness and associated fracture behaviour of bead-filled epoxy/glass fibre hybrid composites

To investigate enhancement of matrix-dominated properties (such as interlaminar fracture toughness) of a composite laminate, two different bead-filled epoxies were used as matrices for the bead-filled epoxy/glass fibre hybrid composites. The plane strain fracture toughness of two different bead-filled epoxies have been measured using compact tension specimens. Significant increases in toughness were observed. Based on these results the interlaminar fracture toughness and fracture behaviour of hybrid composites, fabricated using bead-filled epoxy matrices, have been investigated using double cantilever beam and end notch flexure specimens for Mode I and Mode II tests, respectively. The hybrid composites based on carbon bead-filled matrix shows an increase in both G _IC initiation and G _IIC values as compared to a glass fibre reinforced plastic laminate with unmodified epoxy matrix. The optimum bead volume fraction for the hybrid composite is between 15% and 20%. However, the unmodified epoxy glass-fibre composite shows a higher G _IC propagation value than that of hybrid composites, due to fibre bridging, which is less pronounced in the hybrids as the presence of the beads results in a matrix-rich interply region.     

Interlaminar Fracture Toughness of CF/PEI and GF/PEI Composites at Elevated Temperatures

An experimental study has been conducted to assess temperature effects on mode-I and mode-II interlaminar fracture toughness of carbon fibre/polyetherimide (CF/PEI) and glass fibre/polyetherimide (GF/PEI) thermoplastic composites. Mode-I double cantilever beam (DCB) and mode-II end notched flexure (ENF) tests were carried out in a temperature range from 25 to 130°C. For both composite systems, the initiation toughness, G _IC,ini and G _IIC,ini, of mode-I and mode-II interlaminar fracture decreased with an increase in temperature, while the propagation toughness, G _IC,prop and G _IIC,prop, displayed a reverse trend. Three main mechanisms were identified to contribute to the interlaminar fracture toughness, namely matrix deformation, fibre/matrix interfacial failure and fibre bridging during the delamination process. At delamination initiation, the weakened fibre/matrix interface at elevated temperatures plays an overriding role with the delamination growth initiating at the fibre/matrix interface, rather than from a blunt crack tip introduced by the insert film, leading to low values of G _IC,ini and G _IIC,ini. On the other hand, during delamination propagation, enhanced matrix deformation at elevated temperatures and fibre bridging promoted by weakened fibre/matrix interface result in greater G _IC,prop values. Meanwhile enhanced matrix toughness and ductility at elevated temperatures also increase the stability of mode-II crack growth.     

Post-buckling failure in multi-delaminated composite wind turbine blade materials

This study models the inter-laminar damage due to low velocity impacts on hybrid composite materials typical of those used in wind turbine blade structures. The effect of z-pinning using natural flax yarn on the critical buckling load and post-buckling behaviour of multi-delaminated composite beams was investigated. Laminated composite beams were pinned through their thickness using natural flax yarns to control delamination failure during the post-buckling process. A multiple delamination with a triangular shape was inserted into each of the beams to simulate the damage caused by a low velocity impact e.g. ice, on composite wind turbine blades. For a laminate design of [C₉₀/G₉₀]₄, global collapse caused no delamination failure during the post-buckling test while delamination failure occurred for a laminate design of [C₀/G₀]₄. In this case, z-pinning can significantly increase the failure resistance within a composite structure and it can then postpone the failure process. The buckling process of a multi-delaminated composite beam was also simulated by finite element software ANSYS and the results were substantially verified by relevant experimental results.     

Influence of adsorption behaviour of a silane coupling agent on interlaminar fracture in glass fibre fabric-reinforced unsaturated polyester laminates

The relationship between the interphase consisting of physisorbed and chemisorbed silane on glass fibres and the resultant composite Mode I delamination fracture toughness in glass fibre fabric laminate, was studied. The Mode I interlaminar fracture toughness of the laminate specimen was obtained by using a double cantilever beam (DCB) specimen. The delamination resistance of the laminate specimen finished with two silane concentrations and washed in methanol solvent, is discussed on the basis of the interlaminar fracture toughness. In order to determine the amount of physisorbed and chemisorbed silane on the glass fibre, the amount of total carbon was determined using an analysis instrument. The physisorbed silane migrated into the resin matrix and influenced the mechanical properties and interlaminar fracture of the laminate specimen. The amount of unsaturated polyester resin blended with a silane coupling agent was measured using dynamic mechanical spectroscopy, and a DCB specimen for mechanical properties and fracture toughness.     

平纹织物结构对织物增强复合材料层间断裂韧性影响的研究

本文采用粘贴片式双悬臂梁(DCB)试件和端部切口弯曲(ENF)试件研究了平纹织物的经纬纱密度对玻璃平纹织物/环氧树脂复合材料的Ⅰ型和Ⅱ型层间断裂韧性的影响。实验结果表明织物的密度对层间断裂韧性有显著的影响。提出了在织物增强复合材料层合板中,基体在织物孔洞中形成层间铆接,并且就其与层间G_IC和G_IC的关系进行了研究。      

Interaction of laminate damage and adhesive disbonding in composite scarf joints subjected to combined in-plane loading and impact

Impact tests were carried out on composite laminates and composite scarf repairs, while both were subjected to in-plane loading with tensile pre-strain levels up to 5000 microstrain. The results show that pre-straining of the composite laminates has no noticeable influence on the size of the delamination area for the given impact energy of 8 J, which represents a typical barely-visible impact on thin-skin composite structures. For composite scarf joints, however, resulting damage has been found to be a combination of adhesive disbonding and matrix cracking (delamination and intraply cracking) in the composite laminate. The size of this mixed type of damage increases significantly with increasing pre-strain levels. A finite element model was developed to investigate the interaction between adhesive disbonding and composite delamination. The computational results reveal that both delamination and adhesive disbonding are dominated by the mode II fracture. Since the critical mode II fracture energy release rate for composite laminates (G_IIC = 1.08 kJ/m²) is much less than that pertinent to the adhesive (G_IIC = 3.73 kJ/m²), delamination tends to occur first in the composite laminates, which then shield the growth of disbonding in the adhesive.     

An integrated approach based on acoustic emission and mechanical information to evaluate the delamination fracture toughness at mode I in composite laminate

This paper addresses a new method based on the combination of mechanical behavior and acoustic emission (AE) information of composite materials during mode I delamination. The method is based on a special purpose function, called sentry function, which is defined as the logarithm of the ratio between mechanical energy and acoustic energy (f = Ln(E_s/E_a)). The sentry function is used to study the delamination process and to evaluate the delamination fracture toughness in mode I. The relationship between cumulative fracture toughness energy release rate (G_I) and the integral of the sentry function during crack propagation showed a transition point with two sensitive regions below and above it. This behavior can be followed to obtain the critical strain energy release rate value (G_Ic). Results obtained by means of the sentry function are compared with results obtained by a methodology proposed by other authors.     

Delamination of multidirectional composite laminates at 0°/θ° ply interfaces

The main objective of this study is to develop a methodology for establishing mixed-mode delamination propagation criteria of non-unidirectional laminates. The crack interface was chosen to be 0°/45° and the effort was mainly focused on obtaining the mode I fracture toughness (G_IC). The widely used DCB test was avoided due to anticipated problems with intralaminar damage developing at the ply interface of interest. The ADCB and AMMF methods were used to determine the mixed-mode fracture toughness with the largest amount of mode I. The selected stacking sequence resulted in desirable crack propagation behavior; there was no change of delamination plane, an acceptable crack front profile, no initial specimen curvature, and no energy dissipation through global specimen damage. Finite element simulation was found to be the only tool capable of analyzing the experimental data.     

Carbon nanotube shear-pressed sheet interleaves for Mode I interlaminar fracture toughness enhancement

Failure of composite laminates is often the result of “secondary” transverse stresses causing delamination. One well known approach to prevent such failure is to incorporate a distinct interleaf material into the interlaminar region in order to increase its fracture toughness and, consequently, its resistance to delamination. In the recent years various carbon nanotube (CNT) interleaves gained much attention. This work presents experimental study of the Mode I progressive fracture of carbon/epoxy composite laminates modified with high volume fraction, aligned, non-functionalized and functionalized CNT interleaves. The interleaves used here are thin solid sheets produced from vertically grown multiwalled CNT arrays by shear pressing method. A dry or resin infused sheet is integrated between prepreg plies prior to the laminate cure. The obtained results show that both dry and pre-infused CNT interleaves significantly, up to two times, increase the critical strain energy release rate of the baseline non-interleaved laminate. Two methods of functionalizing CNTs within the preform are explored: O₂/CF₄ plasma and H₂SO₄/KnO₄ wet chemical treatments. Both methods maintain the high alignment and aspect ratio of the CNTs. Although, functionalization results in no additional G_IC toughening compared to the non-functionalized interleaves, the characteristics of the fracture surfaces are dramatically different.     

Influence of silane coupling agents on interlaminar fracture in glass fibre fabric reinforced unsaturated polyester laminates

The relationship between the adhesive properties of the interphase of glass fibre/resin and the resultant composite Mode I delamination fracture toughness in glass fibre fabric laminate (GFFL) was studied. The Mode I interlaminar fracture toughness of GFFL was obtained by using a double cantilever beam (DCB) specimen. The delamination resistance of GFFLs which have two silane coupling agents and three concentration finishes is discussed on the basis of interlaminar fracture toughness. The crack propagation behaviour of DCB testing was mainly divided into stable and unstable manners. The fracture toughness and the crack propagation behaviour were dependent on the types and concentration of silane coupling agents.     

An analytical analysis of energy release rate in bonded composite joints in a mode I condition

A complete analytical solution of mode I strain energy release rate, G_I, was derived for bonded composite joints based on an augmented double cantilever beam (DCB) model. Good agreement was obtained between current and existing comparable theoretical solutions for this joint with a long adhesive bond. For a short bond length joint, the current solution can greatly reduce the degree of the mathematical singularity encountered in analyses of thick, short beams and avoid it entirely for thin, long beams. A correlation between the current theoretical and associated ASTM solutions was established. A bonded DCB laminate test case was conducted, and good agreement was obtained between the experimental and current theoretical results. Commentary was included regarding the tested critical strain energy release rate and the deduced critical adhesive peel stress.     

Damage performance of particles filled quasi-isotropic glass–fibre reinforced polyester resin composites

The purpose of this work was to determine the toughening mechanisms in interlayered quasi-isotropic glass–fibre reinforced polyester resin (GFRP) composites. Particles of polyethylene and aluminium tri-hydrate, Al(OH)3, were mixed with the polyester resin prior to laminating with woven E-glass-fibre cloth. Mode-I, mode-II, and impact tests were performed to determine critical strain energy-release rates (GIc and GIIc), absorbed energy and residual compressive strength for the laminates with and without particulate additions. Mode-I and mode-II delamination toughness were characterized using double cantilever beam (DCB) and end-notched flexure (ENF) specimens, respectively, and the delaminated surfaces of specimens were examined using scanning electron microscopy (SEM) to investigate the interlaminar morphology after fracture. The results indicate that the interlaminar toughness (GIc and GIIc), absorbed energy and residual compressive strength values of the GFRP composite increases with increase of particle content. The improved behaviour of particle containing GFRP is linked to stress-concentration induced plastic deformation and crack bridging. Polyethylene particles increase the toughness of the matrix material, which results in composites with higher values of mode-I, mode-II and impact than the composites with aluminium tri-hydrate particles. © 1998 Chapman & Hall     

Effect of resin and fibre properties on impact and compression after impact performance of CFRP

The effect of resin and fibre properties on composite impact, compression after impact (CAI) and mode II energy release rate (G_IIC) performance has been studied. Impact events were instrumented to record values of P_c, the critical load for initiation of impact damage. Impact response of the laminates was strongly influenced by the fracture toughness of the resin. In contrast, use of high strength and high stiffness fibres did not improve the resistance to impact. The differences in impact and CAI response of the laminates were largely a consequence of the impact damage created at the damage threshold, P_c, rather than of the differences in delamination growth. As a strong correlation was found between G_IIC values measured by delamination tests, and those calculated from measurements of P_c, it is suggested that instrumented impact testing may be a more convenient way of determining G_IIC in CFRP laminates than delamination tests.     

Effect of the loading rate on mode I interlaminar fracture toughness of laminated composites

The objective of the present study is to determine the influence of the loading rate on the critical energy release rate G_Ic of fibre-reinforced epoxy laminates. In order to perform pure mode I loading at higher opening velocities, a new test device is developed. The approach is based on a symmetrical opening displacement applied to a DCB specimen. In the data reduction, the influence of the kinetic energy has to be taken into account. The results obtained on the unidirectional carbon-epoxy laminate T300/914 at crack opening rates up to 1.6 m/s show a slight effect of the loading rate on G_Ic.