共查询到20条相似文献,搜索用时 171 毫秒
1.
ITO透明导电薄膜以其优良的透明导电性能在平面液晶显示(LCD)、电致发光(EC)等多个领域得到了广泛的应用.制备ITO薄膜的方法很多,其中采用溶胶-凝胶法制备ITO透明导电薄膜具有成本低,设备简单,工艺可控,有利于大面积成膜等优点,因而受到了广泛的关注.较详尽地介绍了ITO薄膜的透明导电机理、溶胶-凝胶法的工艺特征,并初步论述了溶胶-凝胶法制备ITO透明导电薄膜的应用和发展前景. 相似文献
2.
ITO透明导电薄膜的制备方法及研究进展 总被引:1,自引:0,他引:1
概述了透明导电薄膜的分类及ITO薄膜的基本性质,综述了用于制备ITO薄膜的磁控溅射法、真空蒸发法、溶胶-凝胶法、喷雾热解法、化学气相沉积法,论述了不同制备方法的优缺点。最后,介绍了ITO薄膜的应用现状,并对ITO薄膜的发展趋势进行了展望。 相似文献
3.
4.
5.
6.
7.
8.
9.
10.
以钛酸丁酯为原料,采用改进的溶胶-凝胶法制备ITO负载纳米TiO2薄膜,通过XRD、SEM和UV-Vis等检测方法对薄膜样品进行表征,并考察其在双室光电化学池中制氢反应的光催化活性。结果表明:纳米TiO2薄膜为锐钛矿-金红石混晶结构,当溶胶中P25粉末含量为0.09g/mL时制备的TiO2薄膜产氢量最大,光催化性能较好。 相似文献
11.
12.
系统地研究了溶胶-凝胶(Sol-Gel)方法制备(Pb_(1-X)La_x)Ti_(1-x/4)O_3(简称PLT)薄膜时催化剂(或pH值)、溶液浓度在室温下对形成溶胶和凝胶的影响规律,用X射线结构分析和SEM研究了热处理工艺对薄膜结构及晶粒尺寸的影响。实验表明,浓度、醋酸含量都存在一个最佳的范围,且随铜(La)含量的增加,该范围减小;实验还发现,随着La含量的增加,薄膜的晶化温度降低。在单晶(100)Si衬底上成功地制备出了具有钙钛矿型结构、厚度约为200nm、均匀、致密、无裂纹的PLT晶态薄膜。 相似文献
13.
M. Premkumar S. Vadivel 《Journal of Materials Science: Materials in Electronics》2017,28(12):8460-8466
Tin doped indium oxide (ITO) thin films were prepared by sol–gel spin coating method with In (NO3)·3H2O and SnCl4·5H2O as indium and tin sources, respectively. The as deposited samples were annealed at various temperature such as, 300, 400, 500 and 600?°C for 2 h in ambient atmosphere. The grown ITO thin films are polycrystalline in nature with cubic structure of In2O3 with the space group La3 and the results are in good agreement with the standard JCPDS data (card no#06-0416). In addition crystalline size increases with increasing annealing temperature from 25 to 55 nm. Polycrystalline with uniform smooth surface was observed by SEM micrographs. The optical band gap energy was found to be decreased from 3.85 to 3.23 eV as the annealing temperature is increased from 300 to 600?°C. The humidity sensing performance (high sensitivity and fast response time) was significantly improved for 600?°C thin films samples, which is probably due to smaller energy band gap and physisorption between the water molecules and the surface of the thin films. The films were further characterized by PL and EDS analysis. The effect of temperature on humidity sensing mechanism of ITO thin films is also discussed. 相似文献
14.
Shiju Yang Fengqing Zhang Xiaobin Xie Xiaodong Guo Liping Zhang Suhua Fan 《Journal of Materials Science: Materials in Electronics》2017,28(20):14944-14948
BiFeO3 (BFO) and transition metal (Cu, Zn, Mn) doped BFO thin films were successfully fabricated on indium tin oxide (ITO)/glass substrate using sol–gel process, spin coating and layer by layer technique. Compared to the pure BFO thin film, improved ferroelectric and leakage current properties were observed in the transition metal doped BFO thin films. The transition metal (Cu, Zn, Mn) doped BFO thin films have varying degrees of lower leakage current compared with the pure BFO film. The substitution of Cu and Zn increase the remnant polarization of BFO thin films. The values of remnant polarization (2Pr) were 120.6 and 126.7 μC/cm2 at 933 kV/cm for Cu-doped and Zn-doped BFO thin film, respectively. 相似文献
15.
Manikantan K. Shanmugasundaram K. Thirunavukkarasu P. Rajamanickam A. T. 《Journal of Materials Science: Materials in Electronics》2022,33(23):18432-18451
Journal of Materials Science: Materials in Electronics - The spotlight of this research is premiering of Sol–Gel dip-coating technique in fabricating the nanorod-shaped BiVO4 with thin films... 相似文献
16.
Negar Rajabi Felora Heshmatpour Rasoul Malekfar Hamid-Reza Bahari-Poor Selda Abyar 《Materials Science-Poland》2014,32(1):102-106
Indium tin oxide (ITO) films were deposited on glass substrates by dip-coating and thermal pyrolysis methods. Sn (IV) is often used in the spray method as a precursor salt, but in this research we have employed a new procedure that uses Sn (II) and In(NO3)3 for preparation of transparent conductive thin films. Then, colloidal Ag was deposited on the ITO layers in order to compare the two synthesis methods, and the structural and electrical properties of the resultant films were investigated by FESEM, XRD, and four-terminal resistometry. The obtained films are polycrystalline with a preferred orientation of (200). The XRD patterns of the films indicate that in both films, the Sn phase is crystallized separately from In2O3. The presence of a Sn peak and the overall low intensity of XRD peaks suggest relative crystallization of ITO structure. For this reason, Ag films were deposited by dip coating method using a colloidal sol. By analyzing the XRD patterns of Ag-ITO films after eliminating the Sn peak, the increased intensity of the peaks confirmed the relatively good crystallization of the ITO films. The results show that the films with a sheet resistance as low as 2 × 10?2 Ω·cm, which is beneficial for solar cells, were achieved. 相似文献
17.
采用Sol-Gel工艺制备了Si基Bi4TiO12铁电薄膜.研究了退火温度、退火时间、薄膜厚度等对薄膜晶相结构的影响.研究表明,退火温度对Si基Bi4Ti3O12铁电薄膜晶相结构的影响最为显著,而且随退火温度升高,Bi4Ti3O12薄膜更趋向于沿c-轴取向的生长;退火时间在30分钟内对薄膜晶相结构的影响比较明显;薄膜厚度及30分钟以上的退火处理对薄膜晶相结构的影响不大. 相似文献
18.
通过微波辐射溶胶一凝胶法(sol-gel)法在导电玻璃(ITO)基体上制备TiO2纳米薄膜光催化剂,考察不同加热方式、微波时间、酸处理、薄膜层数等对TiO2纳米粒子及薄膜的影响。以可见光谱(UV-VIS)、X射线衍射(XRD)对TiO2薄膜进行了表征,并通过薄膜光催化降解铬黑T溶液的性能进行了研究。实验表明,ITO玻璃表面的TiO2纳米薄膜经HNO3和微波处理后,因协同效应使薄膜的光催化活性大大增强。 相似文献
19.
Indium tin oxide (ITO) thin films with well-controlled layer thickness were produced by dip-coating method. The ITO was synthesized by a sol-gel technique involving the use of aqueous InCl3, SnCl4 and NH3 solutions. To obtain stable sols for thin film preparation, as-prepared Sn-doped indium hydroxide was dialyzed, aged, and dispersed in ethanol. Polyvinylpyrrolidone (PVP) was applied to enhance the stability of the resulting ethanolic sols. The transparent, conductive ITO films on glass substrates were characterized by X-ray diffraction, scanning electron microscopy and UV-Vis spectroscopy. The ITO layer thickness increased linearly during the dipping cycles, which permits excellent controllability of the film thickness in the range ~ 40-1160 nm. After calcination at 550 °C, the initial indium tin hydroxide films were transformed completely to nanocrystalline ITO with cubic and rhombohedral structure. The effects of PVP on the optical, morphological and electrical properties of ITO are discussed. 相似文献