DIN-100MnCrW4模具钢开裂原因分析

对DIN－100MnCrW4模具钢开裂原因进行了分析。结果表明，模具钢 属淬火开裂，主要原因是材料内部组织不均匀所致。     

Cr12MoV模具钢宽带激光淬火开裂的组织分析

分析了Cr12MoV模具钢淬火开裂原因,借助于扫描电镜和光镜,观察断口表面形貌和金相组织,根据断口特征和金相组织分析,该模具钢淬火开裂的主要原因是晶粒粗大、碳化物呈不均匀状态分布。     

水溶性淬火介质JX-1118型在H13等热作模具钢淬火中的应用

用JX-1118水溶液作为淬火介质代替传统淬火油对H13热模具钢进行热处理,考察工件热处理后的机械性能及淬裂情况,并分别测试试样在淬火及两次回火后的洛氏硬度,分析淬火件的各种机械性能.结果表明,该介质具有理想的冷却速度和良好的淬透性,淬火后的工件获得了较理想的硬化层深度,有效地解决了油淬不硬、水淬易裂等问题,同时也改善...     

8418钢熔铝料桶开裂分析

8418热作模具钢制熔铝料桶使用过程中在冷却孔处发生开裂,采用扫描电镜及能谱仪、光学显微镜、洛氏硬度计、直读光谱仪,对其开裂原因进行了分析。结果表明,料桶冷却孔内具有含Ca、S、Cl元素的介质,导致其发生了应力腐蚀开裂。     

大型轴承钢球开裂分析

对大型轴承钢球在淬火过程中的开裂进行了失效分析,采用宏微观形貌、化学成分、金相显微组织分析、硬度测试、SEM微观断口形貌等手段,分析了钢球开裂的原因.结果表明,钢球开裂为淬火开裂,淬火温度过高是导致淬火钢球开裂的主要原因.     

模具钢淬透性及淬火变形分析研究

通过对影响模具钢淬透性因素和淬火变形的机理分析研究,指出了模具钢的淬透性及淬火热处理变形的影响因素,在制定淬火热处理工艺时,应充分考虑工件的形状、钢中的碳含量,根据工件所要求的力学性能,合理选择淬火方法及冷却介质,防止变形及开裂,以提高产品质量。     

3Cr2W8V钢热作模具早期开裂原因及对策

分析了3Cr2W8V钢制P-Cu合金焊料热挤压模、呆扳手热锻模和电力扣件热锻模淬火时或使用中多次发生早期开裂的原因。针对错综复杂的失效现象，利用扫描电镜等设备分析了断口的宏观和微观形貌、碳化物分布等显微组织特征。从模具生产过程研究表明，几种模具开裂原因并不相同，逐一采取了相应对策，取得良好效果。     

一种新型热作模具钢热处理工艺

研究了热处理工艺对一种新型热作模具钢组织和性能的影响。结果表明:低于1100℃淬火,存在带状组织及偏析,硬度和磨损性能较低。1100℃淬火时,组织比较均匀,有较好的硬度和耐磨性。淬火温度升高到1150℃时,形成粗大的马氏体组织,硬度降低,磨损量增加。该热作模具钢经1100℃淬火后,在回火过程中,逐渐析出碳化物,析出的碳化物类型由渗碳体逐渐向合金碳化物转变,硬度和磨损抗力增加。当回火温度进一步升高时,合金碳化物尺寸逐渐增大,晶粒粗化,这些原因都导致该热作模具钢硬度下降,磨损量升高。该热作模具钢较佳的热处理工艺为:1100℃/油淬+2次560℃×2 h回火。     

H13钢的热处理工艺研究

H13钢(4Cr5MoVlSi)是新型的热作模具钢,可以广泛用于要求高韧性和冷热疲劳抗力,工作温度≤700℃的热作模具或轴类件。本文论述了不同锻后退火工艺、淬火工艺、回火工艺对该钢组织和性能的影响,提出了最佳热处理工艺参数。实践证明,能提高H13钢的使用寿命和性能,具有明显的经济效益。     

模具钢淬透性及淬火变形分析研究

通过对影响模具钢淬透性因素和淬火变形的机理分析研究,指出模具钢的淬透性及淬火热处理变形的影响因素是十分复杂的问题。在制定淬火热处理工艺时,应充分考虑工件的形状、钢中的碳含量,根据工件所要求的力学性能,合理选择淬火方法及冷却介质,防止变形及开裂,提高产品质量。     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

THERMODYNAMICS STUDY ON THE DECOMPOSITION OF CHROMITE WITH KOH

Institute of Process Engineering, Chinese Academy of Sciences, China, has proposed a method for oxidative leaching of chromite with potassium hydroxide. Understanding the mechanism of chromite decomposition, especially in the potassium hydroxide fusion, is important for the optimization of the operating parameters of the oxidative leaching process. A traditional thermodynamic method is proposed and the thermal decomposition and the reaction decomposition during the oxidative leaching of chromite with KOH and oxygen is discussed, which suggests that chromite is mainly destroyed by reactions with KOH and oxygen. Meanwhile, equilibrium of the main reactions of the above process was calculated at different temperatures and oxygen partial pressures. The stable zones of productions, namely, K2CrO4 and Fe2O3, increase with the decrease of temperature, which indicates that higher temperature is not beneficial to thermodynamic reactions. In addition, a comparison of the general alkali methods is carried out, and it is concluded that the KOH leaching process is thermodynamically superior to the conventional chromate production process.     

INFLUENCE OF HEAT TREATMENT ON DAMPING BEHAVIOUR OF THE MAGNESIUM WROUGHT ALLOY AZ61

The effect of isochronal heat treatments for 1h on variation of damping, hardness and microstructural change of the magnesium wrought alloy AZ61 was investigated. Damping and hardness behaviour could be attributed to the evolution of precipitation process. The influence of precipitation on damping behaviour was explained in the framework of the dislocation string model of Granato and Lücke.     

Theoretical Analysis for the Motion and Temperature of Melt Droplets in Spray Degassing Process

The motion of melt droplets in spray degassing process was analyzed theoretically. The height of the treatment tank in spray degassing process could be determined by the results of theoretical calculation of motion of melt droplets. To know whether the melt droplets would solidify during spraying process, the balance temperature of melt droplets was also theoretically analyzed. Then proof experiments for theoretical results about temperature of melt droplets were carried. In comparison, the experimental results were nearly similar to the calculation results.     

Growth Kinetics of Single Inclusion Particle in Molten Melts

On the basis of the single-particle framework, a new theory on inclusion growth in metallurgical melts is developed to study the kinetics of inclusion growth on account of reaction and collision. The studies show that the early growth of inclusion depends on reaction growth and Brawnian motion collision, and where the former is decisive, the late growth depends on turbulence collision and Stokes＇ collision, and where the former is dominant; collision growth is very quick during the smelting process, lessened in the refining process, but nearly negligible in the continuous casting process.     

Three-Dimensional Growth of Coherent Ferrite in Austenite: A Molecular Dynamics Study

Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.     

An Easy Way to Quantify the Adhesion Energy of Nanostructured Cu/X(X=Cr,Ta,Mo,Nb,Zr) Multilayer Films Adherent to Polyimide Substrates

An approach based on film buckling under simple uniaxial tensile testing was utilized in this paper to quantitatively estimate the interfacial energy of the nanostructured multilayer films(NMFs) adherent to flexible substrates. The interfacial energies of polyimide-supported NMFs are determined to be *5.0 J/m2 for Cu/Cr, *4.1 J/m2 for Cu/Ta,*2.8 J/m2 for Cu/Mo, *1.1 J/m2 for Cu/Nb, and *1.2 J/m2 for Cu/Zr NMFs. Furthermore, a linear relationship between the adhesion energy and the interfacial shear strength is clearly demonstrated for the Cu-based NMFs, which is highly indicative of the applicability and reliability of the modified models.     

High-Speed Friction Stir Welding of SiC_p/Al–Mg–Si–Cu Composite

A 17 vol% SiCp/Al–Mg–Si–Cu composite plate with a thickness of 3 mm was successfully friction stir welded(FSWed) at a very high welding speed of 2000 mm/min for the first time. Microstructural observation indicated that the coarsening of the precipitates was greatly inhibited in the heat-affected zone of the FSW joint at high welding speed, due to the significantly reduced peak temperature and duration at high temperature. Therefore, prominent enhancement of the hardness was achieved at the lowest hardness zone of the FSW joint at this high welding speed, which was similar to that of the nugget zone. Furthermore, the ultimate tensile strength of the joint was as high as 369 MPa, which was much higher than that obtained at low welding speed of 100 mm/min(298 MPa). This study provides an effective method to weld aluminum matrix composite with superior quality and high welding efficiency.