Formation and mechanical properties of stationary shoulder friction stir welded 6005A-T6 aluminum alloy

6005A-T6 aluminum alloy is welded by stationary shoulder friction stir welding (SSFSW). At a constant rotational velocity of 2000 rpm, the effect of welding speed on mechanical properties of SSFSW joint are investigated in detail. Defect-free joint with gloss surface and small flash is attained and no cracks appear at the bending angle of 180°. Compared with traditional friction stir welding (FSW), width of rotational shoulder affected zone is relatively small because of the smaller diameter of rotational shoulder. Increasing welding speed is benefit for reducing the width of softening region and the softening degree. The fracture position of welding joint locates in thermo-mechanically affected zone and the fracture surface morphology presents the typical ductile fracture. The maximum tensile strength of joint at the welding speed of 400 mm/min reaches 82% of base metal (BM).     

Microstructure,mechanical and corrosion properties of friction stir welded high nitrogen nickel-free austenitic stainless steel

Friction stir welding (FSW) was applied to a 2.4 mm thick high nitrogen nickel-free austenitic stainless steel plate using tungsten–rhenium (W–Re) tool. The high-quality weld was successfully produced at a tool rotational speed of 400 rpm and a traveling speed of 100 mm/min. The microstructure, mechanical and corrosion properties of the weld were studied. The nitrogen content of the weld was almost identical to that of base metal (BM). FSW refined grains in the stir zone (SZ) through dynamic recrystallization and led to increase in hardness and tensile strength within the SZ, while the ductility was slightly decreased. The failure of tensile specimens occurred in the BM. TEM results revealed precipitates of Cr₂₃C₆ of size ~ 1 μm in the SZ, although their content was small. The precipitation of Cr₂₃C₆ and increase in δ-ferrite in the SZ led to small decrease in both pitting and intergranular corrosion resistance.     

Effect of welding parameters on microstructure and mechanical properties of AA6061-T6 butt welded joints by stationary shoulder friction stir welding

Stationary shoulder friction stir welding (SSFSW) butt welded joints were fabricated successfully for AA6061-T6 sheets with 5.0 mm thickness. The welding experiments were performed using 750–1500 rpm tool rotation speeds and 100–300 mm/min welding speeds. The effects of welding parameters on microstructure and mechanical properties for the obtained welds were discussed and analyzed in detail. It is verified that the defect-free SSFSW welds with fine and smooth surface were obtained for all the selected welding parameters, and the weld transverse sections are obviously different from that of conventional FSW joint. The SSFSW nugget zone (NZ) has “bowl-like” shapes with fairly narrow thermal mechanically affected zone (TMAZ) and heat affected zone (HAZ) and the microstructures of weld region are rather symmetrical and homogeneous. The 750–1500 rpm rotation speeds apparently increase the widths of NZ, TMAZ and HAZ, while the influences of 100–300 mm/min welding speeds on their widths are weak. The softening regions with the average hardness equivalent 60% of the base metal are produced on both advancing side and retreating side. The tensile properties of AA6061-T6 SSFSW joints are almost unaffected by the 750–1500 rpm rotation speeds for given 100 mm/min, while the changing of welding speed from 100–300 mm/min for given 1500 rpm obviously increased the tensile strength of the joint and the maximum value for welding parameter 1500 rpm and 300 mm/min reached 77.3% of the base metal strength. The tensile fracture sites always locate in HAZ either on the advancing side or retreating side of the joints.     

Effect of tool rotational speed and pin profile on microstructure and tensile strength of dissimilar friction stir welded AA5083-H111 and AA6351-T6 aluminum alloys

The relatively new welding process friction stir welding (FSW) was applied in this research work to join 6 mm thick dissimilar aluminum alloys AA5083-H111 and AA6351-T6. The effect of tool rotational speed and pin profile on the microstructure and tensile strength of the joints were studied. Dissimilar joints were made using three different tool rotational speeds of 600 rpm, 950 rpm and 1300 rpm and five different tool pin profiles of straight square (SS), straight hexagon (SH), straight octagon (SO), tapered square (TS), and tapered octagon (TO). Three different regions namely unmixed region, mechanically mixed region and mixed flow region were observed in the weld zone. The tool rotational speed and pin profile considerably influenced the microstructure and tensile strength of the joints. The joint which was fabricated using tool rotational speed of 950 rpm and straight square pin profile yielded highest tensile strength of 273 MPa. The two process parameters affected the joint strength due to variations in material flow behavior, loss of cold work in the HAZ of AA5083 side, dissolution and over aging of precipitates of AA6351 side and formation of macroscopic defects in the weld zone.     

Characterization of friction stir welded boron carbide particulate reinforced AA6061 aluminum alloy stir cast composite

Development of welding procedures to join aluminum matrix composite (AMCs) holds the key to replace conventional aluminum alloys in many applications. In this research work, AA6061/B₄C AMC was produced using stir casting route with the aid of K₂TiF₆ flux. Plates of 6 mm thickness were prepared from the castings and successfully butt joined using friction stir welding (FSW). The FSW was carried out using a tool rotational speed of 1000 rpm, welding speed of 80 mm/min and axial force of 10 kN. A tool made of high carbon high chromium steel with square pin profile was used. The microstructure of the welded joint was characterized using optical and scanning electron microscopy. The welded joint showed the presence of four zones typically observed in FSW of aluminum alloys. The weld zone showed fine grains and homogeneous distribution of B₄C particles. A joint efficiency of 93.4% was realized under the experimental conditions. But, FSW reduced the ductility of the composite.     

Microstructures and mechanical properties in dissimilar AZ91/AZ31 spot welds

The stir zone microstructures and mechanical properties of dissimilar AZ91/AZ31 friction stir spot welds made using different tool designs and tool rotational speed settings are investigated. Intermingled AZ91 and AZ31 lamellae are formed in the stir zones of dissimilar spot welds made using threaded, three-flat/0.7 mm/threaded and three-flat/no-thread tools and tool rotational speeds ranging from 1500 to 3000 rpm. The intermingled lamellae have chemical compositions, which are similar to those of the upper and lower sheets in the dissimilar sandwich. The flats on the rotating tool facilitate the downward transfer of upper and lower sheet materials in the location close to the pin periphery and therefore intermingled AZ91 and AZ31 lamellae are formed in the stir zones of dissimilar spot welds produced using a three-flat tool without a thread.The distance (Y) from the tip of the hook region to the keyhole periphery has a dominant influence on the mechanical properties of dissimilar AZ91/AZ31 spot welds, since the hook regions are curved inwards towards the axis of the rotating tool. The highest failure load properties and largest Y-values are found in dissimilar spot welds made using threaded and three-flat/0.7 mm/threaded tools and tool rotational speeds from 1500 to 3000 rpm. Dissimilar spot welds made using a rotational speed of 1000 rpm have the smallest Y-values and the lowest failure load properties.     

Microstructure and tensile strength of friction stir welded joints between interstitial free steel and commercially pure aluminium

In the present study, the joining of interstitial free steel and commercial pure aluminium was carried out by friction stir welding (FSW) technique using tool rotational speeds of 600, 900, 1200 rpm and traverse speed of 100 mm/min. The microstructure and micro-hardness of the weld interface have been investigated. Optical microscopy was used to characterize the microstructures of different regions of friction stir welding joints. The scanning electron microscopy-back scattered electron (SEM-BSE) images show the existence of the different reaction layers in the welded zone. The Al₃Fe intermetallic compound has been observed in the weld interface and their thickness increase with the increase in tool rotational speed. Tensile strength was also evaluated and maximum tensile strength of ∼123.2 MPa along with ∼4.5% elongation at fracture of the joint have been obtained when processed at 600 rpm tool rotational speed.     

Microstructure and interface characterization of dissimilar friction stir welded lap joints between Ti–6Al–4V and AISI 304

The feasibility of dissimilar friction stir welding (FSW) in overlap configuration between Ti–6Al–4V alloy (Ti64) and AISI 304 austenitic stainless steels (304SS) was investigated. Sound joints were achieved when placing titanium as the upper workpiece. Joints were successfully produced by employing a welding speed of 1 mm/s and rotational speeds of 300 and 500 rpm. A lamellar microstructure was formed in the stir zone of Ti64, where grain size was found to increase with increasing rotational speed, and austenitic equiaxed grains were obtained near the interface of 304SS coupon. Energy dispersive X-ray spectroscopy (SEM-EDS) of the interface revealed a thin intermixed region and suggested intermetallic compound formation. Microhardness data in the titanium weld zone for both rotational speeds exhibited slightly lower values than the base material, with the lowest values in the heat affected zone, whereas the microhardness values in the stainless steel side around the weld center were found to be higher than those obtained for the base material.     

AA7075 bit for repairing AA2219 keyhole by filling friction stir welding

In the present study, 7.8 mm thick AA2219 rolled plates were successfully filling friction stir welded (FFSW) without keyhole using a semi-consumable tool. The influences of the bit’s geometric parameters and the plunge speed on the joint’s mechanical properties were investigated. Microstructure of the joint, especially at the interface, was observed. The results revealed that the AA7075 bit’s employment was able to decrease the shedding bit material effectively. During tensile tests, the maximum ultimate tensile strength (UTS) and elongation of the joint were 179.6 MPa and 13.7%, equivalent to 96.6% and 99% of the original defect-free friction stir welding (FSW) joint, respectively. The defect-free FFSW joints were produced at lower plunge speeds, and the fracture locations were at the softened region within the heat affected zone (HAZ) adjacent to the thermo-mechanically affected zone (TMAZ) on the retreating side. With increasing the plunge speed, the fracture location was more mainly dependent on the interface strength instead of the hardness distribution.     

Effect of welding parameters on microstructure and mechanical properties of friction stir welded joints of a super high strength Al–Zn–Mg–Cu aluminum alloy

Samples made of a super high strength aluminum alloy with high Zn content were friction stir welded with rotation rates of 350–950 rpm and welding speeds of 50–150 mm/min. The effect of welding parameters on the microstructure and mechanical properties was investigated. It was observed that the grain size of the nugget zones decreased with the increasing welding speed or the decreasing tool rotation rate. Most of the strengthening precipitates in the nugget zone were dissolved back and the intragranular and grain boundary precipitates in the heat affected zone coarsened significantly. The greatest ultimate tensile strength of 484 MPa and largest elongation of 9.4 were obtained at 350 rpm−100 mm/min and 350 rpm−50 mm/min, respectively. The ultimate tensile strength and elongation deteriorated drastically when rotation rate increased from 350 to 950 rpm at a constant welding speed of 100 mm/min.     

Microstructural characteristics and mechanical properties of non-combustive Mg–9Al–Zn–Ca magnesium alloy friction stir welded joints

Non-combustive Mg–9Al–Zn–Ca magnesium alloy was friction stir welded with rotation speeds ranging from 500 to 1250 rpm at a constant welding speed of 200 mm/min. Defect-free joints were successfully produced at rotation speeds of 750 and 1000 rpm. The as-received hot extruded material consisted of equiaxed α-Mg grains with β-Mg₁₇Al₁₂ and Al₂Ca compounds distributed along the grain boundaries. Friction stir welding produced much refined α-Mg grains accompanied by the dissolution of the eutectic β-Mg₁₇Al₁₂ phase, while Al₂Ca phase was dispersed homogeneously into the Mg matrix. An increase in rotation speed increased the α-Mg grain size but not significantly, while microstructure in the heat affected zone was almost not changed compared with the base material. The hardness tests showed uniform distributed and slightly increased harness in the stir zone. Results of transverse tensile tests indicated that the defect-free joints fractured at the base material, while longitudinal tensile tests showed that the strength of the defect-free welds was improved due to microstructural refinement and uniform distribution of intermetallic compounds.     

Microstructural evolution and mechanical properties of friction stir welded joint of Fe–Cr–Mn–Mo–N austenite stainless steel

2 mm thick Fe–18.4Cr–15.8Mn–2.1Mo–0.66N high nitrogen austenite stainless steel plate was successfully joined by friction stir welding (FSW) at 800 rpm and 100 mm/min. FSW did not result in the loss of nitrogen in the nugget zone. The arc-shaped band structure, consisting of a small amount of discontinuous ferrite aligning in the bands and fine austenite grains, was a prominent microstructure feature in the nugget zone. The discontinuous ferrite resulted from newly formed ferrite during welding and the remained ferrite, whereas the fine austenite grains were formed due to dynamic recrystallization of the initial austenite during FSW. The fine dynamically recrystallized grains in the nugget zone significantly increased the hardness compared to that of the base material. The strength of the joint was similar to that of the base material, with the joint failing in the base material zone.     

Microstructure feature of friction stir butt-welded ferritic ductile iron

This study conducted friction stir welding (FSW) by using the butt welding process to join ferritic ductile iron plates and investigated the variations of microsturcture in the joined region formed after welding. No defects appeared in the resulting experimental weld, which was formed using a 3-mm thick ductile iron plate and tungsten carbide alloy stir rod to conduct FSW at a rotational speed of 982 rpm and traveling speed of 72 mm/min. The welding region was composed of deformed graphite, martensite phase, and dynamically recrystallized ferrite structures. In the surface region and on the advancing side (AS), the graphite displayed a striped configuration and the ferritic matrix transformed into martensite. On the retreating side (RS), the graphite surrounded by martensite remained as individual granules and the matrix primarily comprised dynamically recrystallized ferrite. After welding, diffusion increased the carbon content of the austenite around the deformed graphite nodules, which transformed into martensite during the subsequent cooling process. A micro Vickers hardness test showed that the maximum hardness value of the martensite structures in the weld was approximately 800 HV. An analysis using an electron probe X-ray microanalyzer (EPMA) indicated that its carbon content was approximately 0.7–1.4%. The peak temperature on the RS, 8 mm from the center of the weld, measured 630 °C by the thermocouple. Overall, increased severity of plastic deformation and process temperature near the upper stir zone (SZ) resulted in distinct phase transformation. Furthermore, the degree of plastic deformation on the AS was significantly greater than that on the RS, and relatively complete graphite granules and the fine ferrite grains resulting from dynamic recrystallization were observed on the RS.     

The effect of tool rotational and traverse speed on friction stir weldability of AISI 430 ferritic stainless steels

In this study, the effects of tool rotational speed and traverse speed on welding of AISI 430 (X6Cr17, material number 1.4016) ferritic stainless steels by friction stir welding method are examined. Two specimens with dimension of 3 × 100 × 200 mm were joined in butt position. Tool rotational speeds were determined to be 560–1400 min⁻¹ and traverse speeds as 80–200 mm/min. During the studies, tool pressure force 3.5 kN and tool angle of 0° was kept constant. Hard metal carbide (WC-Co hard metal identified as K10) with equilateral triangle tip profile was used as the tool material. Determination of the tool advance speeds related to the tool rotation speeds giving the best-looking weld seals with acceptable values of mechanical properties was aimed.During welding of the specimens joined in butt position, the temperature change due to time and variation of the pressure force applied on welded specimens by the tool shoulder has been recorded. It has been observed that the best mechanical resistance values were obtained at tool rotational speed of 1120 min⁻¹ through five tool rotational speeds (560–1400). Also it has been observed that the best mechanical resistance values were obtained at traverse speed of 125 mm/min through five traverse speeds (80–200) with the constant tool pressure force of 3.5 kN and tool angle of 0°.     

Influence of tool geometry and rotational speed on mechanical properties and defect formation in friction stir lap welded 5456 aluminum alloy sheets

Friction stir welding of AA5456 aluminum alloy in lap joint configuration is with two different tempers, T321 and O, and different thicknesses, 5 mm and 2.5 mm was investigated. The influences of tool geometry and various rotational speeds on macrostructure, microstructure and joint strength are presented. Specifically, four different tool pin profiles (a conical thread pin, a cylindrical–conical thread pin, a stepped conical thread pin and Flared Triflute pin tool) and two rotational speeds, 600 and 800 rpm, were used. The results indicated that, tool geometry influences significantly material flow in the nugget zone and accordingly control the weld mechanical properties. Of particular interest is the stepped conical threaded pin, which is introduced for the first time in the present investigation. Scanning electron microscopy investigation of the fracture location of samples was carried out and the findings correlated with tool geometry features and their influences on material flow and tension test results. The optimum microstructure and mechanical properties were obtained for the joints produced with the stepped conical thread pin profile and rotational speed of 600 rpm. The characteristics of the nugget zone microstructure, hooking height, and fracture location of the weld joints were used as criteria to quantify the influence of processing conditions on joint performance and integrity. The results are interpreted in the framework of physical metallurgy properties and compared with published literature.     

Joint properties of friction welded 6061 aluminum alloy/YSZ–alumina composite at low rotational speed

In this study, a ceramic composite of alumina–yttria stabilized zirconia (YSZ) was friction welded to 6061 aluminum alloy. Alumina rods containing 25 wt.% YSZ were formed using slip casting and subsequently sintered at 1600 °C to form a solid body. The 6061 aluminum alloy sample was cut and polished, and then subjected to friction welding experiments. Both rods were 16 mm in diameter. The results of this study showed that the alumina–25 wt.% YSZ composite was able to be friction welded to 6061 aluminum alloy at a lower rotational speed of 630 rpm compared with high rotational speeds. The friction force was maintained at 5 KN for a frictional time of 30 s. Optical Microscopy (OM) and Field Emission Scanning Electron Microscope (FESEM) were used to analyze the microstructure of the products, particularly at the interface of the joints. The joints were also examined with EDX line and area (energy dispersive X-ray) in order to determine the phases formed during the low speed welding. The mechanical properties including bending strength and Vickers microhardness were measured. The experimental results indicated that the mechanical strength of friction welded alumina–25 wt.% YSZ composite/6061 aluminum alloy components were obviously affected by joining in the low rotational speed (630 rpm), having higher strength as compared to higher rotational speed.     

Friction stir welded T-joints optimization

The increasing use of aluminium alloys in transportation industry, such as railways, shipbuilding and aeronautics, promotes the development of more efficient and reliable welding processes. Friction stir welding (FSW) is a prominent solid-state joining technology that arose as a possible reliable welding solution. Optimized process parameters are not regularly used in previous studies found in the literature, in particular T-joints, which difficult the process industrial application. This study is focused on the optimization of friction stir welded T-joints using the Taguchi method. Mechanical tests of 27 different welded joints were carried out, and results were analysed using ANOVA, mean effect and response surface methodology (RSM). The tool rotational speed was verified to be the most influent factor in the joint mechanical properties, and is strongly dependent on the shoulder/probe diameters ratio. It was also shown that using 1000 rpm, 3.90 mm of probe depth and shoulder/probe diameters ratio of 2.5 (shoulder diameter of 15 mm) it may be achieved improved joint strength. For the optimized parameters it was verified that the welding speed does not have a significant influence. Equations to predict the joints mechanical properties were also derived through multiple regression.     

Effect of anisotropy on fatigue properties of 2198 Al–Li plates joined by friction stir welding

Al–Li alloys are characterized by a strong anisotropy in mechanical and microstructural properties with respect to the rolling direction. In the present paper, 4 mm sheets of 2198 Al–Li alloy were joined via friction stir welding (FSW) by employing a rotating speed of 1000 mm/min and a welding speed of 80 mm/min in parallel and orthogonal direction with respect to the rolling one. The joints mechanical properties were evaluated by means of tensile tests at room temperature. In addition, fatigue tests were performed by using a resonant electro-mechanical testing machine under constant amplitude control up to 250 Hz sinusoidal loading. The fatigue tests were conducted in axial control mode with R = σ_min/σ_max = 0.33, for all the welding and rotating speeds used in the present study.     

Failure analysis of tungsten based tool materials used in friction stir welding of high strength low alloy steels

A non-consumable tool is a vital requirement for friction stir welding (FSW) of high melting point alloys such as steel and titanium. In this investigation, an attempt was made to understand the pre-weld and post-weld microstructural characteristics of three tungsten based alloy FSW tools viz. 90%W, 95%W and 99%W. High strength low alloy (HSLA) steel plates of 5 mm thickness were welded using the above tools with a tool rotational speed of 600 rpm and welding speed of 30 mm/min. Microstructural characteristics of the FSW tools, before and after welding, were analyzed using optical microscopy (OM), scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD) techniques. From this investigation, it is found that the tool made of 99%W doped with 1% La₂O₃ exhibited microstructural stability due to absence of Fe–Co–Ni phase formation at elevated temperatures during FSW process.     

Microstructure and mechanical properties of friction stir welded 6082 AA in as welded and post weld heat treated conditions

Friction stir welding of 6082 AA-T651 was performed using three different combinations of feed rates (90, 140 and 224 mm/min) and tool rotational speeds (850, 1070 and 1350 rpm). Mechanical properties of the weldments were evaluated by hardness measurements on the transverse section and tensile testing, while microstructure evaluation was done by optical microscopy and electron back scattered diffraction (EBSD). Irrespective to welding parameters the dynamically recrystallized grains in the stir zone were measured to be in the range of 2–3 μm for different feeds rates and rotational speeds. A considerable loss in hardness in the stir zone and more severely in the thermo-mechanically affected zone was noted due to dissolution of β′ and β″ second phase particles. A post weld heat treatment (PWHT) of 175 °C for 5 and 12 h was given to the weldments for all welding conditions and the mechanical properties and microstructure were re-evaluated. The hardness and strength were partially recovered and this was attributed to the possible re-precipitation of the β″ precipitates. The grain size barely exhibited a change, whereas the texture displayed a significant diminish in the Goss orientation after PWHT.