Effect of Bondline Thickness on Mixed-Mode Debonding of Adhesive Joints to Electroprimed Steel Surfaces

Structural applications of adhesive bonding have been increasing in recent years due to improvements in the types of adhesives available and in improved knowledge of bonding procedures. Consequently, there exists a demand for techniques to assess adhesive joint strength, particularly along bondline interfaces where compliant adhesives contact more rigid metallic surfaces. The present study investigates the mixed-mode response of cracked-lap-shear (CLS) joints bonded with unprimed and electroprimed steel adherend surfaces. Three bondline thicknesses, representative of structural automotive joints, were evaluated for unprimed and primed bondlines. Experimental results for static load versus debond extension were input to finite element analyses for computing debond parameters (strain energy release rates). The debonds always initiated at a through-the-thickness location that had the greatest peel component of strain energy release rate. The total strain energy release rate values correlated well with trends in joint strength as a function of bondline thickness.     

Behaviour of Bi-adhesive Joints

The use of relatively low modulus adhesive at the ends of overlap in a bi-adhesive bondline of a bonded joint can reduce the stress concentration significantly and, therefore, potentially lead to higher strength of the joint. This study presents the two-dimensional and three-dimensional nonlinear (geometric and material) finite element analyses of adhesively bonded single lap joints having modulus-graded bondline under monotonic loading conditions. The adhesives were modelled as an elasto-plastic multi-linear material, while the substrates were regarded as both linear elastic and bi-linear elasto-plastic material. The computational simulations have been performed to investigate the bondline behaviour by studying the stress and strain distributions both at the mid-plane as well as at the interface of the bondline. It has been observed that the static strength is higher for joints with bi-adhesive bondlines compared to those with single adhesives in bondline. Higher joint strength has also been observed for optimum bi-adhesive bondline ratio through parametric studies. Effects of load level, and bondline thickness on stress distribution in the bi-adhesive bondline have also been studied. 3D analysis results reveal the existence of complex multi-axial stress/strain state at the ends of the overlap in the bondline which cannot be observed in 2D plane strain analysis. About 1/3rd of the width of the joint from the free edge in the width direction has 3D stress state, especially in the compliant adhesive of the bondline. Magnitudes of longitudinal and lateral stress/strain components are comparable to peel stress/strain components. It has also been analytically shown that the in-plane global stiffness of the joint remains unaffected by modulus gradation of the bondline adhesive.     

A shear-lag model for functionally graded adhesive anchors

A shear-lag model for stress transfer through an adhesive layer of variable stiffness joining an anchor rod and the concrete is presented and the effect of such an inhomogeneous bondline on interfacial shear stress distribution in comparison with that of a homogeneous bondline anchor subjected to monotonic axial tension is investigated. A closed-form solution is presented for arbitrary distribution of shear stiffness of the bondline considering both bonded and debonded embedded-end conditions of the anchor. Subsequently, the specific cases of linear and constant distribution of stiffness are discussed in detail, and it is shown how the general solution can be simplified for these examples. For validation, the distribution of shear stress along the bondline for the aforementioned cases is compared with that of equivalent axisymmetric Finite Element (FE) models and the results are found to be in good agreement. The theoretical solution developed can be readily used to evaluate the pull-out performance of post-installed adhesive anchors. Variable stiffness adhesive interfaces deserve an interest in practical applications either to estimate the effect of loss of interface stiffness, due to degradation of the adhesive material, or to engineer the interface with optimum distribution of stiffness so as to maximize the structural performance of bonded systems.     

Analysis of tubular adhesive joints with a functionally modulus graded bondline subjected to axial loads

The strength and lifetime of adhesively bonded joints can be significantly improved by reducing the stress concentration at the ends of overlap and distributing the stresses uniformly over the entire bondline. The ideal way of achieving this is by employing a modulus graded bondline adhesive. This study presents a theoretical framework for the stress analysis of adhesively bonded tubular lap joint based on a variational principle which minimizes the complementary energy of the bonded system. The joint consists of similar or dissimilar adherends and a functionally modulus graded bondline (FMGB) adhesive. The varying modulus of the adhesive along the bondlength is expressed by suitable functions which are smooth and continuous. The axisymmetric elastic analysis reveals that the peel and shear stress peaks in the FMGB are much smaller and the stress distribution is more uniform along its length than those of mono-modulus bondline (MMB) adhesive joints under the same axial tensile load. A parametric evaluation has been conducted by varying the material and geometric properties of the joint in order to study their effect on stress distribution in the bondline. Furthermore, the results suggest that the peel and shear strengths can be optimized by spatially controlling the modulus of the adhesive.     

Effect of Nanoclay Incorporation on the Impact Properties of Adhesively Bonded Composite Structures

During manufacturing or service conditions, adhesively bonded composites are often subjected to impact. This impact may result in a reduction in strength and structural integrity of engineering components that are composed of adhesively bonded composite structures. The investigation of the degradation of strength of structural joints is, therefore, of paramount importance for their successful performance. Impact resistance of bondline in adhesively joined composites can be altered by the addition of nanoclay in the adhesive during fabrication of adhesive joints. In this study, impact test was carried out on graphite–epoxy composite panels bonded with nanoclay adhesive at different impact energies using drop-weight impact test equipment. Adhesive joints were fabricated by adding nanoclay in volume fractions of 1, 2 and 5% in the adhesive bondline. For comparison, plain adhesive joints were fabricated without nanoclay incorporation in the bondline. Impact testing was performed on these joints at 5, 10 and 20 J, to study the effect of inclusion of nanoclay in the epoxy adhesive. In order to determine the flexural load bearing capacity and stiffness reduction after impact, a three-point bending test was conducted on unimpacted and impacted specimens. The results showed that there was an improvement in impact capacity, however there was a reduction in flexural strength due to nanoclay incorporation.     

A stress singularity approach to failure initiation in a bonded joint with varying bondline thickness

The stress singularity at the theoretical point of maximum stress in an uncracked single lap joint is analysed by a finite element method. By treating the interface corner of a bonded joint (between adherend and adhesive) as a perfectly bonded wedge and using a fracture mechanics method, considerable advantages over other continuum mechanics approaches for investigating the bondline thickness effect on joint strength are shown. This study has essentially two aims: (i) determination of the strength of the singularity by finite element analysis and comparison with the analytical prediction of Bogy for varying bondline thickness; and (ii) determination of stress intensity factors for varying bondline thickness. Good agreement is shown between the numerically-calculated strength of the singularity with the analytical value obtained from Bogy. The calculated stress intensity, after an initial decrease in the low bondline thickness range, is found to increase with increasing bondline thickness. This agrees well with the trends predicted by experiments.     

Design and analysis of functionally graded adhesively bonded double supported tee joint of laminated FRP composite plates under varied loading

The present research deals with three-dimensional nonlinear finite element analyses for a functionally graded adhesively bonded tee joint made of laminated fiber reinforced polymeric composites when the tee joint is subjected to different types of loadings. The out-of-plane stress components have been evaluated along the interfacial surfaces of bond line of the tee joint. Using the stress values, the failure indices are computed by using Tsai–Wu coupled stress failure criterion in order to predict the location of onset of failures within the interfacial surfaces. Accordingly, critical location is identified based on the magnitude of failure indices for varied load conditions. It has been observed that tee joint under bending load is vulnerable for early failure compared with that when the joint is subjected to tensile and compressive loading. The location of failure is found to be different in tee joint under bending load compared with tensile and compressive loadings. Further, efforts have been made to reduce out-of-plane stress concentration by implementing functionally graded adhesive (FGA) with appropriate smooth and continuous gradation function profile. Further, effects of material gradation function profile with varied modulus ratios on out-of-plane stresses and failure indices are observed along the different interfacial surfaces. Series of numerical simulation result significant reduction in peak values failure index. Based on the present research findings, the FGA is recommended for higher and efficient joint strength. Results also exhibit delayed failure onset and improved structural integrity in the tee joint structure with the use of FGA material.     

Stress Analysis of Adhesively Bonded Electroprimed Steel Lap Shear Joints

Structural applications for adhesive bonding have been increasing in recent years due to improvements in the types of adhesives available and in improved knowledge of bonding procedures. Consequently, there exists a demand for precise numerical modeling of adhesive joint behavior, particularly along bondline interfaces where low surface energy adhesives contact high surface energy metallic oxides. The purpose of the present study is to determine the effect of electrodeposited organic paint primer (ELPO) on the stress and strain distributions within an adhesively bonded single-lap-shear joint. Initial experimental studies have shown that bonding to ELPO-primed steel adherends has enhanced strength and durability characteristics compared to conventional bonds to unprimed steel surfaces. Recent studies based on finite element analysis of varied single-lap-shear joint moduli and thicknesses, and subsequent testing of joints with two different adhesive moduli, have indicated the mechanisms involved in this phenomenon. The presence of the ELPO-primer reduced peak peel and shear stresses and allowed for more uniform stress distribution throughout the joint.     

Stress Analysis of Adhesively Bonded Electroprimed Steel Lap Shear Joints

Structural applications for adhesive bonding have been increasing in recent years due to improvements in the types of adhesives available and in improved knowledge of bonding procedures. Consequently, there exists a demand for precise numerical modeling of adhesive joint behavior, particularly along bondline interfaces where low surface energy adhesives contact high surface energy metallic oxides. The purpose of the present study is to determine the effect of electrodeposited organic paint primer (ELPO) on the stress and strain distributions within an adhesively bonded single-lap-shear joint. Initial experimental studies have shown that bonding to ELPO-primed steel adherends has enhanced strength and durability characteristics compared to conventional bonds to unprimed steel surfaces. Recent studies based on finite element analysis of varied single-lap-shear joint moduli and thicknesses, and subsequent testing of joints with two different adhesive moduli, have indicated the mechanisms involved in this phenomenon. The presence of the ELPO-primer reduced peak peel and shear stresses and allowed for more uniform stress distribution throughout the joint.     

Stress analysis at the interface of metal-to-metal adhesively bonded joints subjected to 4-point bending: Finite element method

This paper presents a study of stress states in two-dimensional models of metal-to-metal adhesively bonded joints subjected to 4-point flexural loading using the finite element (FE) method. The FE simulations were carried out on adhesive bonded joints of high support span to specimen thickness ratio undergoing extensive plastic deformations. Two different adhesive types with eight different adhesive layer thicknesses each varying between 50 μm and μm were considered. The lower interfaces in the brittle adhesive were observed to be under a lower stress state because of the constraint exerted by a relatively stiff lower adherend. The ductile adhesive layers were under a lower state of stress as a result of the lower elastic modulus. It is concluded that the degree of plastic deformation in the adhesive is dictated by the adherend stiffness and the load transfer along the interface. The effect of load and support pins is noticeable at all adhesive thicknesses. High stress localisation exists in the vicinity of the load pins. The constraint exerted by the adherends dictates the deformation gradient through thickness of the adhesive layer. Adhesive joint behaviour as determined by the adhesive properties is investigated and also experimentally validated. Conclusions were drawn by correlating the adhesive and adherend stress states.     

Experimental and numerical analysis of single-lap joints for the automotive industry

Lap joints are used extensively in the manufacture of cars. In order to determine the effect of using a structural adhesive instead of spot-welding, a detailed series of tests and finite element analyses were conducted using a range of loadings. The adhesive was a toughened epoxy and the adherend was mild steel typical of that used in the manufacture of car bodyshells. The lap joints were tested in tension (which creates shear across the bondline), four-point loading (pure bending) and three-point loading (bending plus shear). Various parameters were investigated such as the overlap length, the bondline thickness and the spew fillet. The major finding is that three-point bending and tension loading are very similar in the way in which they affect the adhesive while the four-point bend test does not cause failure because the steel yields before the joint fails. A failure criterion has been proposed based on the tensile load and bending moment applied to the joint.     

复合材料粘接修理结构中胶层的应力分布

利用有限元方法,研究了复合材料粘接修理结构中胶层的弹性模量对其应力分布的影响。分析了胶层出现屈服和未屈服两种情况下,胶层的第1主应力,剥离应力和xy面剪切应力的分布随胶层弹性模量的变化情况。胶层的第1主应力随弹性模量的增大而增大,未屈服时,应力分布梯度也逐渐增大,大部分载荷集中到胶层的端部和破孔边缘。但是,出现屈服时,应力分布梯度则逐渐下降,大部分胶层承担相应的载荷。最大剥离应力出现在胶层的端部,并随胶层弹性模量的增大而增大。胶层两个粘接面的xy面剪切应力分布并不一样,但都随着胶层弹性模量的增大而增大。     

Interfacial Chemistry of an Aluminum-to-EPDM Rubber Bonding System

During recent assessment of aging in aluminum-to-rubber bonds on stored solid rocket motors, corrosion and minor insulator debonds were observed. A test was conducted to study the progressive effect of exposure to high humidity on the bondline; elevated temperature was used to accelerate the aging. In a parallel test, samples were held at elevated temperature in a dry atmosphere. The test results were compared with the analyses of corroded and noncorroded hardware samples. The predominant corrosion product detected at the bondlines was aluminum oxide/hydroxide. In general, there was a very good correlation between the Cl:Al atomic percent ratio calculated from X-ray photoelectron spectroscopy analysis of the ruptured bondline surfaces and the visual characterization of the extent of corrosion. The Cl:Al ratio, which represented the ratio of primer to corrosion product at the locus of failure, varied from 0.4 to 47. The implications for metal-to-rubber bond fabrication and storage are discussed.     

Analysis of mixed adhesive joints considering the compaction process

Incorporating a material properties variation along the bondlines has proved to be a useful method for improving adhesive joints performance. In this work, the potential of the technique is analysed for a single lap joint using the mixing adhesives approach. In order to include the compaction process effect in the structural analysis during the joint assembly, a computational fluid-dynamic model capable of integrating different resins along the bondline has been developed. Then, the results obtained from this model are mapped into a finite element model through an application developed for this purpose. Several parametric studies have been carried out comparing different configurations in terms of maximum load capacity of the joints. Finally, one of these joints configurations has been manufactured using a special device developed for assembling these mixed adhesive joints and tested. This banded configuration have shown both numerically and experimentally an ultimate load improvement of over 70%.     

Evaluation of FRP/wood adhesively bonded epoxy joints on environmental exposures

This article describes the evaluation of the durability of joints composed of wood adherends with a bonded layer of fibre-reinforced polymer (FRP) fabric. Carbon and glass fibres in an epoxy matrix were studied. The main purpose of FRP usage with timber in the construction industry is generally to improve the stiffness/strength of reinforced members without any influence on their service-life or any environmental impact. From the perspective of the timber reinforcement process, optimal dimensional stability during moisture changes in wood should be one of the most important criteria for such joints. Therefore, FRP/wood joints were evaluated with regard to the influence of real external environmental conditions on the bondline over a period of 40?months. During exposure to these conditions, specimen failures and defects were continuously visually evaluated. The decisive factor in this evaluation was bond integrity, verified by the tensile shear strength of the FRP/wood joint. After the experimental study, it was noted that the first 20?months have a significant effect on bondline failure occurrences, which involve decreases in tensile shear strength. In the next 20?months, the FRP/wood bondlines resist other severe hygrothermal stresses without significant strength decreases. An additional observed parameter was the percentage of wood failure in the bonded area of single lap joints, which characterises the mode of failure of the bonded joint. To determine the influence of ageing on adhesive due to ultraviolet radiation and varying temperature, infrared absorption spectroscopy analysis was performed to reveal changes in the macromolecular structure of the epoxy adhesive. Findings showed that UV radiation had a significant influence on the degradation of the adhesive structure.     

Modeling Concepts for Studying Ultrasonic Wave Interaction with Adhesive Bonds

Recent research has shown that such adhesive bondline defects as chemical segregation, variation in cure, gas entrapment or inadequate surface preparation are responsible for many adhesively bonded structural failures. Analytical models have been developed in this work that can be used to relate these “flaws” to the manner in which they affect the reflection of an ultrasonic pulse from such a bondline. The results of this study provide a substantial resource base for extended research through which ultrasonic inspection can become a reliable NDT technique for bond strength determination.     

Interfacial Chemistry of an Aluminum-to-EPDM Rubber Bonding System

During recent assessment of aging in aluminum-to-rubber bonds on stored solid rocket motors, corrosion and minor insulator debonds were observed. A test was conducted to study the progressive effect of exposure to high humidity on the bondline; elevated temperature was used to accelerate the aging. In a parallel test, samples were held at elevated temperature in a dry atmosphere. The test results were compared with the analyses of corroded and noncorroded hardware samples. The predominant corrosion product detected at the bondlines was aluminum oxide/hydroxide. In general, there was a very good correlation between the Cl:Al atomic percent ratio calculated from X-ray photoelectron spectroscopy analysis of the ruptured bondline surfaces and the visual characterization of the extent of corrosion. The Cl:Al ratio, which represented the ratio of primer to corrosion product at the locus of failure, varied from 0.4 to 47. The implications for metal-to-rubber bond fabrication and storage are discussed.     

Measurement of adhesive shear properties by short beam shear test based on higher order beam theory

This paper refers to the measurement of the shear properties of adhesive bonding by a new beam theory using the short beam shear (SBS) test configuration. A novel higher-order sandwich beam theory has been developed to analyze the adhesive bonded beam that consists of two adhered laminates and a single layer of adhesive in between. The closed form analytical solution for the SBS test model of the adhesively bonded beam is obtained in terms of deflection and stress distribution. The present theory has been used for calculating the adhesive shear modulus from the structural compliance. The initiation of stiffness degradation for the short beam shear test model was used as the critical load value for deriving the adhesive shear strength. A finite element model is built for validating the present model, and to evaluate its suitability for measuring adhesive shear properties. The present theory shows better accuracy for measuring the shear modulus than existing theories for both thin and thick adhesive layers. The measured strength values are more accurate than those obtained from the single lap joint shear test model. This theory can be used for adhesive materials with linear elastic deformation behavior.     

Advances in the proof test for certification of bonded repairs – Increasing the Technology Readiness Level

The availability of an efficient, cost-effective repair technology is an important maintenance requirement to restore structural integrity to metallic and composite airframe structures damaged in service. Generally repair involves attachment of a reinforcing structural element or patch to replace the damaged load path. Traditionally, the reinforcements are attached to the structure with rivets or bolts; however, attachment by adhesive bonding offers many structural and cosmetic advantages.However, bonded repairs of primary structure are very difficult to certify this is because available non-destructive procedures, such as ultrasonics or thermography are unable to detect weak adhesive bonds. In view of the limitation of non-destructive inspection an alternative approach is to directly apply stress to the actual repair bond region or to a very close simulation of the region.In this paper, further work is documented on a proof test of bonded repair coupons (BRCs) that are bonded to the parent structure at the same time as bonding of the repair patch. Therefore, the BRCs are close representation of the actual repair bond strength. To assess the bond strength, immediately after patch application and also possibly through the life of the repair, the BRCs are subject to a previously determined proof load in torsion.The aim of the study is to improve the Technical Readiness Level of the test when applied to various parent-structure/patch-repair systems, including carbon-epoxy/carbon-epoxy; aluminium/boron-epoxy and aluminium/aluminium. Improved BRC application methods were developed to increase the reliability and consistency of the results, and sensitivity to cure condition, surface treatment, contamination, and fatigue damage were evaluated.A detailed finite element (FE) study was undertaken to: a) simulate stresses in the BRC, adhesive and parent structure during the proof test, b) compare the stresses in the patch and BRC when the parent material is under stress and c) investigate the influence of BRC proximity to the patch tip when the parent material is under stress.A conclusion from the FE analysis and fatigue study was that a BRC with the appropriate ply configuration could represent the bondline stresses experienced at the patch tip, and hence could also be used to monitor fatigue damage.     

Metallic multi-material adhesive joint testing and modeling for vehicle lightweighting

While adhesive bonding has been shown to be a beneficial technique to join multi-material automotive bodies-in-white, quantitatively assessing the effect of adherend response on the ultimate strength of adhesively bonded joints is necessary for accurate joint design.In the current study, thin adherend single lap shear testing was carried out using three sheet metals used to replace mild steel when lightweighting automotive structures: hot stamped Usibor® 1500 AS ultra-high strength steel (UHSS), aluminum (AA5182), and magnesium (ZEK 100). Six combinations of single and multi-material samples were bonded with a one-part toughed structural epoxy adhesive and experimentally tested to measure the force, displacement across the bond line, and joint rotation during loading. Finite element models of each test were analyzed using LS-DYNA to quantitatively assess the effects of the mode mixity on ultimate joint failure. The adherends were modeled with shell elements and a cohesive zone model was implemented using bulk material properties for the adhesive to allow full three-dimensional analysis of the test, while still being computationally efficient.The UHSS-UHSS joint strength (27.2 MPa; SD 0.6 MPa) was significantly higher than all other material combinations, with joint strengths between 17.9 MPa (SD 0.9 MPa) and 23.9 MPa (SD 1.4 MPa). The models predicted the test response (average R2 of 0.86) including the bending deformation of the adherends, which led to mixed mode loading of the adhesive. The critical cohesive element in the UHSS-UHSS simulation predicted 85% Mode II loading at failure while the other material combinations predicted between 41% and 53% Mode II loading at failure, explaining the higher failure strength in the UHSS-UHSS joint.This study presents a computational method to predict adhesive joint response and failure in multi-material structures, and highlights the importance of the adherend bending stiffness and on joint rotation and ultimate joint strength.