可逆式冷轧对钢板织构及铁素体晶粒尺寸的影响

在实验室通过可逆式和连续式冷轧及退火模拟试验,研究了可逆式冷轧对DX51D(低碳铝镇静钢)和DX54D(无间隙原子钢)钢板织构及铁素体晶粒尺寸的影响。试验结果表明:(1)可逆式冷轧态试样α取向线{115}、{335}织构密度明显大于冷连轧试样,可逆式与连续式冷轧态试样γ取向线{111}织构密度无明显差别;(2)DX54D可逆轧制退火态试样γ取向线{111}织构密度大于冷连轧试样,其α取向线织构密度则与冷连轧试样相当;(3)DX51D可逆轧制退火态试样织构密度与冷连轧试样相当;(4)可逆轧制退火态试样的铁素体晶粒尺寸小于冷连轧试样。     

“ASP+罩式退火工艺”生产Ti-IF钢的织构演变

对济钢"ASP+罩式退火工艺"下生产的Ti-IF钢的热轧、冷轧及退火试样的织构演变进行分析。借助XRD测定并计算了热轧、退火及冷轧试样的取向分布函数和相关织构组分的体积分数。结果发现,济钢Ti-IF钢热轧板形成了较强的{111}面织构;在冷轧和退火后γ纤维织构显著增强;冷轧织构在罩式退火后,{111}<110>织构强度减弱,{111}<112>织构增强,{111}/{100}比值增加。     

可逆式冷轧对钢板织构及铁素体晶粒尺寸的影响

在实验室通过可逆式和连续式冷轧及退火模拟试验,研究了可逆式冷轧对DX51D（低碳铝镇静钢）和DX54D（无间隙原子钢）钢板织构及铁素体晶粒尺寸的影响。试验结果表明：（1）可逆式冷轧态试样α取向线{115}、{335}织构密度明显大于冷连轧试样,可逆式与连续式冷轧态试样7取向线{111}织构密度无明显差别;（2）DX54D可逆轧制退火态试样7取向线{111}织构密度大于冷连轧试样,其α取向线织构密度则与冷连轧试样相当;（3）DX51D可逆轧制退火态试样织构密度与冷连轧试样相当;（4）可逆轧制退火态试样的铁素体晶粒尺寸小于冷连轧试样。     

退火工艺及冷轧压下率对CSP工艺低碳冷轧板微观组织及织构演变规律的影响

以包钢CSP工艺生产的5.0 mm热轧板在实验室分别压下到1.75,1.25和0.75 mm冷硬板为原料,在实验室模拟了包钢罩式退火工艺,观察了不同压下率试样的显微组织.实验表明,通过观察罩式退火过程中试样的组织的变化,确定了再结晶开始温度在540℃左右,再结晶终了温度为700℃左右.并用X射线检测了试样在热轧和成品两个阶段的织构.结果表明,随着冷轧压下率的增大,再结晶进行的速度增:大,成品试样的织构密度增大,织构类型以{111}<110>和{111}<112>织构为主,但两者织构密度相差不大.     

冷轧压下率对连续退火Ti-IF钢组织和织构的影响

以工业生产的Ti-IF钢热轧板为研究材料,结合连续热镀锌线的工艺特点,采用实验室冷轧、盐浴退火方法和金相、X射线织构测试等分析手段,研究了冷轧压下率对组织和织构的影响规律。试验结果表明,随着冷轧压下率从60%提高到90%,冷轧态α取向线上的取向密度不断增强,而且主要形成了{223}110和{114}110织构,γ线上的{111}110和{111}112织构亦有所增强;退火后铁素体晶粒尺寸从9.0级细化到10.5级;试验钢退火后仍具有较强的{223}110和{114}110织构,且随着冷轧压下率的提高,{111}织构有增强的趋势。要获得强的{111}织构,冷轧压下率需在80%以上。     

可逆式冷轧对钢板织构及铁素体晶粒尺寸的影响

在实验室通过可逆式和连续式冷轧及退火模拟试验,研究了可逆式冷轧对DX51D（低碳铝镇静钢）和DX54D（无间隙原子钢）钢板织构及铁素体晶粒尺寸的影响。试验结果表明：①可逆式冷轧态试样α取向线{115}、{335}织构密度明显大于冷连轧试样,可逆式与连续式冷轧态试样γ取向线{111}织构密度无明显差别;②DX54D可逆轧制退火态试样γ取向线{111}织构密度大于冷连轧试样,其α取向线织构密度则与冷连轧试样相当;③DX51D可逆轧制退火态试样织构密度与冷连轧试样相当;④可逆轧制退火态试样的铁素体晶粒尺寸小于冷连轧试样。     

ASP工艺下Ti-IF钢微观织构演变规律研究

利用X射线衍射三维取向分布函数(ODF),对济钢"ASP+罩式退火工艺"下生产的Ti-IF钢的热轧、冷轧及退火、平整试样的织构演变规律进行研究。结果表明:济钢Ti-IF钢热轧板形成了较强的{111}面织构,在冷轧和退火后γ纤维织构强度显著增强;经罩式退火后,{111}110织构强度减弱,{111}112织构强度增强,V({111})/V({100})增大;经平整工序后高斯织构强度略有增强;随着碳含量的增加,Ti-IF钢在各生产工序的有利织构{111}减少,有害织构{100}增加,成形性能变差。     

热轧板初始组织对冷轧无取向硅钢织构演变的影响

研究了27.5 mm热轧板的初始组织(热轧态,850℃退火、950℃退火)对冷轧态和870℃退火的0.5mm冷轧无取向硅钢50W600薄板(/%:0.004C、0.33Si、0.38Mn、0.099P、0.007S、0.32Al)织构演变的影响。结果表明,经冷轧后冷轧板织构中{100}〈011〉和{112}〈110〉织构密度明显增大,末退火热轧板轧成的冷轧板织构密度较退火热轧板轧成的冷轧板强;经未退火热轧板冷轧成的薄板再结晶退火后的织构中主要为{100}〈011〉、{110}〈011〉和{111}〈112〉,退火热轧板冷轧成的薄板再结晶退火后的织构除{100}〈011〉和{110}〈011〉外还有密度较强的高斯织构。     

冷轧压下率对IF钢织构的影响

采用CSP工艺生产厚度为3.5 mm的IF热轧钢板,分析了冷轧压下率对冷轧织构、退火织构、各组分含量、{111}/{100}比值的影响。结果表明,采用71.4%的冷轧压下率生产的IF钢{111}织构占比最大,最有利于冲压性能的提高。     

B对含P高强度无间隙原子钢{111}面织构的影响

借助光学显微镜(OM)、X射线衍射(XRD)技术及电子背散射衍射(EBSD)技术,分析了2种含P高强度无间隙原子(IF)钢的热轧组织和热轧、冷轧及退火织构,结果表明:不含B与含B的高强IF钢热轧后,均得到多边形铁素体,但不含B热轧板晶粒尺寸较大。2种钢热轧板织构均比较散漫,γ纤维织构强度较弱,而不含B的IF钢经过80%大变形量冷轧以后,获得强的γ纤维织构,{111}面织构的体积分数达到41.41%,而含B的IF钢冷轧后{111}面织构的体积分数为33.83%。含B的IF钢冷轧后{112}110织构组分的体积分数比不含B的IF钢要高。2种实验钢在810℃退火60~180s以后,{111}面织构强度进一步增强,不含B的IF钢退火120s后{111}面织构的体积分数最大达到72.8%,而含B的IF钢退火120s后{111}面织构的体积分数最大达到66.6%。     

IF钢冷轧退火板中第二相粒子分析与研究

采用CSP工艺生产的IF冷轧钢板,分析了热轧卷取温度、冷轧压下率、退火温度及保温时间对退火板中第二相粒子的影响。结果表明,提高卷曲温度、增大冷轧压下率,提高退火温度、延长保温时间均促进退火板中第二相粒子Ti(CN)与FeTiP聚集并复合生长,有利于{111}织构的发展。     

Textures and Properties of Hot Rolled High Strength Ti-IF Steels

The texture evolution in a high strength Ti-IF steel during the processing of hot rolling, cold rolling, and annealing is studied. For comparison, both ferrite rolling and austenite rolling are employed. It is found that the texture type is the. same after ferrite rolling and austenite rolling, but the texture intensity is much higher in the ferrite rolled sample. Furthermore, texture characteristics at the surface are absolutely different from those at the mid sec tion in both ferrite rolled and austenite rolled samples, as well as under the cold rolled and annealed conditions. The shear texture { 110 } 〈001 〉 disappears and orientation rotates along { 110 } 〈001 〉→ { 554 } 〈 225 〉→ { 111 } 〈 112 〉→{111}〈110〉→{223}〈110〉 during cold rolling. Compared to the austenite rolled sample, the properties of the cold rolled and annealed sheet which is subjected to ferrite rolling are higher.     

退火工艺及压下率对超低碳CSP冷轧薄板织构的影响

在实验室用电阻炉模拟了包钢CSP工艺生产的以62.0%和71.4%压下率冷轧的1.9 mm和1.0 mmCD01钢(0.047%C)和SPCC钢(0.041%C)冷轧板的700℃罩式退火工艺。结果表明,冷轧板退火后主要以{111}〈110〉和{111}〈112〉织构为主;71.4%压下率冷轧板快速升温退火后{112}〈110〉取向密度最大,且大角度晶界所占比例较大,织构密度较大,织构主要集中在γ取向线附近。     

Evolution of Through-Thickness Texture in Ultra Purified 17%Cr Ferritic Stainless Steels

 Texture inhomogeneity usually takes place in ferritic stainless steels due to the lack of phase transformation and recrystallization during hot strip rolling, which can deteriorate the formability of final sheets. In order to work out the way of weakening texture inhomogeneity, conventional hot rolling and warm rolling processes have been carried out with an ultra purified ferritic stainless steel. The results showed that the evolution of through-thickness texture is closely dependent on rolling process, especially for the texture in the center layer. For both conventional and warm rolling processes, shear texture components were formed in the surface layers after hot rolling and annealing; sharp α-fiber and weak γ-fiber with the major component at {111}<110> were developed in both cold rolled sheet surfaces, leading to the formation of inhomogeneous γ-fiber dominated by {111}<112> after recrystallization annealing. In the center layer of conventional rolled and annealed bands, strong α-fiber and weak γ-fiber textures were formed; the cold rolled textures were comprised of sharp α-fiber and weak γ-fiber with the major component at {111}<110>, and inhomogeneous γ-fiber dominated by {111}<112> was formed after recrystallization annealing. By contrast, in the centre layer of warm rolled bands, the texture was comprised of weak α-fiber and sharp γ-fiber, and γ-fiber became the only component after annealing. The cold rolled texture displayed a sharp γ-fiber with the major component at {111}<112> and the intensity of γ-fiber close to that of α-fiber, resulting in the formation of a nearly homogeneous γ-fiber recrystallization texture in the center layer of the final sheet.     

Texture of Cold Rolled Strip of Fe-3Si Steel Produced by Thin Slab Casting and Rolling

 The hot rolled strip of Fe-3Si steel was experimentally produced by thin slab casting and rolling (TSCR) process in the laboratory. The texture evolution rule was investigated during hot rolling and cold rolling. The texture distribution of cold rolled strips with four kinds of cold rolling reduction schedules was observed through X-ray diffraction method, and the orientation density variation of 1/16 layer, 1/8 layer, 1/4 layer, and 1/2 layer in thickness was analyzed. The cold rolled texture of steel A with four kinds of cold rolling reduction schedules was mainly composed of α and γ fibers. Cold rolling reduction ratio of 70% was more beneficial for obtaining more γ fibers. The γ fiber texture orientation density of {111}<011> and {111}<1 12> was the largest on the 1/8 layer and 1/4 layer and the least on the 1/16 layer and 1/2 layer for steel B. The texture orientation density of {001}-{223}<110> in the α fibers for steel C was increased, but the texture orientation density of {332}-{110}<110> was low.     

CSP制无取向硅钢热轧、常化、冷轧织构的演变

运用EBSD和X射线衍射技术,研究了模拟CSP流程生产无取向硅钢在热轧-常化-冷轧过程中织构的演变。热轧板沿板厚方向应力场和温度场的差异导致由表至中织构锋锐度增高,织构类型存在明显变化,表层主织构为B类纤维织构,次表层为A类纤维织构,中心层为旋转立方织构{001}<110>。常化过程削弱了这种差异性,但中心层仍保留了一定强度的立方织构{001}<100>。冷轧板表层及中心层的主织构均为{112}<110>、{111}<112>,表层织构锋锐度较中心层的强。分析表明热轧、常化、冷轧织构的演变与基体初始织构、组织密切相关。表层、次表层热轧板织构经常化演化成散漫、分布较均匀的织构,中心层主要织构由{001}<-1-10>绕RD逆时针旋转45°演化至{001}<0-10>。冷轧后织构演变为以{223}<110>为主的B类织构和以{111}<112>为主的A类织构。     

冷轧压下率和再结晶退火温度对Ti-IF钢织构和成型性能的影响

采用背散射衍射技术(EBSD)研究了3.13 mm热轧板的冷轧压下量(65%~80%)和再结晶退火温度(660~780℃)对0.64~1.10 mm Ti-IF钢冷轧板(/%:0.02C、0.01Si、0.10Mn、0.013P、0.011S、0.064 Ti、0.028Al、0.002 0N)的织构和成型性能应变硬化指数(n)、塑性应变比(r)的影响。结果表明,Ti-IF钢冷轧板在冷轧压下率为75%时{111}织构含量最大,成型性能最佳;在740℃以下再结晶退火时材料{111}<110>织构含量高,高于740℃时材料{111}<112>织构含量高;在660~780℃再结晶退火随温度增高,材料{111}织构含量增加,成型性能提高。     

热轧钢板固溶元素析出对冷轧织构的影响

将热轧钢板在不同温度保温处理析出固溶元素后,在实验室四辊冷轧机上进行轧制,通过透射电镜观察（TEM）和三维取向分析（ODF）,研究了热轧钢板中固溶元素的析出对冷轧织构的影响。结果表明：热轧钢板经700℃和1000℃保温处理后,其冷轧织构仍保持了非{111}织构特征;热轧板中固溶元素析出为二相粒子,有利于冷轧织构中{111}组分的增强,进而具有抑制非{111}织构组分的作用。     

铁素体不锈钢铸轧薄带凝固组织对冷轧退火带晶粒簇的影响

 研究了Cr17铁素体不锈钢铸轧薄带凝固组织对其冷轧退火带晶粒簇、成形性和皱折特性的影响。利用电子背散射衍射技术对Cr17铁素体不锈钢铸轧薄带及相应的冷轧退火带进行了显微织构分析。结果表明：①Cr17铁素体不锈钢铸轧薄带冷轧退火带的晶粒簇依赖于初始铸轧薄带的凝固组织类型;②柱状晶组织的铸轧薄带具有显著的{001}∥ND晶体取向特征,而等轴晶组织的铸轧薄带晶体取向随机、分散;③等轴晶组织铸轧薄带比柱状晶组织铸轧薄带的冷轧退火带具有更少的{001}<110>晶粒簇和更多的{111}<112>、{111}<110>晶粒簇;④铸轧薄带的等轴晶组织比柱状晶组织有利于提高冷轧退火带的成形和抗皱性能。