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结晶器保护渣渣膜的研究 总被引:12,自引:3,他引:9
采用光学显微镜和扫描电镜对工业用结晶器保护渣渣膜进行了观测,结果表明,渣膜厚度约0.7~1mm基本结构有三层,两层结晶层,中间为玻璃层,某些情况下也呈玻璃与结晶交替排列的多层结构,厚度方向上Ca的分布略有差别,一般中心偏高,但同时也发现局部有CaS富集或微气孔现象。 相似文献
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采用表面分析技术,研究了铸造高硅不锈钢在98%H2SO4、0℃介质中,表面膜中元素分布及腐蚀行为与其元素所处价态的关系。试验结果表明,高硅不锈钢在浓硫酸中,表面膜因抗蚀作用不同可分为三层,表面层、中间层和过渡层。表面层及中间层都具有抗腐蚀能力,可阻挡介质对不锈钢基体的浸蚀,中间层中富集硅和铬,主要以SiO2和Cr2O3形式存在。而镍富集在过渡层中,可进一步提高膜的稳定性。 相似文献
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高温退火低保温期,采用惰性气体作保护气体能改善被膜质量。惰性气体Ar与H2、N2相比黏度高, Ar气难于侵入钢卷的各层间挤压出水分子,水分子就在钢板层间保持下来,将会进一步促进被膜的生成。之后导入氢气,促进了退火隔离剂MgO的表面活化性,由于钢板层间是湿氢保护气氛,钢板表面的副氧化层中、难于被还原的Fe2SiO4,将与MgO发生反应,生成Fe2 xMgxSiO4,又继续形成完善的Mg2SiO4镁橄榄石被膜,在这种条件下所生成的被膜将吸收隔离涂层中的Ti,增强了被膜的强度。 相似文献
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硫化廿二酸钼的合成及其摩擦化学研究 总被引:4,自引:2,他引:2
通过低温硫化工艺和复分解反应合成了硫化廿二酸钼,并在四球机上考察了硫化廿二酸钼的摩擦学特性。实验结果发现硫化廿二酸钼的抗磨极压性超过了目前国内外传统的抗磨极压剂硫化异丁烯(Anglamol33),二烷基二硫代磷酸锌(ZDTP),以400#中性油作基础油,四球磨斑直径d392N30min依次为0.56mm、0.62mm和0.82mm,最大无卡咬负荷PB值相应为1176N、1127N和980N,摩擦系数f值比基础油下降了40%。用俄歇能谱(AES)分析了摩擦表面膜,发现在表面深层为50处富含硫和钼,并在该处两者都达到了峰值。据此认为硫化廿二酸钼的减摩、抗摩和极压作用机理是在摩擦表面生成了FeS(或FeS2)和层状结构MoS2的复合无机膜,由于复合膜和MoS2层的扩散渗硫、渗钼作用,增强了复合无机膜的强度,同时由于复合无机膜和MoS2层在摩擦时的相对滑移作用,使硫化廿二酸钼具有减摩、抗摩和极压功能。此外,还提出了润滑膜的结构模型。 相似文献
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对不同成分的含铬铸钢进行了与电化学试验,利用恒电位仪、扫描电镜和XPS手段,研究了试验材料在混合盐(0.1%NaCl+0.5%N2SO4+H2SO4,pH=6)中的抗蚀行为,试验表明铬含量对铸钢耐蚀性有显著的影响。当含理达到8%以上,铸钢表面形成了氧化膜。氧化膜富氧、富铬而贫铁,膜中的Cr/Fe比远大于基体中的值;膜的表层含有铬与铁的氢氧化物和氧化物。这种氧化对含铬约8%的铸钢起到了保护作用。 相似文献
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用乳状液膜从硫酸铵型浸出液中浓缩稀土 总被引:1,自引:0,他引:1
张瑞华 《稀有金属与硬质合金》1996,(4):12-16
在作者所做的"用乳状液膜从氯化钠型浸出液中浓缩稀土"的工作基础上,利用所获得的液膜体系和较佳工艺条件,继续进行了料液类型[即NaCl型和(NH4)2SO4型浸出液的比较实验]、NaAc用量、膜相中有无石蜡、膜回用等条件实验,获得了从(NH4)2SO4型浸出液中浓缩稀土的适用液膜体系N205-P507-煤油-HCl乳状液膜浓缩稀土的浓度达102g/L,稀土提取率达93%。 相似文献
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TA Solokhina LS Shevchenko IuV Se?ku EG Rytik LV Besedina TS Veshchugina 《Canadian Metallurgical Quarterly》1998,98(6):42-46
Usage of quality of life of psychiatric patients' relatives as the parameter of estimation of the quality of psychiatric care is considered. By means of standard questionnaire elaborated by the authors as well as by means of both individual and group conversations the quality of life was analyzed in 40 relatives which lived together with psychiatric patients. Different spheres of their life and difficulties (financial, social-psychologic, production) were examined in families with such patients. The defects of psychiatric care that had direct influence on the quality of life of the psychiatric patients' relatives are outlined. 相似文献
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The effect of 20 different antibiotics on chemotaxis by human neutrophils was studied. Human leukocytes incubated with chloramphenicol, rifampin, sodium fusidate, and tetracyclines in vitro showed markedly depressed migration. The mechanisms by which these antibiotics affect leukotaxis are discussed. 相似文献
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显微维氏硬度测量不确定度评定 总被引:1,自引:0,他引:1
对显微维氏硬度测量不确定度进行评定,建立了不确定度计算的数学模型,确定了影响实验结果的各项因素,计算出了各因素的标准不确定度,得出结果的扩展不确定度,并给出最终测量结果的表达式。 相似文献
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G Steinbach 《Canadian Metallurgical Quarterly》1997,110(7-8):247-250
Totally negative results of epidemiological investigation of random samples do not prove the absence of the infection as the pathogen may be restricted to only a few animals in the herd for a long time. The statement "absence of infection" is critical for such situations. The question is raised, whether the statement "absence of infection" should be generally avoided. Classification of herds and flocks according to the prevalence of the pathogen would be more valid for the implementation of control measures. 相似文献
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Some theories of personality hold that an individual's perception of others is influenced by his own personality characteristics; more specifically, that a trait of low social value will be projected more into others, and that insight into the possession of these characteristics reduces this distortion. These 2 hypotheses were tested by having a group of college students rate each other (including themselves) on degree of friendliness or hostility. Agreement with group rating about self yielded the insight score. In general, the hypotheses were supported; the "friendly" Ss were most accurate in their perception of others, and insight was positively associated with accurate perception. From Psyc Abstracts 36:04:4HL16M. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
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The rates of infection of two methods of external ventricular drainage in use at Atkinson Morley's Hospital--namely, (a) percutaneous drainage with Rickham reservoirs and (b) tunnelled ventriculostomies--were compared in this retrospective review. Percutaneous drainage of CSF with Rickham reservoirs was associated with a 27% rate of infection as identified by positive microbiological cultures; tunnelled ventriculostomy catheters had a 10% infection rate. The difference in the infection rate between the two methods was statistically significant (P < 0.015). Other variables examined, including the age and sex of the patients and the reasons for ventricular drainage, were not associated with an increased rate of infection. Most infections from either method were caused by a coagulase negative staphylococcus. The average duration of ventricular drainage before identification of positive cultures was 5.7 days for Rickham reservoirs and 6.0 days for ventriculostomies. 相似文献