L360管线钢热轧过程静态再结晶行为的研究

奥氏体再结晶行为是影响热轧钢带组织和力学性能的1个主要因素。在热模拟试验的基础上,采用应力松弛法和显微组织观察法,对含Nb和Ti的L360管线钢热轧过程奥氏体静态再结晶行为进行了研究,分析了应变、变形温度、应变速率、原始奥氏体晶粒尺寸对奥氏体静态再结晶的影响。利用线性回归分析,计算出试验钢静态再结晶激活能为203kJ;同时通过回归,得出试验钢热轧过程静态再结晶动力学方程。     

终轧温度对高氮奥氏体钢组织和力学性能的影响

通过加压冶炼、控制轧制方式获得氮质量分数为0.59%的Mn18Cr18N钢板,研究了终轧温度对高氮奥氏体钢组织和力学性能的影响。结果表明,在再结晶区轧制并且终轧温度为970 ℃的钢板,组织为奥氏体等轴晶和部分孪晶,强度较低,塑性、冲击韧性较好;终轧温度为910 ℃的钢板,大部分组织为变形奥氏体晶粒,有少量再结晶晶粒,随着终轧温度降低钢板强度升高,塑性和冲击韧性降低;在未再结晶区轧制并且终轧温度为780 ℃的钢板,组织为变形严重的奥氏体晶粒,强度最高,塑性、韧性最低。所有试验钢有晶界析出的Cr₂N相,降低终轧温度和减缓轧后冷却速度,会增加Cr₂N相的析出。     

薄板坯连铸连轧流程钛微合金钢控制轧制技术

 重点阐述了薄板坯连铸连轧流程钛微合金钢的控制轧制模式及其机理。基于应力松弛试验和双道次压缩热模拟试验,研究分析了薄板坯连铸连轧钛微合金钢的奥氏体再结晶动力学。研究结果表明,轧前铸态粗大奥氏体组织经F1高温大压下后可实现完全静态再结晶;铸坯中固析TiN粒子可以有效阻止奥氏体再结晶晶粒的长大,实现再结晶区控轧。固溶钛的溶质拖曳作用以及形变诱导析出的TiC粒子对奥氏体再结晶具有抑制作用,可以阻止奥氏体再结晶的发生,实现未再结晶区控轧。     

Study on dynamic recrystallization behavior of hot rolled TRIP steel produced by CSP process

The dynamic recrystallization behavior of hot rolled TRIP steel produced by CSP process was studied by means of Gleeble-3500 thermal simulation testing machine in the temperature range of 950-1150℃ with the strain rate of 0.1-10s-1 and the strain of 65%. And the effect of initial austenite grain size on the dynamic recrystallization behavior of TRIP steel was explored. The results show that the finer initial austenite grain size, the higher deformation temperature and the lower strain rate, the more positive austenite dynamic recrystallization of TRIP steel. Moreover, it is found that when the coarse grained samples (initial austenite grain size is 767.54μm) deform in the range of 1050℃ to 1150℃, the austenite dynamic recrystallization will take place, and the dynamic recrystallization activation energy of TRIP steel is deduced as 361539.17J/mol. The Zener-Hollomon parameter equation as a function of strain rate and temperature is determined. And the model of critical strain for dynamic recrystallization, the flow stress model of austenite at high temperature and the grain size model for dynamic recrystallization are also established. The calculation results are coincided well with the experimental results.     

Recrystallization Behavior Design for Controlling Grain Size in Strip Rolling Process

To promote effectively dynamic recrystallization and obtain a homogeneous distribution of ultrafine grain size in strip finish rolling process,the behavior of static and dynamic recrystallization must be appropriately designed to provide an ultrafine austenite microstructure without mixed grain size.The design of rolling schedule was analyzed based on the control of the recrystallization behavior to achieve ultrafine grain size in the strip rolling process of niobium microalloyed steel.The experimental simulations were presented to validate the twice dynamic recrystallization design to achieve ultrafine grain size control.     

Ti对低碳Mn-V钢奥氏体动态再结晶的影响

采用Gleeble热模拟试验机和透射电镜、扫描电镜及定量金相等分析技术,就钛对低碳Mn-V钢奥氏体晶粒长大行为、奥氏体动态再结晶行为等进行了研究.结果表明,含钛钢中形成稳定的碳氮化钛,对阻止再加热奥氏体晶粒长大有利.含钛钢变形抗力比不含钛钢要高,其动态再结晶开始的临界变形量比不加钛钢的小,易于发生再结晶,且含钛钢的再结晶晶粒尺寸相对较细,再结晶晶粒长大速度也更慢.     

Austenite Recrystallization and Controlled Rolling of Low Carbon Steels

The dynamic recrystallization and static recrystallization in a low carbon steel were investigated through single-pass and double-pass experiments. The results indicate that as the deformation temperature increases and the strain rate decreases, the shape of the stress-strain curve is changed from dynamic recovery shape to dynamic recrystallization shape. The austenite could not recrystallize within a few seconds after deformation at temperature below 900 ℃. According to the change in microstructure during deformation, the controlled rolling of low carbon steel can be divided into four stages： dynamic recrystallization, dynamic recovery, strain-induced ferrite transformation, and rolling in two-phase region. According to the microstructure after deformation, the controlled rolling of low carbon steel can be divided into five regions： non-recrystallized austenite, partly-recrystallized austenite, fully-recrystallized austenite, austenite to ferrite transformation, and dual phase.     

CSP热轧TRIP钢动态再结晶行为研究

摘要：采用Gleeble-3500热模拟试验机,在温度为950~1150℃、应变速率为0.1~10s-1和变形量为65%的条件下研究了CSP热轧TRIP钢的动态再结晶行为,探讨了初始奥氏体晶粒尺寸对TRIP钢动态再结晶行为的影响。研究结果表明,初始奥氏体晶粒尺寸越小,变形温度越高,应变速率越慢时,TRIP钢中奥氏体越易发生动态再结晶。其中,粗晶试样（初始奥氏体晶粒尺寸为767.54μm）在1050~1150℃内变形时,将发生动态再结晶。其热变形激活能为361539.17J/mol,确定了Zener-Holloman参数与应变速率和温度的关系式,建立了动态再结晶临界应变模型、高温奥氏体流动应力模型和动态再结晶晶粒尺寸模型,理论模拟结果与试验结果吻合较好。     

生产工艺对320MPa高强度船板钢低温冲击韧性的影响

采用不同的生产工艺制度,E32级船板钢在工业试制过程中的-40℃纵向冲击功波动较大,对此现象的研究表明,在采用两阶段轧制时,由于中间坯的厚度较大,对未再结晶区的变形温度产生影响,易发生在部分再结晶区轧制时,钢板出现混晶,从而造成钢板低温冲击值较低。     

贝氏体非调质紧固件用钢静态再结晶行为分析

为分析贝氏体非调质紧固件用钢的静态再结晶行为,在Gleeble 3500热模拟试验机上进行了双道次压缩试验,并计算了静态再结晶软化率。研究表明,所研究钢种的奥氏体在1 050℃以上易于发生静态再结晶,在850℃以下静态再结晶发生困难;所确定的再结晶模型1可用于预测所研究钢种的静态再结晶的发生情况;利用道次间的静态再结晶细化奥氏体,适宜的轧制温度应控制在950~1 050℃,热机轧制温度应控制在850℃左右。     

微铌处理550MPa热轧带钢的工艺研究

采用Gleeble3500热模拟试验机,研究了含铌Q345钢奥氏体静态再结晶行为、铌的碳氮化物在奥氏体和铁素体中的析出行为等实验,铌在钢中的强化作用机理。根据上述结论,邯钢2250热轧厂生产了以碳、锰为主要成分,并加入微量铌元素,将原热轧带钢Q345的屈服强度由345 MPa提高到550M Pa。对生产的微铌处理550 M Pa钢的组织和力学性能作了检验,在细晶强化、沉淀强化和相变强化等复合强化的综合作用下,热轧带钢屈服强度均达到550 MPa以上,塑性良好。     

锆含量对高强韧Ti-Zr微合金化钢奥氏体组织的影响

为了满足各行业对钢铁材料提出的更高强度、更好韧性的要求,在钢中加入适量的微合金化元素并结合合理的控扎控冷工艺,有利于在高温轧制阶段获得细小均匀的奥氏体再结晶晶粒,这是提高钢材强度及韧性的有效途径之一。通过Gleeble-3800型热模拟试验机,对两种不同锆含量的低碳微合金Ti-Zr钢进行多道次压缩变形试验,模拟实际轧制情况,研究试验钢在不同锆含量和不同变形方式(等温变形和变温变形)下的热变形行为,并结合组织观察分析讨论了锆含量和变形条件对试验钢奥氏体组织细化行为和析出行为的影响。结果表明,变形温度的升高可以降低高锆钢各道次的流变应力。变温变形条件下,锆含量的升高会提高试验钢各道次的流变应力;奥氏体再结晶晶粒会随着锆含量的升高和变形温度的降低而发生细化,采用变温变形方式比等温变形方式更有利于得到细小的奥氏体晶粒,高锆钢在1 050℃→1 25℃→1 000℃变温变形后得到了最小的奥氏体平均晶粒尺寸(为8.2μm);锆含量升高会提高试验钢中析出相的数量,变形方式对析出相数量的影响不大,变形温度的升高会使析出相发生粗化。锆含量增加所导致的形变诱导析出相的增多,以及变温变形过程中温度的降低,起...     

低合金厚板的减量化轧制

 通过挖掘设备潜力,采用奥氏体再结晶区直接轧制+轧后快速冷却工艺在某宽厚板生产线上成功试制了60～85 mm厚Q345系列C Mn低成本厚板,Z向性能稳定达到Z35标准要求。试验结果表明,用该工艺生产低合金厚板可缩短2 min轧制时间,提高了机时产量,促进钢铁工业的可持续发展。     

低成本90mm Q345E特厚板的生产

为了降低强韧性特厚板的生产成本,在某公司通过试验,以碳、锰成分为基本成分,采用300mm断面钢坯,通过执行较为严格的TMCP工艺,使奥氏体再结晶区的轧制温度控制在1100～1050℃,未再结晶区轧制温度在770～800℃,并严格控制轧制速度和道次压下量,同时利用ACC层流冷却避? 糠衷俳峋⑼ü?.6℃/s的冷却速度将轧后钢板冷却在620℃温度范围,最终生产出厚度为90mm、性能符合Q345E级别要求的特厚板,并满足符合Z25的厚度方向性能要求。     

Grain Refinement of Nb Steels by Control of Recrystallization during Hot Rolling

Control rolling of Nb-bearing steels is employed to produce the uniform fine-grained product needed to meet the most stringent strength and toughness specifications. To produce such structures consistently requires a thorough understanding of the effects of compositional and process variables on austenite grain refinement at every stage of the hot rolling process. These effects were examined by means of a laboratory simulation of plate rolling. It was found that limiting the reheated grain size to about 100 μm (by lowering the reheat temperature or by adding Ti to the steel) is essential to assure complete recrystallization and refinement of the initial grain structure without an excessive amount of reduction at high temperatures. Because of the slow cooling rate at the slab center, this initial breakdown stage of rolling must be followed by a hold to allow the slab to cool to the lowest temperature at which recrystallization during rolling will be complete. This procedure will assure that the second roughing stage will produce the finest and most uniform recrystallized structure possible. This structure transforms to a very uniform ferrite-pearlite with a grain size of 10 to 15 μm. If, however, the fine recrystallized austenite is further rolled below the recrystallization temperature (control rolled) it will produce flattened austenite grains that transform to ultra-fine ferrite 4 to 6 μm in diameter. The uniformity of the final structure depends critically on the state of the austenite prior to grain flattening. The austenite must be completely recrystallized, since partially recrystallized regions produce duplex ferrite. Two attempts to change the control-rolling temperature range by modifying composition were unsuccessful. Increasing the Nb content from 0.05 to 0.10 to promote higher-temperature precipitation and boundary pinning did not raise the temperature at which grain flattening began. The addition of Ti to a Nb steel to remove soluble nitrogen and thereby prevent formation of NbCN in favor of the lower-temperature NbC did not promote recrystallization to lower temperatures.     

高韧性管线钢工艺优化研究

研究了高韧性管线用钢热变形过程中的变形奥氏体再结晶规律，轧后冷却过程中的相变规律，优化出实验用钢的合理控轧控冷工艺，采用该工艺，宝钢生产的Ｘ６０￣Ｘ６５级管线钢板的冲击韧性值提高了１倍以上，其综合力学性能达到甚至超过日本进口钢板的实物水平。     

高碳钢线材轧制工艺参数对晶粒尺寸的影响

结合高碳钢线材的生产实际，利用物理冶金理论和实验模型，对奥氏体的变形-再结晶过程进行模拟计算，计算出各道次的奥氏体晶粒尺寸并分析变化规律。模拟计算结果表明，亚动态再结晶在粗轧和中轧阶段起主要作用，在轧制后半程，静态再结晶起主要作用。分析改变生产工艺参数对晶粒尺寸的影响以及晶粒细化的途径。为进一步的相变、性能预测提供指导依据。     

Static recrystallization behavior of 25CrMo4 mirror plate steel during two-pass hot deformation

The static recrystallization behavior of 25 CrMo4 mirror plate steel has been determined by hot compression testing on a Gleeble 1500 thermal mechanical simulation tester. Compression tests were performed using double hit schedules at temperatures of 950-1 150 °C,strain rates of 0. 01- 0. 5 s~(-1),and recrystallization time of 1-100 s. Results show that the kinetics of static recrystallization and the microstructural evolution were greatly influenced by the deformation parameters( deformation temperature,strain rate and pre-strain) and the initial austenite grain size. Based on the experimental results,the kinetics model of static recrystallization has been generated and the comparison between the experimental results and the predicted results has been carried out. It is shown that the predicted results were in good agreement with the experimental results.     

直接轧制工艺对中厚板组织与性能的影响

 连铸坯直接轧制技术作为一种变革性的绿色钢铁生产流程,目前主要用于超薄带和线棒材生产,近年来国内外逐步开始了中厚板直接轧制工艺的探索性工作。直接轧制工艺与常规热轧工艺相比,具有不同的温度履历和物理冶金学过程。选取Nb-Ti微合金钢为研究对象,从产品组织与性能的角度,探讨中厚板直接轧制工艺的可行性。采用炼钢-连铸-轧制中试试验,对比研究了直接轧制工艺及常规热轧工艺下中厚板产品的组织和性能,并基于动态再结晶模型,探讨了直接轧制工艺下试验钢的组织细化机制。研究结果表明,直接轧制工艺下,虽然连铸坯轧前未经过γ-α-γ相变过程,仍保留铸态粗大的奥氏体晶粒,但轧制过程中较大的芯表温差有利于变形向芯部渗透,芯部再结晶进行得更加充分,可以用形变再结晶机制代替常规热轧工艺的相变机制细化成品芯部组织,获得与常规热轧工艺相近甚至更优的显微组织与力学性能。