多向锻造对超高强度不锈钢组织及力学性能的影响

通过光学显微镜(OM)、扫描电子显微镜(SEM)、背散射电子衍射(EBSD)、透射电子显微镜(TEM)对多向锻造淬火后的马氏体超高强度不锈钢的显微组织进行定量表征,分析多向锻造对试验钢显微组织的影响;同时进行力学性能测试,分析多向锻造对试验钢力学性能的影响,讨论不同强化机制对试验钢强度的贡献。结果表明,随着锻造道次的增加,试验钢的原奥氏体晶粒、马氏体板条束(Packet)、板条块(Block)尺寸均逐渐细化,5个道次后原奥氏体晶粒从226.1细化到3.2 μm,Packet尺寸从106.1细化到2.9 μm,Block尺寸从2.3细化到1.5 μm;试验钢的力学性能显著提升,屈服强度由1 030增加至1 175 MPa,冲击功吸收功由140增加至194 J,伸长率也从9.3%增加到了11.6%;试验钢强度的提升主要归功于位错强化与细晶强化并以位错强化为主,且位错强化与细晶强化并不遵从线性叠加强化机制,而更接近均方根叠加机制。     

淬火工艺对马氏体高强钢组织和性能的影响

摘要：采用拉伸、冲击、金相、电子背散射衍射、透射电镜、X射线衍射等试验手段,研究了在线直接淬火+回火（DQT）与离线再加热淬火+回火（RQT）工艺对马氏体高强钢组织性能的影响。结果表明,2种试验钢组织均为板条马氏体,RQT试验钢原奥氏体晶粒及板条束呈等轴状,板条块较短,板条较宽,DQT试验钢原奥氏体晶粒呈扁平状,板条束贯穿整个晶粒,板条块呈细长状,板条宽度较小;位错强化是DQT试验钢强度较RQT高的主要原因;板条束为控制DQT和RQT试验钢韧性的最小单元;DQT试验钢大角晶界比例较低,其具有较大的马氏体板条束尺寸以及更高的位错密度,断裂应力较低,低温韧性较差。     

细晶强化和位错强化对中锰马氏体钢的强化作用

研究了碳和锰含量对淬火中锰马氏体钢的位错密度、残余奥氏体含量、晶粒尺寸等组织结构以及室温力学性能的影响。借助于SEM、EBSD、TEM和XRD表征了材料的微观组织,探讨了马氏体钢的强化机制。结果表明:随着碳含量增加,淬火中锰钢的位错密度和残余奥氏体体积分数逐渐增加,板条束和板条块尺寸逐渐细化,大角晶界百分数逐渐增加,强度逐渐升高;增加锰含量能够提高马氏体钢的位错密度和抗拉强度。分析认为,位错强化和细晶强化是淬火中锰马氏体钢的主要强化机制。马氏体板条尺寸是马氏体抗拉强度的结构控制单元,而原奥氏体晶粒尺寸则是马氏体屈服强度的结构控制单元。     

C-Si-Mn-B系贝氏体钢的强度及强化机制

测定并分析了中碳和中低碳C-Si-Mn-B系贝氏体钢的抗拉强度及强化机制，结果表明，该钢具有较高的强度和良好的塑性，减小贝氏体铁素体板条宽度和提高板条内的位错密度对贝氏体的强化有较大贡献，在贝氏体/马氏体复相组织的强化机制中，应考虑下贝氏体板条对原奥氏体晶粒的分割细化效应以及马氏体对贝氏体板条变形的约束作用。由强化机制计算的强度值与实测值有较好的一致性。     

铈对低合金超高强钢马氏体相变行为的影响

 为了研究稀土元素铈对低合金超高强钢马氏体相变组织及动力学过程的影响,制备了不含铈与铈质量分数为0.079 2%的两组对比试验用钢。采用OM、SEM和TEM分析了试验用钢的显微组织,并利用DIL805A淬火膨胀仪绘制了马氏体相变动力学曲线。研究结果表明,铈的添加细化了原奥氏体晶粒,平均晶粒尺寸由7.63减小到6.42 μm;细小的奥氏体晶粒使马氏体板条宽度得到细化,平均宽度由250减少到211 nm。此外,对于马氏体相变动力学,铈的添加使马氏体相变开始温度(M_s)由391降低到380 ℃;在马氏体相变前中期,铈阻碍了马氏体转变,在马氏体相变后期,铈促进了马氏体转变。     

30CrNi5MoV钢中铬对组织机制的作用及影响

对不同含铬量的30Cr Ni5Mo V钢的奥氏体晶粒度、马氏体束的大小及板条宽度进行研究并探讨这些参数对该钢σp50的影响,讨论了30Cr Ni5Mo V钢中铬对其组织机制的作用和影响。     

舰艇用钢的新发展

ＨＳＬＡ系列钢是舰艇用钢。鞍钢钢铁研究所对ＨＳＬＡ１００钢的生产，金相组织和性能进行了试验研究和初步探讨，认为强化机制应为板条马氏体束，针状铁素体束及其宽度的细化和原始奥氏体晶粒细化。同时，也证明了这种钢在我国现有条件下进行生产是可行的。     

高强度马氏体时效不锈钢的晶粒细化及其力学性能的研究

研究了一种高强度马氏体时效不锈钢逆转变奥氏体再结晶规律、细化晶粒工艺及细晶组织对力学性能的影响.研究表明,通过循环相变a'(→)γ可得到7 um的等轴晶粒,新生晶粒内的板条马氏体块又重新被分割而成为若干个亚晶粒,同时部分单一的马氏体板条束又被夹角略大于60°方向上的若干个小马氏体板条束所分割,从而进一步细化了马氏体组织;与传统热处理工艺1050℃×1h相比,在同样时效处理规程下进行时效处理,钢的屈服强度提高了130 MPa,A、Z分别提高了7.5%、11%,循环相变细化晶粒是同时提高该钢的强度和韧塑性的有效手段.     

高强韧及延伸性能耐磨钢NM600关键技术研发与应用

采用Gleeble-3500 热模拟试验机对超高强耐磨钢NM600 进行试验,研究第1 轧程控轧压下率与原始奥氏体晶粒尺寸的关系.结果表明:当单道次压下率范围在15％～25％时,板坯表面和心部同时发生充分的动态再结晶,得到细小原始奥氏体晶粒.根据耐磨钢NM600 奥氏体连续冷却转变曲线,设定轧后空冷驰豫开始温度Ac3+(30～50)℃,空冷弛豫终止温度为Ac3-(30～50)℃,并通过在线控制冷却,以中等冷却速度冷却至640～660℃,调控淬火前的形变奥氏体晶粒尺寸以及铁素体、珠光体组织形态和尺寸;采用控温控速淬火+低温回火工艺,柔性化控制调质处理后板条马氏体的尺寸.所生产NM600 耐磨钢组织中的马氏体板条束平均宽度为0.602 1～1.745 3μm,抗拉强度1 890～2 135 MPa,-20℃冲击功30～59 J,布氏硬度HBW586?602,延伸率≥10％,实现了高强度、高硬度、高韧性与高延伸性能的良好匹配.     

高级别管线钢X100的试验研究

通过合理的组织、成分设计,在实验室试制成功X100管线钢.利用光学显微镜、透射电镜与背散射电子衍射技术(EBSD),研究了X100钢不同组织构成对力学性能的影响规律及其合理的控冷制度,并通过Gleeble-1500热模拟机获得了试验钢的CCT曲线.结果表明,少量AF(Acicular Ferrite)、GB(Granular Bainite)组织的出现,可使原奥氏体晶粒得到分割,抑制板条束的过分长大,使板条贝氏体束的有效晶粒尺寸得到显著细化,钢板具有最优的细化组织,塑韧性得到明显改善;冷却速度为20～25 ℃/s,终冷温度为380 ℃时,钢板可获得最佳的组织构成与最优的综合力学性能,屈服强度为775 MPa,抗拉强度为855 MPa,伸长率为16.6%,冲击功(-20℃)为218 J.     

Chinalco Signed Framework Agreement for Strategic Cooperation with Harbin Municipal Government

正Last month,Chinalco signed framework agreement for strategic cooperation with Harbin Municipal Government in Harbin Xiong Weiping,Chairman of Chinalco,said that based on the strategic deployment to build world top-class mining company with the highest growth potential,Chinalco was now concentrating all efforts on making strategic transition and structural adjustment,strategic cooperation with the local governments where     

Jiangxi Promotes Jiangxi Copper Corporation To Become The World's Most Competitive Mining Company

<正>According to the latest info from Jiangxi Province State-owned Assets Supervision and Administration Commission,Jiangxi Copper Corporation was approved to become the first pilot enterprise for deepening reform.Contents of the pilot work is"Three Self"(self expansion,self decision-making,self     

Journal of Rare Earths Contents List of Vol.32(2014)

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Contributions to Baosteel Technical Research wanted

正Baosteel Technical Research,a quarterly journal,which is issued domestically and abroad,is run and sponsored by Baosteel Group Corporation.Baosteel Technical Research mainly reports the achievements in technological innovation,academic research,new product development and industrial equipment improvement by Baosteel.It will continue to follow up on hot topics and serve the company’s technological development and progress.Its readers include experts in     

Ministry of Industry and Information Technology: No Short Term Solution For Our Country’s Excess Nonferrous Metal Smelting Capacity

【正】According to the Ministry of Industry and Information Technology,the Ministry has released the 2013 Operation Report on China’s Industrial Communication Indu...     

Chinalco Signed Framework Agreement for Strategic Cooperation with Gansu Province

正Recently,Chinalco and Gansu Provincial People’s Government signed"Framework Agreement for Strategic Cooperation on Reform,Restructuring and Transition Development of Chinalco’s Electrolytic Aluminum Enterprises in Gansu",signifying that the strategic cooperation between Chinalco and Gansu Province had made new substantive progress.     

Unavoidable Economic Cycle:30% Of Nonferrous Metal Companies Were Involved In Restructuring

正Owing to continual downturn in real estate and bulk commodity markets,a number of traditional industries in China suffered unfavorable impact in performance.With the progressive disclosure of third quarter report,the no-pleasant-surprise performance of     

Baotou Rare Earth Became the World's Biggest High Performance Magnetic Material Base

正The High Performance Magnetic Material Phase II Project,an industry upgrading project implemented by Inner Mongolia Baotou IronSteel Rare Earth(Group)Hi-tech Co.,Ltd,recently basically finished equipment commissioning,signifying that the enterprise had developed the production capacity of15000 t/a Nd-Fe-B strip casting alloy and 5000t/a Nd-Fe-B magnet,thus becoming the world’s     

Introducing Two Central Enterprises to Integrate Rare Earth Industry,Shandong Rare Earth Group Breaks Surface

正With the signing of"Letter of intention for Propelling Integration of Shandong Rare Earth Enterprises"between Shandong Province Commission Of Economy and Informatization,China IronSteel Research Institute Group("China Steel Institute"),and China Rare MetalsRare Earth Co.,Ltd("China Rare Earth"),the"Shandong Rare Earth Group"jointly set up by the 3 units thus broke surface.On August 9,reporters of the China Economic Herald learned from Shandong Province     

Aluminium Production by Province or City in 2014

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