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1.
为了满足各行业对钢铁材料提出的更高强度、更好韧性的要求,在钢中加入适量的微合金化元素并结合合理的控扎控冷工艺,有利于在高温轧制阶段获得细小均匀的奥氏体再结晶晶粒,这是提高钢材强度及韧性的有效途径之一。通过Gleeble-3800型热模拟试验机,对两种不同锆含量的低碳微合金Ti-Zr钢进行多道次压缩变形试验,模拟实际轧制情况,研究试验钢在不同锆含量和不同变形方式(等温变形和变温变形)下的热变形行为,并结合组织观察分析讨论了锆含量和变形条件对试验钢奥氏体组织细化行为和析出行为的影响。结果表明,变形温度的升高可以降低高锆钢各道次的流变应力。变温变形条件下,锆含量的升高会提高试验钢各道次的流变应力;奥氏体再结晶晶粒会随着锆含量的升高和变形温度的降低而发生细化,采用变温变形方式比等温变形方式更有利于得到细小的奥氏体晶粒,高锆钢在1 050℃→1 25℃→1 000℃变温变形后得到了最小的奥氏体平均晶粒尺寸(为8.2μm);锆含量升高会提高试验钢中析出相的数量,变形方式对析出相数量的影响不大,变形温度的升高会使析出相发生粗化。锆含量增加所导致的形变诱导析出相的增多,以及变温变形过程中温度的降低,起...  相似文献   

2.
介绍了几种常用的晶粒细化方法,包括微合金细化法、电磁场细化法、纳米析出相细化法、应变诱导相变和形变强化相变,分析了超细晶材料在开发和应用中存在的问题,为钢铁材料晶粒细化的研究及实际应用提供参考。  相似文献   

3.
王超  袁国  王国栋 《钢铁》2023,(9):167-177
针对热轧厚钢板、管型材等产品在高温轧制或焊接条件下组织难以均匀细化的共性问题,开展了基础理论-关键技术-产品工艺的系统研究,通过对已有技术的发展和探索创新,提出基于析出相控制的新型本质细晶钢技术路线。通过“冶炼→连铸→轧制→冷却→焊接”全流程一体化工艺控制,调控钢中高热稳定性微-纳米析出相粒子分布,结合加工工艺优化控制,促进基体和焊接组织均匀细化,突破传统组织性能调控手段及工艺条件限制,显著提升材料综合服役性能,推动实现先进钢材的高性能绿色化制造。采用热力学计算软件分析了低合金钢中部分氮化物和氧化物的析出规律,利用电子探针显微镜和扫描电镜表征了钢中典型高温析出相的结构特征,从析出物的热稳定性及其与基体的交互作用角度说明复合析出相的设计思路。讨论了第二相诱导晶内铁素体形核的贫锰区机制和共格界面机制,采用高温原位表征技术研究了晶内铁素体转变行为,阐述了基于多类型、多尺度复合析出相体系设计的晶界、晶内多重组织细化机制。技术应用于大线能量焊接用钢板、热轧结构钢高温高效轧制、热轧无缝钢管在线组织调控、低成本热轧抗震钢筋等产品和工艺的开发,取得良好应用效果,并在更多产品领域展现出广阔的应用前景。  相似文献   

4.
为了研究Ti-Zr微合金钢轧制变形过程中变形温度和Zr含量对内部应力应变的分布及奥氏体组织演变的影响,通过热模拟实验和金相分析获得3种不同Zr含量的Ti微合金钢应力应变曲线及奥氏体的晶粒尺寸及分布情况。研究结果表明:变形温度的升高会降低3种实验钢的内部应力,促进应力均匀分布,其中0.12Ti-0.02Zr钢应力下降的最明显,Zr的加入会促进Ti微合金钢再结晶奥氏体的形核和形变诱导析出相的析出,形变储能消耗量增大,不容易在变形过程中积累应力和应变;但过多的Zr会因为大量析出相而使实验钢的变形抗力增大,导致应力和应变累积。综合考虑,使用Ti-Zr复合微合金化技术实现奥氏体组织的超细化均匀时,Zr元素的添加量应控制在0.02%左右。  相似文献   

5.
超高碳钢组织超细化的工艺   总被引:3,自引:0,他引:3  
阐述了超高碳钢组织超细化工艺及其机理。这些工艺包括:二阶段热形变处理技术、热形变 离异共析转变处理技术、热形变 DET 形变处理技术、循环热处理技术及复合热处理技术。该超细化组织由极细的铁素体晶粒以及在其中均匀分布的渗碳体颗粒组成。此外,分析了硅、铝、铬等合金元素对相变温度的影响及其对网状碳化物和石墨化的抑制作用,讨论了合金化对超高碳钢的组织超细化的影响。  相似文献   

6.
中碳钢形变及冷却过程中的组织演变   总被引:1,自引:0,他引:1  
热模拟单向压缩下,中碳钢形变温度低于Ad3(786℃)点时,析出形变诱导铁素体(DIF),DIF量随形变温度降低而提高;在低于750℃形变时,DIF量远高于平衡态铁素体含量54%。DIF析出时碳原子高度富集在铁素体晶界和铁素体/奥氏体界面。形变后在低于A1(719℃)温度等温或控冷过程中。过冷奥氏体将发生不同类型的转变:高于Ad3形变试样中,奥氏体转变为铁素体+片层状珠光体;低于Ad3点但高于Ar3(645℃)点形变时,未转变奥氏体转变为铁素体+片层状珠光体+晶界渗碳体;稍高于Ar3点形变时,将获得铁素体+弥散渗碳体的球化组织。  相似文献   

7.
通过实验室模拟试验,研究了高氮钒钢的金相组织和形变诱导铁素体体积分数,分析了钒对高氮钒钢变形诱导相变的影响.试验结果表明,钒的加入促进了形变诱导铁素体相变,细化了铁素体晶粒,提高了形变诱导铁素体体积分数.  相似文献   

8.
超 细 晶 粒 钢 的 制 备 原 理 及 技 术   总被引:1,自引:0,他引:1  
 介绍了国内外超细晶粒钢的发展情况;阐述了晶粒细化对钢铁材料综合性能的影响,从微合金化、形变诱导相变、热处理和新型机械控制轧制技术及磁场或电场处理等方面介绍了获得细化晶粒钢的关键技术,最后从实际应用角度出发,提出了超细晶粒钢生产及应用中存在的问题。  相似文献   

9.
通过对3种不同铌、钒含量的低碳钢进行多道次热压缩变形以模拟中厚板的超细晶轧制工艺,考察了显微组织演变过程、微合金元素和变形条件对组织演变的影响。结果表明:变形过程中有部分奥氏体通过形变诱导相变转变为铁素体;变形并快速冷却后得到平均晶粒尺寸为3~6μm的超细晶组织.铌促进、钒抑制形变诱导铁素体相变,铌、钒微合金化均有较好的细化作用,铌的作用优于钒.再结晶温度以上进行的粗轧有利于精轧时形变诱导铁素体的形成;在精轧温度范围内,增加变形道次、降低道次应变率有利于获得细化的显微组织;降低终轧变形温度对组织细化是最有效的.  相似文献   

10.
真空条件下,在低碳微合金钢中添加微米级ZrC颗粒,使其成为钢在热轧时奥氏体的形变核心及其形变诱导铁素体的再结晶核心以细化晶粒,获得了屈服强度为518 MPa的低碳微合金高强度钢,对钢中第二相粒子包括碳化物析出相及外加ZrC颗粒对钢的强化作用进行了讨论。采用化学相分析及X射线小角散射法研究了钢中析出相的成分、数量及粒度分布,同时用扫描电镜和透射电镜对钢中第二相粒子的形态和微观结构进行了观察,发现尺寸小于18 nm的MC析出相含量较少,未发现小于10 nm的析出相。研究结果表明:细晶强化是试验钢的主要强化方式,位错强化次之,而沉淀强化和固溶强化较小,外加ZrC颗粒在细晶强化和位错强化中产生重要作用。  相似文献   

11.
The continuous cooling transformation behavior, the effect of coiling temperature on microstructure and mechanical properties, and strengthening mechanisms of Ti microalloyed high strength hot strip steel were systematically investigated by thermal simulation testing machine, laboratory rolling mill, SEM and HR-TEM. The dynamic CCT curve was established. The results show that the austenite to ferrite and pearlite transformation takes place when the cooling rate is less than 1??/s. The austenite to bainite transformation accompanied with austenite to ferrite and pearlite transformation takes place when the cooling rate is in the range of 5 ??/s to 10 ??/s. The bainitic transformation temperature is about 600??. The amount of granular bainite decreases, while the amount of lath bainite increases with the increase of cooling rate in the range of 20??/s to 50??/s. Furthermore, the study on the effect of coiling temperature on the microstructure and mechanical properties of experimental steel has shown that the strength and plasticity of tested steel are improved with decreasing the coiling temperature. When the coiling temperature is 550?棬the experimental steel possesses optimal mechanical properties owing to the grain refinement and precipitation of nano-scale TiC particles. And the tensile strength, yield strength and elongation of tested steel were 742MPa, 683MPa and 22??5%, respectively.  相似文献   

12.
 The microstructure characteristics and mechanical properties of a low-silicon TRIP steel containing phosphorus and vanadium at different finish rolling temperatures were studied by laboratory hot rolling experiments. Different ratios of multiphase microstructure (ferrite, granular bainite and retained austenite) are obtained. With a decrease in finish rolling temperature, the volume fractions of ferrite and retained austenite increase. EBSD analysis reveals that most of the ferrite grains are fine, and decreasing of finish rolling temperature leads to an increase in low angle boundaries. Under the joint effects of fine grain strengthening, dislocation strengthening and precipitation strengthening, higher strength is obtained. When the finish rolling temperature is decreased to 800 ℃, the steel has excellent mechanical properties: Rp02=470 MPa; Rm=960 MPa; Rp02/Rm=049; A50=197%; n=025.  相似文献   

13.
 The effect of the run-out table cooling patterns on the microstructure and mechanical properties of Nb microalloyed steel plates was investigated by hot rolling experiment. The results showed that the mixed microstructure containing ferrite, bainite and significant amounts of retained austenite can be obtained through three kinds of cooling patterns on the run-out table under the same hot rolling condition. Three kinds of cooling patterns possess different austenite transformation kinetics, which leads to variations in microconstituent characteristics. The yield strength increases, the tensile strength decreases and the total elongation tends to increase as the cooling patterns Ⅰ, Ⅱ and Ⅲ were applied respectively. The yield strength, the total elongation and the product of tensile strength and ductility reach the maximum values (547 MPa, 37.2% and 28384 MPa·%, respectively) for the steel plate processed by cooling pattern Ⅲ.  相似文献   

14.
韩理  胡海江  王巍  王俊  徐光 《钢铁研究学报》2022,34(10):1145-1152
摘要:变形和等温热处理是高强贝氏体钢主要生产工艺,已有研究表明低于马氏体相变起始温度(Ms)的等温热处理可以促进贝氏体相变动力学,低温奥氏体预变形也可以加速贝氏体相变。研究了低于Ms温度变形对后续等温贝氏体相变动力学和组织的影响,结果表明,并未出现预想的加速相变叠加效应,反而,变形温度低于Ms温度时,贝氏体相变动力学减弱,等温贝氏体相变孕育期延长。低于Ms温度等温相变时,贝氏体铁素体与母相奥氏体位向关系接近K-S关系,变形试样虽然获得了一部分先马氏体,且能提高贝氏体形核率,但并非所有的胚核都能发生长大,变形改变母相奥氏体取向,使贝氏体原本的位向关系遭受破坏,导致有效形核率降低。  相似文献   

15.
通过实验室热轧试验,研究了不同终轧温度下低硅含磷系热轧TRIP钢的组织特征及性能特点。结果表明:终轧温度由900℃降低到790℃,铁素体体积分数增加,贝氏体体积分数降低,残余奥氏体体积分数变化不太明显;终轧温度900和820℃时,得到贝氏体为基体的室温组织;终轧温度降低到790℃时,低温变形促进了奥氏体到铁素体的相变率...  相似文献   

16.
摘要:采用不同的宽展比对水电站用低碳贝氏体钢07MnCrMoVR进行了轧制,对回火前后试验钢的微观组织形貌进行了观察,并对力学性能进行了检验,同时利用EDS能谱分析了回火过程中碳化物析出行为。结果表明:采用较小的宽展比能提高粗轧纵轧阶段的单道次压下率以及变形区系数,有效地破碎奥氏体再结晶晶粒,轧制后获得细小的粒状贝氏体组织,高温回火后析出大量的渗碳体和合金碳化物均匀弥散地分布在贝氏体铁素体基体上。随着回火温度的提高,试验钢强度性能呈现先升高再降低的现象,伸长率和低温冲击韧性持续升高。  相似文献   

17.
 借助MMS-300热模拟试验机研究了控轧温度区间、终冷温度、贝氏体区等温处理以及冷却路径对微合金化热轧TRIP钢组织演变规律的影响。结果表明,随着控轧温度区间“下调”,组织中的铁素体晶粒越来越细小,铁素体量逐渐增加,残余奥氏体量则先增加后减少。终冷温度升高时,组织中的残余奥氏体量也呈现出先增加后减少的变化趋势,而贝氏体温度范围等温时间的延长使残余奥氏体量增加。相对于“缓冷+快冷”,轧后采用“快冷+缓冷+超快冷”冷却路径更有助于铁素体晶粒的细化和奥氏体的残留。在“快冷+缓冷+超快冷”冷却路径下,当控轧温度区间为900~840℃,缓冷温度范围为710~680℃,贝氏体等温处理制度为450℃×5min时,组织中的残余奥氏体量达到最高值113%。  相似文献   

18.
文章利用全自动相变仪对不同锰铬含量的贝氏体钢组织转变进行了试验研究,对比分析了不同锰铬元素含量对贝氏体钢过冷奥氏体相变点的影响,并研究了不同转变温度对贝氏体钢组织转变的影响,试验结果表明贝氏体钢组织转变的最佳温度为330℃,为贝氏体钢生产工艺开发提供了理论依据。  相似文献   

19.
The relationship between microstructure and mechanical properties of gas metal arc weld metal with strength over 890 MPa is discussed. The microstructure of the weld metals is characterized with OM, SEM, TEM and EBSD. The microstructure of the weld metals is mainly composed of martensite and bainite. Experimental results show that the microstructure with predominant fine lath bainite possesses good toughness of 77 .l, while its yield strength is less than 800 MPa. The microstructure of coarse lath martensite and bainite has the lowest toughness of 43 J and its yield strength is 820 MPa. The mixed microstructure with fine martensite, bainite and retained austenite films bears good combination of toughness and yield strength (62 J and 880 MPa, respectively). It is concluded that fine effective grain size and ductile phase of austenite films are two main factors to achieve good mechanical properties.  相似文献   

20.
The current study concerns the development of a low-carbon, microalloyed ultra-high-strength steel on a pilot scale. The continuous cooling transformation has been evaluated, and a flat top “C” curve with a mixed microstructure of bainite and martensite has been obtained at a lower transformation temperature. The steel has been processed thermomechanically, followed by air cooling and water quenching. In addition, a variation in microstructure and mechanical properties at different finish rolling temperatures has been studied. Although a mixture of granular bainite and bainitic ferrite with interlath and intralath precipitation of NbC/NbC(N)/TiC(N) particles are the characteristic microstructural feature of air-cooled steel, the lath martensitic structure along the fine NbC/NbC(N)/TiC(N) precipitate is obtained in case of a water-quenched steel. The high-strength value obtained in the current steel is caused by the accumulated contribution of fine-grained, pancaked austenite, highly dislocated fine lath martensitic structure along with the presence of tiny precipitates of microalloy carbide/carbonitride.  相似文献   

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