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Baran Teoman Chadakarn Sirasitthichoke Andrei Potanin Piero M. Armenante 《American Institute of Chemical Engineers》2021,67(10):e17354
Njs, the minimum agitation speed to just-suspend dispersed solids in liquids in stirred tanks, is a critical parameter to operate industrial processes. The focus of this work was to develop a novel observer-independent method to experimentally obtain Njs in tanks that cannot be visually inspected internally using electrical resistance tomography (ERT). The mean bulk resistivity was measured across electrodes mounted on an ERT linear sensing probe placed inside a stirred tank containing water and glass beads. As the agitation speed increased, more solids became suspended and the resistivity measured by the probe changed. Plots of resistivity variation vs. agitation speed resulted in an S-shaped curve that could be analyzed to determine Njs. The Njs values obtained with this novel approach compared very favorably with those obtained using other methods requiring transparent tanks. It is expected that the ERT method proposed here could find applications in many industrial solid–liquid mixing processes. 相似文献
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An integrated flow model was developed to simulate the fluidization hydrodynamics in a new bubble-driven gas–liquid–solid fluidized bed using the computational fluid dynamic (CFD) method. The results showed that axial solids holdup is affected by grid size, bubble diameter, and the interphase drag models used in the simulation. Good agreements with experimental data could be obtained by adopting the following parameters: 5 mm grid, 1.2 mm bubble diameter, the Tomiyama gas–liquid model, the Schiller–Naumann liquid–solid model, and the Gidaspow gas–solid model. At full fluidization state, an internal circulation of particles flowing upward near the wall and downward in the centre is observed, which is in the opposite direction compared with the traditional core-annular flow structure in a gas–solid fluidized bed. The simulated results are very sensitive to bubble diameters. Using smaller bubble diameters would lead to excessive liquid bed expansions and more solid accumulated at the bottom due to a bigger gas–liquid drag force, while bigger bubble diameters would result in a higher solid bed height caused by a smaller gas–solid drag force. Considering the actual bubble distribution, population balance model (PBM) is employed to characterize the coalescence and break up of bubbles. The calculated bubble diameters grow up from 2–4 mm at the bottom to 5–10 mm at the upper section of the bed, which are comparable to those observed in experiments. The simulation results could provide valuable information for the design and optimization of this new type of fluidized system. 相似文献
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Experimental measurements with six impeller types in solid‐liquid suspensions indicate that impeller power draw in the turbulent regime is approximately proportional to the solid‐liquid suspension density when the solids are distributed throughout the liquid; however, the accuracy of this approach is limited and there are clear differences in the behaviours of the various impellers. In general, power draw increases are less than suspension density increases for impellers with large blade‐trailing vortices, while power draw increases are equal to or greater than suspension density increases for impellers with smaller blade‐trailing vortices. The power draw data is well‐described using linear relations between the impeller power number and the density difference correlating parameter proposed by Micheletti et al.,[9] with the slope of the relation being dependent on impeller type. More extensive testing with a pitched‐blade turbine, using a greater variety of solids, found that the relation between the impeller power number and the density difference correlating parameter is independent of particle size for particles as large as 1 mm (1000 microns). For particles larger than 1.7 mm (1700 microns), in addition to suspension density, the solid volume fraction affects the pitched‐blade turbine power number; however, it is difficult to determine if this effect exists at all scales or if it is a result of the large particle size relative to the impeller dimensions in the experimental system. For large particles, the power draw is increased by the addition of neutrally‐buoyant particles that do not change the suspension density, with the magnitude of the increase being dependent on impeller type. 相似文献
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Jason J. Giacomelli Harry E. A. Van den Akker 《American Institute of Chemical Engineers》2021,67(2):e17097
The 2015 Grenville-Mak-Brown (GMB) correlation for predicting the just suspended condition assumes that the length scale of the suspending eddy is equivalent to the particle diameter. This article investigates the role of the time scale of the relevant eddies with respect to the particle response time. The local turbulence just above the tank bottom is gauged by means of single-phase LESs at the just suspended conditions determined in new experiments in dilute suspensions. By means of a novel nondimensional Suspension number we found that the relevant suspending eddies in the inertial subrange are 1.2–1.5 times larger than the particle size while the required eddy time scale is of the order of two times the particle response time. Further, we concluded that the mean energy dissipation rate is a suitable approximation of the local energy responsible for suspension. These results do not impact the effectiveness of the GMB correlation. 相似文献
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In order to investigate the mechanism of the low‐density solid particle and liquid mixing process, a specialised agitator structure was used. Both computational fluid dynamics simulation and experiments were carried out to study the two‐phase mixing characteristics in the stirred vessel. The mixing process was captured by snapshots. The flow field and solid phase volume fraction evolution were analysed. Experimental and numerical results agreed well with each other. Solid particles floating on the liquid surface were gradually transported to the bottom through the centre of the vessel and the mixing time was predicted and tested. Results indicate that the agitator structure used in this study is able to form an obvious axial circulation in the vessel and then achieve a good performance in low‐density solid and liquid mixing operations. The study provides a valuable reference for the design and optimisation of solid–liquid mixing equipment. © 2011 Canadian Society for Chemical Engineering 相似文献
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The aim of this study was to investigate the effect of feed time of the oil phase on the average droplet size of Pickering emulsions produced in stirred tanks. Three types of impellers were tested: RT, up-pumping PBT (PBTU), and down-pumping PBT (PBTD). All the impellers were tested at two sizes, T/3 and T/2. All configurations were compared at constant tip speed, power per mass, and impeller Reynolds number. The droplet diameters were measured in Mastersizer® 3,000 (Malvern). The results showed that an increase in feed time causes a reduction in the average droplet size. At lower impeller speeds and higher feed times, the effect is more pronounced. It was found that some other geometric parameters also have an impact on the average droplet size. 相似文献
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The minimum speed required for complete suspension (Njs) is a major parameter for solids suspension in stirred tanks. Micale et al. 7th UK Conference on Mixing (2002) determined Njs by using a pressure gauge technique in a model vessel. In the present work Njs was measured by the same later technique in a more practical vessel with varying C/T ratio and the impeller direction of rotation. The results were compared to those obtained by Zwietering Chem. Eng. Sci. 8 , 244–253, (1958) correlation. Agreement was found between results from present work and predictions by Zwietering's correlation with maximum difference not exceeding 17%. 相似文献
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Distribution of solid phase in a solid–liquid suspension being mixed in a vortexing, unbaffled stirred tank is difficult to model numerically. The need is to be able to predict the shape of the vortex (air–water interface) and the distribution of solids in the liquid domain. Typically, the problem is approached with assumptions about the shape of the interface to capture the solid distribution through a multi-phase Eulerian model (doi: 10.1016/j.ces.2018.07.023 ). In this work, a multi-step modelling framework for multi-phase systems that have a free surface along with the dispersion of secondary phase(s) in the liquid domain is proposed. To demonstrate the method, it is applied to a laboratory-scale vortexing unbaffled system reported in the literature (doi: 10.1021/ie071225m ) and a pilot-scale tank (doi: 10.1016/j.cej.2018.10.020 ). The predictions from the computational fluid dynamics model are compared with the experimental profiles of solid volume fractions. Using the model, the effects of solid density, particle size, particle loading, and impeller speed are investigated for the laboratory-scale system. An interesting self-similar nature in the axial distribution of solid is observed when the loading is varied from 0.5 to 10 volume percent. 相似文献
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In this study, the effects of impeller rotation speed, off‐bottom clearance, blade angle, types of solid and liquid, etc., on the suspension pattern of sedimentary particles and particle rise height in liquid were investigated with a hemispherical vessel without baffles under low particle concentration. The transition conditions of suspension pattern between regimes I and II, and regimes II and III, were observed visually, and their non‐dimensional equations were expressed with an acceptable correlation by varying the above operation factors a great deal. Here, regime I is stagnation of particles on a vessel bottom, II is partial suspension, and III is complete suspension in liquid. The non‐dimensional equation of the maximum particle rise height was also successfully obtained. The combination of the non‐dimensional equations of transition and maximum particle rise height permitted us to determine the adequate solid/liquid mixing operation conditions without collision of particles with device parts. 相似文献
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《分离科学与技术》2012,47(15):2409-2417
Simulation of the fluid dynamics of solvent extraction in centrifugal contactors requires advanced models to account for complex physical phenomena including turbulent free-surface flow and liquid-liquid dispersion physics. The use of an open-source computational fluid dynamics (CFD) framework allows for implementation of advanced models not feasible in commercial CFD applications. The open-source CFD package OpenFOAM has been used to simulate turbulent, multiphase flow in the annular centrifugal contactor, including simulations of the mixing zone (annular region), and of the coupled operation of the mixing and separation (rotor interior) zones. These simulations are based on the Volume of Fluid (VOF) methodology along with Large Eddy Simulation (LES) for turbulence. The results from these simulations compare favorably with previous simulations using a commercial CFD tool and with available experimental data. They also give insight into the requirements for more advanced multiphase models needed to accurately capture flows in these devices. 相似文献
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Bastien Delacroix Louis Fradette François Bertrand Bruno Blais 《American Institute of Chemical Engineers》2021,67(11):e17360
The vast majority of solid–liquid mixing studies have focused on high Reynolds number applications with configurations and impeller geometries adapted to this type of regime. However, the mixing of particles in a viscous fluid is an essential element of many contemporary industries. We used the computational fluid dynamics-discrete element method model previously developed in our group to investigate solid–liquid mixing with close-clearance impellers in the laminar regime of operation. We compared different geometries, that is, the double helical ribbon, anchor, Paravisc™, and Maxblend™ impellers. We investigated the impact of fluid viscosity and compared the results with those obtained with the pitched blade turbine, a more commonly used impeller, based on power consumption for equivalent mixing states. This study highlights that the higher the viscosity of the fluid, the more interesting it is to use close-clearance impellers for their ability to generate a strong shear stress and a strong bulk flow in the entire vessel. 相似文献
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Eugene Vorobiev 《American Institute of Chemical Engineers》2022,68(3):e17547
Unified nonlinear model is proposed for the prediction of consecutive solid–liquid filtration and expression at the constant pressure. This model is based on the Darcy–Terzaghi filtration-consolidation equations modified to consider power-law pressure dependence of the specific cake resistance, and transforming Darcy law to the linear form. The model considers nonuniform structure of compressible filter cakes obtained by filtration and following expression. The profiles of local compressive pressure and local cake characteristics are simulated and compared for different moderately and highly compressible filter cakes (H.K. kaolin, CaCO3, silica, activated sludge) based on the analytical and numerical solutions of the model. It is shown that the behavior of solid–liquid expression depends from the initial structure of compressed materials. Consolidation ratio U of the filter cakes with initially nonuniform structure formed by filtration differs from that of semi-solid materials with initially uniform structure. Different methods of determination of consolidation coefficient are analyzed and compared for nonuniformly structured filter cakes. 相似文献
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An inverse liquid–solid circulating conventional fluidized bed (I-CCFB) is realized by injecting particles from the top of a conventional liquid–solid fluidized bed (0.076 m ID and 5.4 m height) that is operated in a newly developed circulating conventional fluidization regime located between the conventional and circulating fluidization regimes. The I-CCFB can achieve a higher solids holdup compared to both conventional and circulating liquid–solid fluidized beds. A new parameter, the bed intensification factor, is defined to quantify the increased solids holdup observed with external solids circulation. The Richardson–Zaki equation is shown to be applicable to the I-CCFB regime and can be used to correlate the slip velocity and solids holdup, both of which increase with the solids circulation rate. A new flow regime map is presented, including the I-CCFB and a variety of other liquid–solid fluidized beds. 相似文献
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Haoliang Wang Xiangyang Li Zai-Sha Mao Chao Yang 《American Institute of Chemical Engineers》2019,65(9):e16668
An invasive image velocimetry (IIV) is developed for measurement of multiphase flows, which starts from the photographs taken by a vision probe and then determines the flow fields after a series of images processing steps. It overcomes the limitations of laser-based velocimetries, especially inapplicability to dense multiphase flows. The measurement results using IIV in the single phase stirred tank agree well with those by laser Doppler velocimetry except for the region close to impeller. The disagreement could mainly be attributed to long frame intervals so that the one-quarter rule of correlation evaluation cannot be satisfied. As it is applied in solid–liquid systems with particles loads above the upper limit of laser-based techniques without refractive matching, the direct and indirect interactions between particles and liquid are preliminarily analyzed based on instantaneous solid–liquid flows. More accurate mean velocities are obtained which provides a useful benchmark for computational fluid dynamics modeling validation in dense multiphase flow. 相似文献
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Fatemeh Gholami;Salman Movahedirad;Mohammad Amin Sobati;Mojtaba Babaei; 《加拿大化工杂志》2024,102(1):177-195
In the present study, the hydrodynamic behaviour of a three-dimensional bubbling fluidized bed reactor was studied using the finite volume method and granular kinetic theory. The effect of two types of gas distributors (i.e., perforated and porous plates) on the gas/solid hydrodynamic was investigated. The residence time distribution model was utilized to check the deviation of the gas flow pattern from the ideal flow patterns for two types of distributors. The parameters indicating the degree of back-mixing, such as mean residence time and dimensionless variance, were calculated. Also, the model was verified through the comparison of the particle velocity with experimental data obtained by the particle image velocimetry–digital image processing (PIV-DIA) technique. It was found that the gas flow pattern in the present bubbling fluidized bed is closer to the mixed flow than the plug flow pattern. It was also found that the porous plate distributor gives more uniform hydrodynamic distributions of gas and solid in the bed, which results in better gas–solid mixing due to the formation of the smaller bubbles. 相似文献