共查询到20条相似文献,搜索用时 343 毫秒
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综述了纳米CeO2在紫外线吸收剂、催化剂领域、抛光粉、电化学上的应用。对目前主要用于制备纳米CeO2的化学制备方法如水热法、化学沉淀法、溶胶-凝胶法、喷雾反应法等做了介绍,总结了纳米二氧化铈制备方法的研究进展,分析了其优缺点,并对其制备方法的研究方向进行展望。 相似文献
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Effect of preparation temperature on the formation of Sr2CeO4 phosphor particles in the spray pyrolysis 总被引:1,自引:0,他引:1
Seung Kwon Hong Dae Soo Jung Hyo Jin Lee Yun Chan Kang 《Korean Journal of Chemical Engineering》2006,23(3):496-498
Sr2CeO4 phosphor particles were prepared by spray pyrolysis at various preparation temperatures. The effect of preparation temperatures
on the morphology, crystal structure and photoluminescence characteristics of the post-treated Sr2CeO4 phosphor particles was studied. Phase pure Sr2CeO4 phosphor particles were not produced by spray pyrolysis without post-treatment. The optimum post-treatment temperature to
produce the Sr2CeO4 phosphor particles with high photoluminescence intensity was 1,000 °C in spray pyrolysis. The spherical morphology of the
as-prepared particles obtained at high preparation temperatures above 1,400 °C had maintained after post-treatment at 1,000
‡C. The relative photoluminescence intensities of the Sr2CeO4 phosphor particles varied with the preparation temperatures in the spray pyrolysis. The as-prepared particles obtained by
spray pyrolysis at preparation temperatures below 1,400 °C converted into phase pure Sr2CeO4 phosphor particles after post-treatment at 1,000 ‡C. The optimum preparation temperature of the as-prepared particles was
1,400 °C to produce the Sr2CeO4 phosphor particles with spherical shape and high photoluminescence intensity in the spray pyrolysis. 相似文献
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分析了喷雾干燥技术的应用现状,指出了喷雾干燥技术在功能性产品制备方面的重要作用。以产品质量作为最终的目标函数,对喷雾干燥技术提出了更高的要求,特别是利用喷雾干燥技术制备高品质功能性材料,要求喷雾干燥技术的内涵更丰富,与交叉学科的联系更广泛。介绍了以喷雾干燥技术为平台的微胶囊制备、复合离子制备、超细化离子制备、喷雾热解法等新方法的基本原理以及制备实例。指出了喷雾干燥技术新的研究发展方向。 相似文献
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Samples of Bulgarian perlite mineral deposit (natural alumino-silicate glass) in the Rhodope mountain were coated with Ag particles via a spray pyrolysis method. This method allows uniform distribution of the silver particles on the outer shell surfaces. SEM, XPS, FT-IR, and XRD methods were applied for characterization of the samples. The XRD investigations of the pristine samples revealed the formation of metallic silver and a small quantity of Ag2O3 phase. The presence of silver was also confirmed by XPS analysis. It was established that Ag/perlite composite prepared by spray pyrolysis is a promising catalyst for ozone decomposition. The high catalytic activity is preserved during the complete course of the catalytic reaction. After the catalytic activity test some structural and phase changes in the samples were observed. The XRD patterns of the ozonated samples proved the presence of metallic silver, AgO and Ag2O3 phases. The FT-IR analyses revealed that some bands, assigned to Si-O-Si stretching modes, were shifted to lower frequencies after the ozone decomposition test. In general, the spray pyrolysis method turned out to be a very suitable technique for preparation of highly active silver-coated perlite catalyst for efficient ozone removal. 相似文献
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The X1 type Y2SiO5:Tb phosphor particles with high brightness were prepared by spray pyrolysis from spray solution with NH4F flux material. The phosphor particles prepared by spray pyrolysis at high preparation temperature had spherical shape, fine size and dense morphology. The mean sizes of the phosphor particles prepared at 900 and 1650 °C were 1.3 and 0.9 μm. The emission spectrum of the phosphor particles prepared by spray pyrolysis at 1650oC had the characteristics of X1 type Y2SiO5:Tb phosphor. The photoluminescence intensity of the phosphor particles directly prepared by spray pyrolysis from spray solution with 20 wt.% NH4F flux of the product at temperature of 1650 °C was 127 and 184% of the X1 and X2 type Y2SiO5:Tb phosphor particles post-treated at 1100 and 1300 °C, respectively. The Y2SiO5:Tb phosphor particles prepared by spray pyrolysis at 1650 °C had X1 type crystal structure because of short residence time of particles inside hot wall reactor of 0.4 s. 相似文献
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介绍了喷雾热解法制备薄膜技术,综述了喷雾热解法制备薄膜的研究进展,着重介绍了喷雾热解法制备铁电薄膜的研究,以及等离子体增强喷雾热解法制备薄膜技术。 相似文献
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喷雾热解法制备高纯超细氧化铝粉 总被引:3,自引:0,他引:3
本文以高纯硫酸铝铵为原料,用喷雾热解法制得纯度大于99.9%、细度为10 ̄20nm的高纯超细α-Al2O3粉。探讨喷雾热解工艺条件对粉体性能的影响。 相似文献
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A Pulse Combustion-Spray Pyrolysis Process for the Preparation of Nano- and Submicrometer-Sized Oxide Particles 总被引:1,自引:0,他引:1
W. Widiyastuti Wei-Ning Wang Agus Purwanto I. Wuled Lenggoro Kikuo Okuyama 《Journal of the American Ceramic Society》2007,90(12):3779-3785
The preparation of nano- and submicrometer particles using an integrated pulse combustion–spray pyrolysis process was investigated for the first time. Zinc oxide nanoparticles with average sizes ranging from 20 to 40 nm were synthesized using a salt precursor with a lower decomposition temperature than the pulse combustion (PC) temperature. Particles of a doped-type oxide, gadolinium oxide-doped with europium, were also produced from a precursor, whose decomposition temperature was higher than the PC temperature, and were observed to be ellipsoidal–toroidal in shape and submicrometer in size. The high-intensity fluctuating pressures generated by PC and the precursor decomposition temperature are proposed as the reasons for the formation of either nanoparticles or aspherical particles. In addition, hot gas fluctuating flow in PC enhanced energy transfer, resulting in more crystalline particles, as compared with particles produced by conventional spray pyrolysis. 相似文献