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《Journal of Sulfur Chemistry》2013,34(6):599-610
An efficient, general, and atom-economic synthesis of organoammonium thioselenophosphinates has been developed by exploiting a three-component reaction between secondary phosphine sulfides, elemental selenium, and various amines. The reaction proceeds under mild conditions (70–75 °C, 1 h, EtOH) to afford thioselenophosphinates in 77–94% yields. 相似文献
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《Journal of Sulfur Chemistry》2013,34(3):257-261
An efficient synthesis of 1,3-diaryl-2,3-dihydro-1,5-benzothiazepines has been developed by the reaction of various 1,3-diaryl-2-propenones with 2-aminothiophenol under thermal solvent-free conditions in the presence of a sub-stoichiometric amount of cyanuric chloride. 相似文献
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《Journal of Sulfur Chemistry》2013,34(6):521-531
Several poly(alkylene sulfide)s have been synthesized in excellent yields from reactions of α,ω -dibromo- and/or α,ω-dichloroalkanes with sodium sulfide nonahydrate under reflux conditions. The procedure is general, simple and convenient for the production of various poly(alkylene sulfide)s and the way reaction parameters influence the properties of the polymers formed has been examined. 相似文献
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《分离科学与技术》2012,47(8):2166-2182