AZ31B合金的铸轧组织

利用金相及扫描电镜对AZ31B合金热模拟和铸轧样组织结构进行研究。研究结果表明：在不同应变量下,热模拟样品的晶粒粒度均随应变速率的增加而减小,而当其他条件相同时,变形量越大晶粒粒度越小,冷却强度降低,合金呈典型铸态组织;利用铸轧技术生产的AZ31B合金,当应变速率一定时,随着初始铸轧温度的降低,铸轧态板材的树枝晶粒度逐渐减小;而在初始铸轧温度一定时,随着应变速率的增大,铸轧态合金板材的树枝晶粒度也逐渐减小;而随着应变速率的提高,树枝晶沿轧向呈流线状排列的趋势增强;在AZ31B合金铸轧过程中,轧制力不能太大,否则容易引起热裂。     

Microstructure and mechanical properties of AZ91 magnesium alloy subject to deep cryogenic treatments

AZ91 magnesium alloy was subjected to a deep cryogenic treatment. X-ray diffraction （XRD）, scanning electronic microscopy （SEM）, and transmission electronic microscopy （TEM） methods were utilized to characterize the composition and microstructure of the treated samples. The results show that after two cryogenic treatments, the quantity of the precipitate hardening β phase increases, and the sizes of the precipitates are refined from 8-10μm to 2-4μm. This is expected to be due to the decreased solubility of aluminum in the matrix at low temperature and the significant plastic deformation owing to internal differences in thermal contraction between phases and grains. The polycrystalline matrix is also noticeably refined, with the sizes of the subsequent nanocrystalline grains in the range of 50-100 nm. High density dislocations are observed to pile up at the grain boundaries, inducing the dynamic recrystallization of the microstructure, leading to the generation of a nanocrystalline grain structure. After two deep cryogenic treatments, the tensile strength and elongation are found to be substantially increased, rising from 243 MPa and 4.4% of as-cast state to 299 MPa and 5.1%.     

离心铸造对AZ91镁合金组织及力学性能的影响

为了研究卧式离心铸造工艺对AZ91镁合金力学性能及显微组织的影响,采用卧式离心铸造方法制备外径为400 mm、厚度为20 mm且长度为1 000 mm的AZ91镁合金管材,并对离心铸造态与自然凝固态AZ91镁合金管材的微观组织及力学性能分别进行了观察与测试.结果表明,离心铸造态AZ91镁合金管材的抗拉强度和伸长率分别为158 MPa和3.4%,与自然凝固态管材相比分别提高了20%和89%.离心铸造态镁合金管材的微观组织得到明显细化.与自然凝固态AZ91镁合金管材相比,离心铸造态AZ91镁合金管材在凝固过程中的共晶转变在很大程度上受到抑制,并形成了以α-Mg为主相的组织.卧式离心铸造方法提高了AZ91镁合金的综合力学性能,并使合金的组织得到细化.     

热挤压镁合金AZ91的微观组织及其力学行为

研究了热挤压镁合金AZ91的微观组织以及在不同试验温度和不同的热处理条件下的拉伸力学性能.结果表明：热挤压可以显著减小AZ91合金的晶粒尺寸，其拉伸力学性能与试验温度密切相关；可以通过热处理来改善其拉伸力学性能，其中人工时效及固溶时效工艺均是改善和提高挤压后AZ91镁合金力学性能的有效途径.此外，利用扫描电镜分析了AZ91镁合金拉伸试样的断口形貌，并探讨了其拉伸断裂机制.     

不锈钢丝增强AZ91镁合金复合材料的显微组织及其力学性能

采用渗流铸造法制备了体积分数约为40%、60%、80%的不锈钢丝增强AZ91镁合金复合材料.利用万能试验机对其进行压缩实验;并利用扫描电镜观察复合材料的显微组织以及压缩后的断口形貌.结果表明:不锈钢丝在AZ91镁合金基体中的分布随着其体积分数的增加逐步均匀;不锈钢丝与AZ91镁合金界面润湿性较好.压缩试验表明:复合材料的抗压强度较AZ91镁合金抗压强度明显提高,40%、60%、80%体积分数的复合材料断裂强度分别为371、387、553 MPa;随着不锈钢丝体积分数的增加,材料的破坏方式由剪切破坏转变为劈裂.     

Improved mechanical properties in AZ31 magnesium alloys induced by impurity reduction

Mechanical properties and microstructures of AZ31 magnesium alloys containing different impurity levels but having the same alloying element content, were investigated at ambient temperature. These AZ31 alloys were produced by semi-continuous casting, wherein the content of impurity was varied systematically. Microstructure observation shows that finer grains are existent in the alloy with lower impurity level. Tensile testing reveals that a reduction of impurity content results in a noticeable increase of the strength and elongation in the alloys in the cast, homogenized and extruded states. As the impurity content decreases from 0.0462wt% to 0.0163wt%, the ultimate tensile strength is evidently enhanced by 62 MPa and the elongation is nearly doubled in the homogenized specimen. The observed property improvement was discussed in terms of the microstructure variation with impurity reduction.     

Kinetics of recrystallization for twin-roll casting AZ31 magnesium alloy during homogenization

The kinetics of recrystallization for twin-roll casting AZ31 magnesium alloy with different thicknesses during homogenization was analyzed.It is shown that fine grains are first formed at the boundaries of deformed bands in the twin-roll casting slab.The recrystallized grains with no strain are gradually substituted for the deformed microstructure of twin-roll casting AZ31 magnesium alloy.The incubation temperature and time for the recrystallization of a twin-roll casting AZ31 magnesium alloy strip with a thickness of 3 mm are lower and shorter than those of the 6-mm thick strip,respectively.The 3-mm thick twin-roll casting magnesium alloy has finer grains than the 6-mm thick strip.The activation energies of recrystallization for twin-roll casting AZ31 magnesium alloy slabs with the thickness of 3 and 6 mm are 88 and 69 kJ/mol,respectively.The kinetics curves of recrystallization for twin-roll casting AZ31 magnesium alloy were obtained.     

轧制工艺对ZA35合金组织和性能的影响

为了提高ZA35合金的力学性能,采用轧制工艺制备ZA35合金板坯,利用x-射线衍射仪(XRD)、金相显微镜(OE)、扫描电子显微镜(SEM)以及能谱分析(EDS)等技术分析和检测了ZA35合金铸态、不同轧制态和热处理态的显微组织和性能.结果表明:轧制可以显著提高ZA35合金的综合力学性能,使抗拉强度提高了27.8%,硬度指标提高了36.4%,伸长率比铸态增加了近2倍.轧制使合金组织细化,初生α相增多,ε相由块状变成细小的点状弥散分布于枝晶间.轧制合金在经过365℃固溶3h和120℃时效12h热处理后合金力学性能最好,抗拉强度达到512MPa、伸长率为4.9%、硬度为HB127.     

Al-Cu-Mg硬铝合金TIG焊焊接接头的组织与力学性能

为了研究Al-Cu-Mg硬铝合金TIG焊焊接接头的组织与力学性能,采用ER4043焊丝对2A12硬铝合金进行了焊接实验.利用光学显微镜、扫描电子显微镜、透射电子显微镜、能谱分析仪和硬度计对Al-Cu-Mg硬铝合金的组织和力学性能进行了表征.结果表明,焊缝的强度和塑性较低,焊缝边缘为柱状晶,中心为枝晶组织,晶界存在大量低熔点共晶体.近缝区存在明显的晶界液化现象,晶粒为圆润的等轴晶,焊缝的硬度大幅度下降.固溶区焊缝的硬度和母材相近,基体中存在大量的针状S'相,可对该区域起到强化作用.过时效区基体软化现象比较严重,存在很多S(Al2Cu M g)相.     

Characterization of microstructure evolution and mechanical properties of the spray-deposited AZ31 magnesium alloy

The cylindrical billets of a Mg-3Al-1Zn (AZ31) alloy were synthesized by spray deposition processing. The microstruc-ture evolution and mechanical properties of the alloy were investigated. The results reveal that the microstructure of the AZ31 alloy is refined significantly by spray deposition processing. A homogeneous and equiaxial-grain structure with an average grain size of 17 μm is obtained. Further grain refinement with an average grain size of 5 μm is attributed to dynamic recrystallization during e...     

钕对AZ91镁合金组织及机械性能的影响

采用微观分析、机械性能测试及断口分析等方法研究了钕对AZ91-Nd镁合金(w(Nd)=0,0.1%,0.3%,0.5%,1.0%,1.5%)的微观组织和机械性能的影响。结果表明:Nd以固溶和金属间化合物(A l11Nd3)的形式存在时具有细化晶粒、抑制二次β相析出、使不完全离异共晶转化为离异共晶的作用;Nd通过固溶强化、析出强化和细晶强化增加了合金强度和硬度,并改善了塑性;加入Nd后合金的断裂机制从脆性解理断裂转变为准解理断裂。     

Microstructure and mechanical properties of ZE10 magnesium alloy prepared by equal channel angular pressing

ZE10 magnesium alloy was subjected to equal-channel angular pressing(ECAP) up to 12 passes in a die with an angle of 120° between the two channels at 250-300°C.An inhomogeneous microstructure of bimodal grains including fine grains of 1-2 μm as well as coarse grains of about 20 μm was obtained after the initial 1-4 ECAP passes.The grain size became increasingly homogeneous with further ECAP processing and the grains were significantly refined to 1-2 μm after 8 passes and further refined to 0.5-1 μm after 12...     

Preparation of 2024/3003 gradient materials by semi-continuous casting using double-stream-pouring technique

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Effect of ultrasonic power and casting speed on solidification structure of 7050 aluminum alloy ingot in ultrasonic field

With the experiment and finite element simulation, the influences of power ultrasonic on the solidification structure of 7050 aluminum alloy ingot in semi-continuous casting were researched, and the effects of casting speed on solidification structure in ultrasonic field were also analyzed. The experiment and simulation results show that the solidification structure of the ingot is homogeneously distributed, and its grain size is obviously refined at ultrasonic power of 240 W. The average grain sizes, which can be seen from the Leica microscope, are less than 100 μm. When the casting speed is 45-50 mm/min, the best grain refinement is obtained.     

Semisolid die forging process,microstructures and properties of AZ31 magnesium alloy mobile telephone shells

A semisolid slurry of AZ31 magnesium alloy was prepared by vibrating wavelike sloping plate process,and the semisolid die forging process,microstructures,and properties of the magnesium alloy mobile telephone shell were investigated.The semisolid forging process was performed on a YA32-315 four-column universal hydraulic press.The microstructures were observed by optical microscopy,the hardness was analyzed with a model 450SVD Vickers hardometer,the mechanical properties was measured with a CMT5105 tensile ...     

Microstructure and mechanical properties of Al-Zn-Cu-Mg-Sc-Zr alloy after retrogression and re-aging treatments

The mechanical properties and stress corrosion cracking (SCC) resistance of an Al-Zn-Cu-Mg-Sc-Zr alloy under different aging conditions were investigated. The dependence of microstructure and mechanical properties on aging parameters was evaluated by tensile test, hardness test and conductivity measurement. The results show that for the alloys with retrogression and re-aging treatment (RRA), the conductivity increases with the retrogression time and temperature, while the tensile strength decreases. The transmission electron microscopy (TEM) results show that the precipitates η(MgZn₂) at grain boundary aggregate apparently with retrogression time and the precipitates inside the matrix exhibit the similar distribution to T6 temper, which comprises fine GP zones, large η′(MgZn₂) and η(MgZn₂) phases. According to the mechanical properties and microstructure observations, the optimal RRA regime is recommended to be 120 °C, 24 h + 180 °C, 30 min + 120 °C, 24 h. The strength level of the alloy after the optimum RRA treatment is similar to that in T6 condition and the SCC resistance is improved obviously in contrast to T6 condition.     

挤压铸造对ZA27合金组织及性能的影响

研究了挤压铸造对ZA27合金组织及性能的影响.挤压铸造可以显著提高合金的综合力学性能，抗拉强度指标提高了约19.2%，硬度指标提高了约25.5%，延伸率比重力铸造合金增加了近2倍.挤压铸造使合金的组织细化，并使组织中共晶体的数量明显增多，尺寸减小.共晶体由粗大的长条状变成细小的层片状，ε相由棒状或块状变成细小的点状弥散分布于枝晶间.电子探针分析表明，挤压铸造明显改善了合金元素的显微偏析，使试件整体成份均匀.     

Y和Ce对AZ91D镁合金显微组织和力学性能的影响

为了开发低成本、高强度、耐高温的新型镁合金,研究了微量Y、Ce对AZ91D镁合金显微组织和力学性能的影响。研究结果表明:Y和Ce复合加入AZ91D镁合金,能明显细化组织晶粒,从而改善合金在室温和高温下的力学性能。当加入0.6%Ce-0.3%Y(质量分数)时,合金晶粒细化效果较好,其室温和高温力学性能比较理想。