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SBS与MMA本体接枝物的合成与表征 总被引:5,自引:0,他引:5
以过氧化苯甲酰(BFO)作引发剂,用甲基丙烯酸甲酯(MMA)既作为热塑性弹性体(SBS)的溶剂又作为与SBS进行接枝共聚反应的单体,合成得到了接枝共聚物SBS-g-MMA;用红外光谱、核磁共振谱、透射电镜、扫描电镜及动态粘弹谱对其组成和结构进行了表征。 相似文献
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橡胶增韧AS树脂研究 总被引:2,自引:0,他引:2
用NBR、EVA、MBS和CPE单独或联合增韧AS树脂,研究表明,MBS/NBR和MBS/CPE对AS树脂有协同增韧效应,EVA可作为AS/NBR体系的相容剂,NBR中AN含量将影响增韧效果,并用TEM和SEM观察了共混物的形态。 相似文献
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PPO/SEBS-g-MAH共混体系的冲击断面和微观形变过程 总被引:4,自引:0,他引:4
用扫描电子显微镜(SEM)观察了PPO/SEBS和PPO/SEBS-g-MAH共混物的常温缺口冲击断面,发现PPO/SEBS共混体系的冲击断布有大量韧窝;PPO/SEBS-g-MAH共混体系由呈现中心为棒,四周为环的冲击断面形貌,对PPO/SEBS-g-MAH冲击断的应力发白区的SEM观察结果表明在冲击断面下方,合金发生大的取向;TEM的观察结果显示在应力发白区内,弹性体周围存在大量的微穴,未发现 相似文献
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介绍了一种新的快速成型技术-多相喷射沉积(MJS),分析讨论了MJS快速成型系统的设计,原型零件的成型工艺过程,制定了后处理工艺,最后给出了用MJS制备Ni60金属多孔材料的显微组织和性能。 相似文献
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根据济南二机床集团公司应用计算机建立信息管理系统十多年的经验,指出关系型DMBS系统必须有类似SQL的第四代主同级语言来支持,ORACLERDBMS是标准的关系型DMBS的数据操纵语言。介绍了济南二机床集团应用ORCALERDBMS的实例。 相似文献
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积木式建模系统(BMBS)是构造模型库管理系统的一种先进方法,它可以给用户提供一个模型库的原型系统,用户根据自己的需求,建造面向特定对象的模型库。由于BMBS必须以集成知识环境为支撑,所以它实际上又可以成为开发DSS的原型系统。本文介绍了我们开发的BMBS。 相似文献
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介绍用IBM-PC计算机辅助测试SSPA器件参数的12位高速数据采集系统。该系统带有缓冲RAM,对SSPA的视频信号采集速度可达500kHz,适合于各种需要对SSPA器件进行高速高精度采集的应用。 相似文献
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用IBM—PC计算机测试SSPA器件参数的数据采集系统 总被引:3,自引:1,他引:2
介绍用IBM-PC计算机辅助测试SSPA器件参数的12位高速数据采集系统。该系统带有缓冲RAM,对SSPA的视频信号采集速度可达500kHz,适合于各种需要对SSPA器件进行高速高精度采集的应用。 相似文献
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S. Gómez M.D. Vlad J. López M. Navarro E. Fernández 《Materials science & engineering. C, Materials for biological applications》2013,33(6):3329-3335
Sawbones© open-cell foams with different porosity grades are being used as synthetic bone-like models for in vitro mechanical and infiltration experiments. However, a comprehensive characterization of these foams is not available and there is a lack of reliable information about them. For this reason two of these foams (Refs. 1522-505 and -507) have been characterized at the micro architectural level by scanning electron microscopy, computed tomography and image data analysis. BoneJ open software and ImageJ open software were used to obtain the characteristic histomorphometric parameters and the three dimensional virtual models of the foams. The results showed that both foams, while having different macro porosities, appeared undistinguishable at the micro scale. Moreover, the micro structural features resembled those of osteoporotic rather than healthy trabecular bone. It is concluded that Sawbones© foams behave reasonably as synthetic bone-like models. Consequently, their use is recommended for in vitro comparison purposes of both mechanical and infiltration testing performed in real vertebra. Finally, the virtual models obtained, which are available under request, can favour comparisons between future self-similar in vitro experiments and computer simulations. 相似文献
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《International Journal of Impact Engineering》2001,25(5):455-472
The mechanical properties at room temperature of three polymeric foams (namely EPP, PUR and PS/PA foams) have been experimentally evaluated in both static and impact loading conditions. The energy absorption characteristics have been examined both through the energy-absorption diagram method and through the efficiency diagram method. The meaning of the efficiency parameter, already used in the literature, has been explained in a proper, satisfactory way. It is shown that the maximum of the efficiency identifies the condition for optimal energy absorption of the foam, while the maximum stress reaches a value limited through other design considerations. The efficiency diagram method is then used to obtain synthetic diagrams useful to characterize the material and to help the design of energy absorbing components. These synthetic selection diagrams are obtained for the three tested materials. Finally, some consideration are drawn comparing the mechanical performance of the three considered types of foams and their dependency on density. 相似文献
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Samina Arif Gary Burgess Ramani Narayan Bruce Harte 《Packaging Technology and Science》2007,20(6):413-419
Green Cell® foam (GCF) is a biodegradable foam packaging material produced from a proprietary cornstarch blend. It is commercially available in a variety of laminations and constructions. Cushioning ability and thermal resistance (R‐value) are the fundamental properties needed to compete against synthetic foams. Since GCF is starch based and biodegradable, a concern was that moisture would likely affect its physical properties. Cushioning characteristics and insulation R‐values of 1 and 2 inch foams were determined as a function of temperature and moisture content. The ASTM method D1596 was used to determine the cushioning properties and an ice melt test was used to determine the thermal resistance. Moisture sorption isotherms were developed at three temperatures (20, 25 and 30°C) to determine its moisture sensitivity. The 1‐inch‐thick foam had lower G values at lower static stresses than synthetic foams, but had higher G values at higher static stresses. The 2‐inch‐foam had G values similar to that of synthetic foam materials. Dimensional changes were observed at higher relative humidity (RH) conditions, especially at 30°C. The R‐values at higher humidities were also less than that of synthetic materials. Copyright © 2007 John Wiley & Sons, Ltd. 相似文献
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中间相沥青基泡沫炭的气泡生长过程 总被引:4,自引:0,他引:4
以AR合成中间相沥青为原料,在不同的温度下发泡制得了泡沫炭.采用扫描电镜和光学显微镜等分析手段对中间相沥青基泡沫炭的气泡生长机理进行了初步研究,讨论了温度对泡孔结构的影响.结果表明,当温度从480℃升至540℃时,平均泡孔直径从500μm升到800μm.最初形成的泡沫在熔融沥青中分布不均匀,汇集在沥青的上表面;气泡在Z轴方向的形状是椭球形,在Z轴垂直方向为球形.中间相沥青基泡沫炭气孔的形状和泡沫的体积密度密切相关.形成的泡沫体在z轴方向存在明显的体积密度梯度. 相似文献
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Edgar B. Montufar Tania Traykova Josep A. Planell Maria-Pau Ginebra 《Materials science & engineering. C, Materials for biological applications》2011,31(7):1498-1504
Hydroxyapatite foams are potential synthetic bone grafting materials or scaffolds for bone tissue engineering. A novel method to obtain injectable hydroxyapatite foams consists in foaming the liquid phase of a calcium phosphate cement. In this process, the cement powder is incorporated into a liquid foam, which acts as a template for macroporosity. After setting, the cement hardens maintaining the macroporous structure of the foam. In this study a low molecular weight surfactant, Polysorbate 80, and a protein, gelatine, were compared as foaming agents of a calcium phosphate cement. The foamability of Polysorbate 80 was greater than that of gelatine, resulting in higher macroporosity in the set hydroxyapatite foam and higher macropore interconnectivity. Gelatine produced less interconnected foams, especially at high concentrations, due to a higher liquid foam stability. However it increased the injectability and cohesion of the foamed paste, and enhanced osteoblastic-like cell adhesion, all of them important properties for bone grafting materials. 相似文献
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This study presents comprehensive morphological and mechanical properties (static, dynamic) of open-cell rigid foams (Pacific
Research Laboratories Inc. Vashon, WA) and a synthetic vertebral body derived from each of the foams. Synthetic vertebrae
were comprised of a cylindrical open-cell foam core enclosed by a fiberglass resin cortex. The open-cell rigid foam was shown
to have similar morphology and porosity as human vertebral cancellous bone, and exhibited a crush or fracture consolidation
band typical of open-celled materials and cancellous bone. However, the foam material density was 40% lower than natural cancellous
bone resulting in a lower compressive apparent strength and apparent modulus in comparison to human bone. During cyclic, mean
compression fatigue tests, the synthetic vertebrae exhibited an initial apparent modulus, progressive modulus reduction, strain
accumulation and S-N curve behaviour similar to human and animal vertebral cancellous bone. Synthetic open-cell foam vertebrae
offer researchers an alternative to human vertebral bone for static and dynamic biomechanical experiments, including studies
examining the effects of cement injection.
Presented, in part, at the XXth Congress of the International Society of Biomechanics and 29th Annual Meeting of the American
Society of Biomechanics, Cleveland, OH, July 31-August 5, 2005 相似文献
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Domain-Decomposition Singular Boundary Method for Stress Analysis in Multi-Layered Elastic Materials
This paper applies an improved singular boundary method (SBM) in conjunction with domain decomposition technique to stress analysis of layered elastic materials. For problems under consideration, the interface continuity conditions are approximated in the same manner as the boundary conditions. The multi-layered coating system is decomposed into multiple subdomains in terms of each layer, in which the solution is approximated separately by the SBM representation. The singular boundary method is a recent meshless boundary collocation method, in which the origin intensity factor plays a key role for its accuracy and efficiency. This study also introduces new strong-form regularization formulas to accurately evaluate the origin intensity factors for elasticity problem. Consequently, we dramatically improve the accuracy and convergence of SBM solution of the elastostatics problems. The proposed domain-decomposition SBM is tested on two benchmark problems. Based on numerical results, we discuss merits of the present SBM scheme over the other boundary discretization methods, such as the method of fundamental solution (MFS) and the boundary element method (BEM). 相似文献
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The biocompatibility and the load-bearing ability of lightweight titanium made it possible to be used as a biomaterial, especially in hip revision and fixation surgery. It was initially shown that sand-blasted or surface-roughened titanium implants had an improved bone-bonding ability over the bioinert metallic surfaces. Plasma-spraying of a phase mixture of loosely-attached calcium phosphates on titanium implants further improved their in vivo bone-bonding ability. However, stoichiometric calcium hydroxyapatite ceramic of high crystallinity is known to have poor in vivo resorbability, and is shy of taking part in bone remodeling and of being resorbed by the osteoclasts. Supersaturated calcium phosphate (CaP) solutions, such as synthetic body fluids (SBF), on the other hand, are able to form “carbonated, hydrophilic and apatite-like” CaP nanoaggregates on titanium surfaces. A Tris-buffered SBF solution with an HCO3− concentration of 27 mM was used in this study. Neat, NaOH-etched, and SBF-coated (biomimetic coating) titanium foams were compared with in vitro cell culture experiments by using rat osteoblasts. SBF-coated foams were found to yield the highest protein concentration at the end of the in vitro culture tests. Such biomimetic coatings were easily formed on flat strips, springs, or 3D foams of titanium, without any geometric constraints. The coated titanium springs and foams were characterized by using XRD, SEM, and FTIR. 相似文献
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Broekema FI van Oeveren W Zuidema J Visscher SH Bos RR 《Journal of materials science. Materials in medicine》2011,22(4):1081-1086
Topical hemostatic agents can be used to treat problematic bleedings in patients who undergo surgery. Widely used are the
collagen- and gelatin-based hemostats. This study aimed to develop a fully synthetic, biodegradable hemostatic agent to avoid
exposure to animal antigens. In this in vitro study the suitability of different newly developed polyurethane-based foams
as a hemostatic agent has been evaluated and compared to commonly used agents. An experimental in vitro test model was used
in which human blood flowed through the test material. Different modified polyurethane foams were compared to collagen and
gelatin. The best coagulation was achieved with collagen. The results of the polyurethane foam improved significantly by increasing
the amount of polyethylene glycol. Therefore, the increase of the PEG concentration seems a promising approach. Additional
in vivo studies will have to be implemented to assess the application of polyurethane foam as a topical hemostatic agent. 相似文献