Vacuum effects on fatigue crack growth in submicrometre‐thick freestanding copper films

To clarify vacuum effects on fatigue crack growth in freestanding metallic thin films, experiments were conducted on approximately 500‐nm‐thick copper films inside a field emission scanning electron microscope. Fatigue crack growth accompanied by intrusion/extrusion formation occurred in vacuum, and da/dN was smaller than in air in the middle‐ΔK region (ΔK ≈ 1.7‐3.1 MPam^1/2). Conversely, in the low‐ΔK region (ΔK ? 1.7 MPam^1/2), da/dN was larger in vacuum than in air. Further, fatigue crack growth in vacuum occurred below the fatigue threshold in air (ΔK_th,air). A nonpropagating crack after reaching ΔK_th,air continued to propagate in vacuum when the environment changed from air to vacuum. This indicates that fatigue crack growth resistance is smaller in vacuum than in air under the same effective driving force. The fatigue damage area near the crack paths in vacuum in the low‐ΔK region became wider, suggesting that the nucleation of fatigue damage was enhanced in vacuum.     

A cumulative damage model for fatigue life estimation of high‐strength steels in high‐cycle and very‐high‐cycle fatigue regimes

A cumulative fatigue damage model is presented to estimate fatigue life for high‐strength steels in high‐cycle and very‐high‐cycle fatigue regimes with fish‐eye mode failure, and a simple formula is obtained. The model takes into account the inclusion size, fine granular area (FGA) size, and tensile strength of materials. Then, the ‘equivalent crack growth rate’ of FGA is proposed. The model is used to estimate the fatigue life and equivalent crack growth rate for a bearing steel (GCr15) of present investigation and four high‐strength steels in the literature. The equivalent crack growth rate of FGA is calculated to be of the order of magnitude of 10^?14–10^?11 m/cycle. The estimated results accord well with the present experimental results and prior predictions and experimental results in the literature. Moreover, the effect of inclusion size on fatigue life is discussed. It is indicated that the inclusion size has an important influence on the fatigue life, and the effect is related to the relative size of inclusion for FGA. For the inclusion size close to the FGA size, the former has a substantial effect on the fatigue life. While for the relatively large value of FGA size to inclusion size, it has little effect on the fatigue life.     

A general scenario of fish‐eye crack initiation on the life of high‐strength steels in the very high‐cycle fatigue regime

When high‐strength steels are subjected to very high‐cycle fatigue loading, crack initiation site shifts from surfaces to the interior, and a fish‐eye forms on the fracture surface. Majority of the fatigue life is estimated to be associated with the formation of this internal crack morphology. In the present work, features of such internal cracks in two high‐strength steels are studied. Specifically, three initiation patterns are investigated. A general internal crack initiating scenario is proposed base on an understanding of dislocation slip in the materials. A simplified threshold is calculated from Young's modulus and interatomic spacing, defining the transition from the initiation stage to the crack propagation. The relationship between internal crack initiation and slower descending S‐N curves is discussed.     

Near‐threshold fatigue crack growth properties of wrought magnesium alloy AZ61 in ambient air,dry air,and vacuum

Environmental influences on near‐threshold fatigue crack growth in wrought magnesium alloy AZ61 were investigated. Fatigue tests were performed in ambient (humid) air, dry air, vacuum, and dry nitrogen gas at 19 kHz cycling frequency and load ratio R = ?1. Threshold stress intensity factor amplitudes, K_th, determined for limiting growth rates below 5 × 10^?13 m/cycle were 1.1 MPam^1/2 in ambient air and 1.2 MPam^1/2 in dry air. A much higher K_th of 1.9 MPam^1/2 was measured in vacuum and dry nitrogen gas. This suggests oxygen to be the most detrimental constituent of ambient air that increases near‐threshold crack propagation rates and decreases K_th. The deleterious effect of humidity is comparatively small. Corrosive influences are effective at ultrasonic cycling frequency for growth rates below approximately 3 × 10^?9 m/cycle. The crack propagation curves in ambient and dry air show a plateau‐like regime where the fracture mode changes from purely ductile to a mixed ductile and brittle mode. In vacuum and dry nitrogen gas, a ductile crack path is found for all investigated crack growth rates.     

Small fatigue crack growth behavior of titanium alloy TC4 at different stress ratios

In this paper, the small fatigue crack behavior of titanium alloy TC4 at different stress ratios was investigated. Single‐edge‐notch tension specimens were fatigued axially under a nominal maximum stress of 370 MPa at room temperature. Results indicate that fatigue cracks in TC4 initiate from the interface between α and β phases or within α phase. More than 90% of the total fatigue life is consumed in the small crack initiation and growth stages. The crack growth process of TC4 can be divided into three typical stages, ie, microstructurally small crack stage, physically small crack stage, and long crack stage. Although the stress ratio has a significant effect on the total fatigue life and crack initiation life at constant σ_max, its effect on crack growth rate is indistinguishable at R = ?0.1, 0.1, and 0.3 when crack growth rate is plotted as a function of ?K.     

In situ synchrotron ultrasonic fatigue testing device for 3D characterisation of internal crack initiation and growth

This work presents a new ultrasonic fatigue testing device for studying the initiation and propagation mechanisms of internal microstructurally short fatigue cracks using in situ synchrotron tomography. Its principle is described as well as the method used for automatically detecting crack initiation and its subsequent growth. To promote internal crack initiation, specimens containing internal casting defects were tested between the high cycle and very high cycle fatigue regimes (10⁷‐10⁹ cycles). Preliminary results show the ability of this new device to initiate an internal microstructurally short crack in a reasonable testing time and monitor its growth.     

Non-destructive observation of internal fatigue crack growth in Ti–6Al–4V by using synchrotron radiation μCT imaging

The propagation of an internal fatigue crack in Ti–6Al–4V was non-destructively observed by synchrotron radiation μCT imaging to clarify the crack growth rate in very high cycle fatigue. The results show that the internal crack propagated quite slowly at a rate of less than 10⁻¹⁰ m/cycle. The propagation rate of an internal crack was compared with that of a surface crack in air and in high vacuum to examine the internal fracture process in terms of the environment around the crack. The rate of the internal crack was similar to that of the surface crack in high vacuum, but was significantly lower than that in air. This led us to conclude that the low propagation rate of the internal crack is due to the vacuum-like environment inside the crack.     

High-cycle fatigue properties in Ti–5% Al–2.5% Sn ELI alloy with large grain size at cryogenic temperatures

High‐cycle fatigue properties were investigated for Ti–5% Al–2.5% Sn ELI alloy with a mean α grain size of 80 μm, which had been used for liquid hydrogen turbo‐pumps of Japanese‐built launch vehicles. At cryogenic temperatures, the fatigue strength in high‐cycle region did not increase in proportion to increments of the ultimate tensile strength and the fatigue strengths at around 10⁶ cycles were about 300 MPa independent of test temperatures. Fatigue cracks initiated in the specimen interior independent of the test temperatures of 4 K, 77 K and 293 K. At 4 K and 77 K, several crystallographic facet‐like structures were formed at crack initiation sites. On the other hand, there were no facet‐like structures that could be clearly identified at the crack initiation sites at 293 K. Low fatigue strengths in longer‐life region at cryogenic temperatures could be attributable to the formation of large sub‐surface crack initiation sites, where large facet‐like structure are formed.     

Fatigue life assessment of nodular cast iron containing casting defects

The fatigue behaviour of a nodular cast iron containing casting defects has been investigated in the high-cycle fatigue regime. In this paper, we propose a fatigue life assessment model for flawed materials based on a fracture mechanics approach which takes into account the position and size of the defect, short crack behaviour and the notch effect introduced by the defect. The fatigue behaviour of smooth samples, and long and short crack behaviour have been experimentally determined in order to identify the relevant mechanical parameters; these being introduced into the model. An experimental study has been made both in air and in vacuum in order to account for the position of the defect, noting that internal defects are supposed to be under vacuum conditions. Experimental results, which are based on a two-crack front-marking technique specially developed for this study, show that the propagation of natural cracks is controlled by the effective stress intensity factor in air as well as in vacuum. The K calculation for a short crack in the stress field of a notch is analysed using numerical elastic–plastic results. Comparison between experimental results and the computation of fatigue life for fatigue lives less than 10⁶ cycles shows that the fatigue behaviour of nodular cast iron is controlled by a propagation process. The model proposed is thus relevant for fatigue lives less than 10⁶ cycles so that the defect can be considered as a crack and the initiation stage neglected. Closer to the fatigue limit, this study shows that the initiation stage should be considered in the assessment of fatigue life of nodular cast iron, because a single macroscopic propagation assessment is not enough to describe the whole fatigue life. The defect cannot be considered as a pre-existent crack in the high-cycle fatigue range (>10⁶ cycles), and the initiation stage that contains microcrack propagation around the defect should be evaluated when assessing the high-cycle fatigue life of nodular cast iron.     

Effects of Shot‐Peening on Fretting Fatigue Crack Growth Behavior in Ti‐6Al‐4V

Abstract: The effects of shot‐peening on fretting fatigue crack growth behaviour in titanium alloy, Ti‐6A1‐4V were investigated. Three shot‐peening intensities: 4A, 7A and 10A were considered. The analysis involved the fracture mechanics and finite element sub‐modelling technique to estimate crack propagation lives. These computations were supplemented with the experimentally measured total fretting fatigue lives of laboratory specimens to assess the crack initiation lives. Shot‐peening has significant effect on the initiation/propagation phases of fretting fatigue cracks; however this effect depends upon the shot‐peening intensity. The ratio of crack initiation and total life increased while the ratio of the crack propagation and total life decreased with an increase of shot‐peening intensity. Effects of residual compressive stress from shot‐peening on the crack growth behaviour were also investigated. The fretting fatigue crack propagation component of the total life with relaxation increased in comparison to its counterpart without relaxation in each shot‐peened intensity case while the initiation component decreased. Improvement in the fretting fatigue life from the shot‐peening and also with an increase in the shot‐peening intensity appears to be not always due to increase in the crack initiation resistance from shot‐peened induced residual compressive stress.     

Non-propagating crack behaviour at giga-cycle fretting fatigue limit

Fretting fatigue fracture of industrial machines is sometimes experienced after a long period of operation. It has been a question whether the fatigue limit which means infinite life really exists in fretting fatigue or not. Fretting fatigue tests in ultra high cycle region up to 10⁹ cycles were performed. Test results showed that the S‐N curve had a knee point around 2 × 10⁷ cycles and a clear fatigue limit was observed in the giga‐cycle regime for partial slip conditions. An electropotential drop technique was applied to detect the crack growth behaviour under the contact pad. The real‐time measurement of crack depth during the fretting fatigue test at the fatigue limit showed that a crack initiated at an early stage and then ceased to grow after 2 × 10⁷ cycles and the crack became a non‐propagating crack. These results indicated that the fatigue limit exists in fretting fatigue and infinite endurance is achieved by the mechanism of forming a non‐propagating crack.     

Investigating environmental effects on small fatigue crack growth in Ti–6242S using combined ultrasonic fatigue and scanning electron microscopy

In situ ultrasonic fatigue with a cyclic frequency of 20 kHz was employed in an environmental scanning electron microscope (ESEM) to characterize fatigue crack formation and growth in the near alpha titanium alloy Ti–6242S. The role of environment on small fatigue crack initiation and growth was investigated in vacuum and in variable pressures of saturated water vapor, as well as in laboratory air. Small crack growth behavior from cracks initiated at FIB-produced micro-notches indicated a significant environmental dependence, with fatigue crack growth rates increasing with increasing partial pressures of water vapor. Environment also influenced crack initiation lifetime in that cracks initiated earlier in laboratory air than in vacuum or saturated water vapor environments. Transgranular, crystallographic crack growth was observed in each environment, with the crack path in primary α grains producing facets parallel to basal planes when crack size was small. Small crack growth resistance had a marked sensitivity to microstructural features, such as α/α grain boundaries with high misorientation and α/α + β boundaries. These initial investigations demonstrate the usefulness of in situ ultrasonic fatigue instrumentation (UF-SEM) as a new tool for the characterization of environmental and microstructural influences on very high cycle fatigue (VHCF) behavior.     

Fatigue behaviour of SiCp-reinforced aluminium composites in the very high cycle regime using ultrasonic fatigue

The fatigue behaviour of a 2009/SiC/15p‐T4 DRA composite has been examined in the very high cycle fatigue (VHCF) regime where 10⁷≤N_f≤ 10⁹ cycles. Ultrasonic fatigue was used to achieve the very high cycle counts. Careful processing yielded a composite with a very homogeneous particle distribution with minimal clustering. Fatigue crack initiation was observed almost exclusively at AlCuFe inclusions with no crack initiation observed at SiC particle clusters. Fatigue lives at a given stress level exhibited minimal scatter and subsurface crack initiation was observed in all cases. This behaviour is consistent with the presence of a low number density of critical inclusions that are responsible for crack initiation very early in fatigue life.     

Fatigue crack nucleation and growth in filled natural rubber

Rubber components subjected to fluctuating loads often fail due to nucleation and the growth of defects or cracks. The prevention of such failures depends upon an understanding of the mechanics underlying the failure process. This investigation explores the nucleation and growth of cracks in filled natural rubber. Both fatigue macro‐crack nucleation as well as fatigue crack growth experiments were conducted using simple tension and planar tension specimens, respectively. Crack nucleation as well as crack growth life prediction analysis approaches were used to correlate the experimental data. Several aspects of the fatigue process, such as failure mode and the effects of R ratio (minimum strain) on fatigue life, are also discussed. It is shown that a small positive R ratio can have a significant beneficial effect on fatigue life and crack growth rate, particularly at low strain range.     

Driving forces for localized corrosion‐to‐fatigue crack transition in Al–Zn–Mg–Cu

Research on fatigue crack formation from a corroded 7075‐T651 surface provides insight into the governing mechanical driving forces at microstructure‐scale lengths that are intermediate between safe life and damage tolerant feature sizes. Crack surface marker‐bands accurately quantify cycles (N_i) to form a 10–20 μm fatigue crack emanating from both an isolated pit perimeter and EXCO corroded surface. The N_i decreases with increasing‐applied stress. Fatigue crack formation involves a complex interaction of elastic stress concentration due to three‐dimensional pit macro‐topography coupled with local micro‐topographic plastic strain concentration, further enhanced by microstructure (particularly sub‐surface constituents). These driving force interactions lead to high variability in cycles to form a fatigue crack, but from an engineering perspective, a broadly corroded surface should contain an extreme group of features that are likely to drive the portion of life to form a crack to near 0. At low‐applied stresses, crack formation can constitute a significant portion of life, which is predicted by coupling macro‐pit and micro‐feature elastic–plastic stress/strain concentrations from finite element analysis with empirical low‐cycle fatigue life models. The presented experimental results provide a foundation to validate next‐generation crack formation models and prognosis methods.     

Fracture toughness and growth of short and long fatigue cracks in ductile cast iron EN‐GJS‐400‐18‐LT

Heavy components of ductile cast iron frequently exhibit metallurgical defects that behave like cracks under cyclic loading. Thus, in order to decide whether a given defect is permissible, it is important to establish the fatigue crack growth properties of the material. In this paper, results from a comprehensive study of ductile cast iron EN‐GJS‐400‐18‐LT have been reported. Growth rates of fatigue cracks ranging from a few tenths of a millimetre (‘short’ cracks) to several millimetres (‘long’ cracks) have been measured for load ratios R=?1, R= 0 and R= 0.5 using a highly sensitive potential‐drop technique. Short cracks were observed to grow faster than long cracks. The threshold stress intensity range, ΔK_th, as a function of the load ratio was fitted to a simple crack closure model. Fatigue crack growth data were compared with data from other laboratories. Single plain fatigue tests at R=?1 and R= 0 were also carried out. Fracture toughness was measured at temperatures ranging from ?40 °C to room temperature.     

High cycle fatigue mechanisms in a cast AM60B magnesium alloy

ABSTRACT We examine micromechanisms of fatigue crack initiation and growth in a cast AM60B magnesium alloy by relating dendrite cell size and porosity under different strain amplitudes in high cycle fatigue conditions. Fatigue cracks formed at casting pores within the specimen and near the surface, depending on the relative pore sizes. When the pore that initiated the fatigue crack decreased from approximately 110 µm to 80 µm, the fatigue life increased two times. After initiation, the fatigue cracks grew through two distinct stages before final overload specimen failure. At low maximum crack tip driving forces (K_max < 2.3 MPa√m), the fatigue crack propagated preferentially through the α‐Mg dendrite cells. At high maximum crack tip driving forces (K_max > 2.3 MPa√m), the fatigue crack propagated primarily through the β‐Al₁₂Mg₁₇ particle laden interdendritic regions. Based on these observations, any proposed mechanism‐based fatigue model for cast Mg alloys must incorporate the change in growth mechanisms for different applied maximum stress intensity factors, in addition to the effect of pore size on the propensity to form a fatigue crack.     

Growth behaviour of small surface fatigue cracks in AISI 304 stainless steel

A series of axial tensile fatigue tests (R = 0.1) was carried out to investigate the initiation and the growth behaviours of very small surface fatigue cracks under two different surface conditions (viz. smooth and pitted surfaces) of AISI 304 stainless steel at room temperature. This paper deals with both of the two approaches regarding the analysis of fatigue: the approach based on the concept of fracture mechanics and low cycle fatigue. In particular, both the initiation and growth of cracks and the coalescence of small cracks by fatigue in the specimen have been investigated by the methods of surface replicas and photomicrographs. Quantitative information such as the initiation period, growth and coalescence behaviours of small cracks, and crack growth properties were systematically obtained. The results show that the accurate determination of these parameters is critical for the application of fracture mechanics to fatigue life assessment.     

Nanograin layer formation at crack initiation region for very‐high‐cycle fatigue of a Ti–6Al–4V alloy

The microstructural features and the fatigue propensities of interior crack initiation region for very‐high‐cycle fatigue (VHCF) of a Ti–6Al–4V alloy were investigated in this paper. Fatigue tests under different stress ratios of R = ?1, ?0.5, ?0.1, 0.1 and 0.5 were conducted by ultrasonic axial cycling. The observations by SEM showed that the crack initiation of VHCF presents a fish‐eye (FiE) morphology containing a rough area (RA), and the FiE and RA are regarded as the characteristic regions for crack initiation of VHCF. Further examinations by TEM revealed that a layer of nanograins exists in the RA for the case of R = ?1, while nanograins do not appear in the FiE outside RA for the case of R = ?1, and in the RA for the case of R = 0.5, which is explained by the Numerous Cyclic Pressing model. In addition, the estimations of the fatigue propensities for interior crack initiation stage of VHCF indicated that the fatigue life consumed by RA takes a dominant part of the total fatigue life and the related crack propagation rate is rather slow.     

Corrosion fatigue behaviour of a 15Cr‐6Ni precipitation‐hardening stainless steel in different tempers

Systematic fatigue experiments, including both high‐cycle axial fatigue (S–N curves) and fatigue crack growth (FCG, da/dN–ΔK curves), were performed on a precipitation‐hardening martensitic stainless steel in laboratory air and 3.5 wt% NaCl solution. Specimens were prepared in three tempers, i.e. solution‐annealed (SA), peak‐aged (H900) and overaged (H1150) conditions, to characterize the effects of ageing treatment on the corrosion fatigue (CF) resistance. S–N results indicated that fatigue resistance in all three tempers was dramatically reduced by the aqueous sodium chloride environment. In addition, the smooth‐surface specimens in H900 temper exhibited longer CF lives than the H1150 ones, while those in SA condition stood in between. However, for precracked specimens, the H1150 temper provided superior corrosive FCG resistance than the other two tempers. Comparison of the S–N and FCG curves indicated that early growth of crack‐like defects and short cracks played the major role in determining the CF life for smooth surface. The differences in the CF strengths for the S–N specimens of the given three tempers were primarily due to their inherent differences in resistance to small crack growth, as they were in the air environment.