共查询到20条相似文献,搜索用时 56 毫秒
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纳米材料的气相燃烧合成一般是指利用气体燃料燃烧提供高温,通过物理或者化学过程从气溶胶中获得纳米材料的过程。气相燃烧法可以制备不同结构的纳米材料,具有过程连续、易于规模化、无后处理、低成本等优点,是纳米材料制备最具工业化潜力的方法之一。气相燃烧制备纳米材料涉及快速高温反应和产物单体成核、生长、凝并、团聚等过程,这些过程互相关联、交互影响;纳米材料制备过程中材料结构调控及材料生长机理成为近年来国内外的研究重点。主要介绍了气相燃烧反应器结构、材料制备、结构调控、应用性能和工业生产等方面的研究进展,并对其前景进行了展望。 相似文献
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准一维氧化物纳米材料因其独特的光学性能、电学性能及几何结构而成为当前纳米材料研究领域的热点和重点.论述了直接氧化法制备准一维氧化物纳米材料原理,着重介绍了这一方法在准一维氧化物纳米材料制备中的应用,并对其前景作了简要的展望. 相似文献
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稀土氧化物纳米材料的合成与制备近年来已成为国内外学者研究的一个热点。本文介绍了国内外稀土氧化物纳米材料制备及合成方法的研究进展,并对稀土氧化物纳米材料的制备方法进行了分类。同时,综合比较了各自的优点和缺点,并对各种制备方法在各个领域的应用前景进行了一定的展望。 相似文献
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Flash synthesis of flower-like ZnO nanostructures by microwave-induced combustion process 总被引:1,自引:0,他引:1
Flower-like ZnO particles were fabricated from zinc nitrate and urea via the microwave-induced combustion technique (MICT). The structure and morphology of the products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and selected area electron diffraction (SAED). The effects of growth conditions such as microwave power, radiation time, and molar ratio of urea/Zn2+ were investigated. Results show that the morphologies and particle sizes of the final products depend on the molar ratio of urea/Zn2+. The SEM images of ZnO flowers grown in different periods were employed to explain the formation mechanism. This study provides a simple and efficient approach for synthesizing flower-like ZnO heterostructures. 相似文献
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Hydrothermal synthesis is of considerable interest due to its low cost, simplicity and relatively low growth temperature (typically below 200 °C). Since the synthesis is performed in aqueous solutions (no organic solvents), it can also be safe and environmentally friendly (depending on precursor chemicals). Consequently, it has been a subject of intense research in recent years. In this article, we review recent progress in hydrothermal synthesis of zinc oxide nanomaterials, with focus on practical relevance for a variety of applications. 相似文献
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对高马赫数导弹天线罩材料的性能要求进行了评述,综述了国外天线罩材料的研究进展,特别是重点介绍了美国等军事强国近年来研制的天线罩材料的温度、强度、介电特性以及工艺性能。分析了我国在该领域的研究现状,并提出了今后的发展方向。 相似文献
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社会快速发展带来巨大经济效益的同时,也带来了一系列生态环境问题,如水污染、大气污染和污染物排放。催化降解被认为是处理各种污染的一种有效策略,相对于传统的光催化,压电催化是近几年提出的一种全新的催化方式。通过压电催化将机械能转化为化学能是解决当前水污染难题的一个有效手段,大量的压电材料被应用于压电催化降解的研究,其中BaTiO3基纳米粉体作为一种典型的压电材料,因具有成本低、压电活性强等优点,引起了研究者的广泛关注。本文首先对压电催化的理论和起源进行了概述,列举了一些常用的压电催化材料并针对其压电催化应用进行举例。围绕BaTiO3介绍了其基本结构、纳米BaTiO3粉体的常用制备方法和在压电催化领域的应用及一些典型的改性方法。最后对BaTiO3基纳米粉体在压电催化领域的未来发展趋势进行了展望。 相似文献
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Habibzadeh S Mortazavi Y Khodadadi AA 《Journal of nanoscience and nanotechnology》2010,10(9):6003-6008
A novel technique of chloride solution combustion synthesis (CSCS) is employed for preparation of SnO2 nanoparticles, using SnCl4 and sorbitol as a novel precursor and a fuel, respectively. Ammonium nitrate is also used as a combustion aid. The solution combustion synthesis is a single-step and simple method for nanoparticles synthesis. However, it commonly uses nitrate precursors. In this study tin chloride is used in CSCS method for the first time, employing ammonium nitrate as a combustion aid. The nanoparticles are characterized by means of XRD, SEM, EDS and BET and applied in sensing of carbon monoxide and methane. The molar ratio of fuel plus oxidant to SnCl4 (psi) and the ratio of fuel-to-oxidant (phi) were varied in the modified CSCS technique. The smallest nanoparticles size, i.e., 3.9 nm with 220 m2 x g(-1) obtained at phi = 1 and psi = 1. The sensor fabricated based on the SnO2 nanoparticles obtained by CSCS method shows 2-3 times higher sensitivity to CO than the one obtained by the conventional sol-gel method. The CSCS sensors show high sensitivity to CO at temperatures lower than 300 degrees C, at which insignificant sensitivity to methane is observed. This makes the sensor selective to CO in presence of methane. 相似文献
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Lianxia Chang Haibin Yang Wuyou Fu Jianzhen Zhang Qingjiang Yu Hongyang Zhu Jiuju Chen Ronghui Wei Yongming Sui Xiaofen Pang Guangtian Zou 《Materials Research Bulletin》2008,43(8-9):2427-2433
The amorphous MoS2 nanoparticles have been synthesized by a simple oxidation–reduction reaction in an aqueous solution. A series of products with different morphologies, such as MoS2 nanospheres, inorganic fullerene-like nanospheres, nanorods and Mo bended rods, can be obtained by annealing the amorphous MoS2 nanoparticles under N2 atmosphere under 400–1200 °C. These products have been characterized by X-ray diffraction, field emission scanning electronic microscopy, transmission electron microscopy and high-resolution transmission electron microscopy in detail. The possible transformation mechanism for the structure has been discussed based on the experimental results. In addition, the optical properties of IF-MoS2 have also been performed by UV–vis absorption spectroscopy. 相似文献
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As nanotechnology rapidly advanced over the past decades, a variety of nanomaterials have been developed and studied. Among them, SiC nanomaterials have recently attracted increasing attention for their demonstrated unique chemical and physical properties as well as wide potential applications. This article provides a comprehensive review of the recent progress on the synthesis, novel properties, and applications of SiC nanomaterials. It begins with the introduction of various techniques used for the rational design and synthesis of SiC nanomaterials, with an emphasis on vapor-based and solution-based methods. Discussion is then made on the mechanical, luminescent, electrical, thermal, and wetting properties of SiC nanomaterials as well as the characterizations that reveal them. Thereafter, various intriguing applications particularly in composites, field emitters, field effect transistors, sensors, nanoelectromechanical devices, catalyst, supercapacitors, bioimaging probes and microwave absorbers are highlighted. Finally, this review is concluded with an outlook of future research on SiC nanomaterials, major challenges to be met and possible solutions. 相似文献