放电等离子烧结技术的应用

本文主要介绍了一种粉末烧结技术——放电等离子烧结。首先从结构设计上进行了介绍,放电等离子烧结的主要原理是在粉末进行压力烧结的同时施加电流,最终实现材料的致密化。放电等离子烧结的主要优点是烧结温度低、时间短、升温快、材料致密等。最后列举了放电等离子烧结技术在热电材料、硬质材料、功能梯度材料等的应用实例,论述表明放电等离子烧结技术是一种可以制备高性能材料的烧结技术。     

放电等离子烧结技术的原理及应用

放电等离子烧结(SPS)是一种用于材料烧结致密化的新技术，为深入研究和探讨其技术优势，介绍了SPS的基本原理和系统的组成，讨论了SPS技术在纳米材料的制备、梯度功能材料的烧结和高致密度、细晶粒陶瓷制备等方面的应用，并对其研究和应用前景予以展望。     

脉冲电流烧结技术的研究进展

脉冲电流烧结（Ｐｕｌｓｅ ｅｌｅｃｔｒｉｃ ｃｕｒｒｅｎｔ ｓｉｎｔｅｒｉｎｇ，ＰＥＣＳ）是材料科学领域开发出的一种新型快速烧结技术，已广泛应用于金属与合金、结构陶瓷、氧化物超时体、复合材料、热电材料、离电材料、高分子材料以及功能梯度材料的制备；检验结果，对脉冲电流烧结非导电性粉体的烧结过程和机理，提出自己的观点。     

关于不同粒度粉末层间烧结收缩不同步问题的探讨

在利用粉末烧结法制备梯度功能材料的过程中,会涉及到不同材质或同材质不同粒度粉末共同烧结的问题.主要结合多孔材料和膜材料的烧结,对现有实现共同烧结的技术进行对比,着重介绍了通过调整烧结工艺以达到共烧的方法,并对该技术的发展进行了展望.     

现代烧结技术在难熔金属材料中的应用

微波烧结、放电等离子体烧结、选择性激光烧结作为材料烧结致密化的新技术是活化烧结和快速烧结的有机结合,它们不仅具有升温速度快、烧结时间短、抑制晶粒长大、组织结构可控等独特的优势,而且还具有生产周期短、高效节能的巨大工业应用价值和前景,已成为当今材料领域的研究热点。难熔金属材料及其合金的烧结一直是难熔材料制备和烧结领域的难题,为了进一步探索难熔金属材料及其合金的新型烧结技术,探讨了微波烧结、放电等离子体烧结、选择性激光烧结在难熔金属材料及其合金制备中的应用现状,综述了其工作原理、特点及系统组成。     

放电等离子烧结(SPS)技术

放电等离子烧结（SPS）技术是一种新型的材料制备技术。介绍了SPS技术的发展概况、原理、特点及在材料制备领域的应用。最后，对SPS主发展前景进行了展望。     

电磁场作用下的粉末成形固结技术研究进展

外加电场或磁场作用下粉末成形固结技术是快速制备高性能材料的新途径。应用前景广阔。重点综述了外加电场作用下放电等离子烧结技术和外加磁场作用下动磁压制技术的原理、特点及应用情况。并展望了今后粉末成形固结技术的研究方向。     

放电等离子烧结技术

本文介绍了近岂年在日本迅速发展的放电等离子烧结技术，除概要地介绍了这种烧结新技术的原理和特点外，着重介绍了放电等离子烧结技术在制备梯度功能材料和快速烧结结晶粒陶瓷方面的重要应用，其中后者包括了作者最近在日本大阪府立产业技术研究所取得的部分研究结果。     

超导磁体在NdFeB永磁材料制备技术中应用研究

概述了超导磁体技术的研究进展,分析了超导磁体在NdFeB永磁材料制备过程中的应用前景,重点讨论了超导磁体在烧结NdFeB磁体、NdFeB铸锭组织、HDDR(氢化-歧化)工艺制备NdFeB纳米晶粉末等领域的具体应用情况.     

SPS----一种制备高性能材料的新技术

0引言 块状体材料可以由不同的制备技术获得:物理或化学气相沉积技术从气相出发直接制备固态材料;溶融-冷凝及溶胶-凝胶技术从液相出发制备固态材料.然而,大量先进材料,如精细陶瓷、硬质合金、纳米复合材料等,都采用一种更普遍应用的技术--粉末烧结来合成,也即从固态的粉末出发制备致密的固态材料.这一过程的关键点是如何在实现致密化的前提下,有效地控制合成材料中晶粒的尺寸和形貌以及界面的适度结合.     

A Perspective on Emerging and Future Sintering Technologies of Ceramic Materials

Novel sintering methods have emerged in the recent past years, which have raised great interest in the scientific community. Relying on electric field effects, high heating rates, the use of mechanical pressure, or hydrothermal conditions, they offer fundamental advantages compared to conventional sintering routes like minimizing the energy consumption and enhancing the process efficiency. This perspective aims at explaining these effects in a general way and presenting the status quo of using them for the processing of high-performing ceramic materials. In detail, this work focuses on flash sintering, ultrafast high-temperature sintering, spark plasma sintering, cold sintering, and photonic sintering methods based on different light sources. The specificities, potentials, and limitations of each method are compared, especially in the light of a possible industrialization.     

Experimental investigations into sintering of magnetic abrasive powder for ultrasonic assisted magnetic abrasive finishing process

The importance of magnetic abrasive powder (MAP) in finishing the surface of work materials as a flexible cutting tool in the presence of a magnetic field during the ultrasonic assisted magnetic abrasive finishing (UAMAF) process is quite evident. A sufficiently intense magnetic field provides the desired magnetic force to the iron particles. This holds nonmagnetic abrasive particles firmly and thus makes flexible chains. However, at higher rotational speeds of the magnet due to the requirement of high centripetal force, the chains start flying away from the finishing zone. In the present work, to overcome this deficiency, bonded MAPs were developed using the sintering technique. The effect of various process parameters on the magnetic property (magnetization) of sintered MAPs was investigated. Design of experiments (DoE) was planned as per the L₈ orthogonal array of the Taguchi method, and magnetizations along with M-H curves for all eight different MAPs were measured. Subsequently, analysis of experimental data was carried out using various techniques to optimize the process parameters. It was observed that sintering temperature affects magnetization the most. Scanned microscopy (SEM) and X-ray diffraction (XRD) analysis were also carried out to investigate bonding strength in sintered MAP.     

磁场在金属材料制备成形中的应用

讨论了稳恒磁场、变化磁场对金属凝固组织、基体中合金元素的固溶度以及Al-Cu合金热裂的影响,介绍了动磁压制技术的原理、特点及应用情况,磁场在提高NdFeB永磁体的磁性能和在粉末固相、液相烧结致密化中的应用,并展望了磁场在金属凝固和粉末冶金中未来的研究和应用发展前景.     

Microstructure and Temperature Distribution in ZnAl2O4 Sintered Body by Pulse Electric Current

Microstructure of reaction sintering of ZnAl2O4 at 1500℃ by hot-pressing(HP) and pulse electric current was investigated. The results indicated that the existed cracks in sintered body were caused by structure mismatch. It is the evidence that periodical temperature field existed during pulse electric current sintering of nonconductive materials.The distance between high temperature areas was related to die diameter.     

影响ZTA陶瓷微波烧结的主要工艺过程

通过对ＺＴＡ陶瓷进行微波烧结试验,了解影响陶恣微波烧结速率的主要工艺过程,探索有关微波烧结机理;采用以ＴＥ４４４为基准模式的微波谐振倥,在混合加热模式的基础上增设辅助加热体,同ＺＴＡ陶瓷微波烧结,ＺＴＡ材料中ＺrO2含量越高,该材料的烧结速度越快;输入功率的提高有助于提高烧结速率;辅助加热体的老化现象降低微波烧结速率;微波烧结过程中应避免出现热剧变现象。     

脉冲电流烧结机理的研究进展

脉冲电流烧结（Pulse electric current sintering,PECS)是材料科学领域开发出一种新型快速烧结技术。已广泛应用于金属与合金、结构陶瓷、氧化物超导体、复合材料、热电材料、高分子材料以及功能梯度材料的制备。本文简介脉冲电流烧结特征,结合PECS烧结条件对铜粉末和氧化铝粉体致密化及显微结构影响的实验证据,就脉冲电流烧结过程和机理进行探讨。     

Hybrid processing and anisotropic sintering shrinkage in textured ZnO ceramics

Abstract

We have studied the combined effects of the templated grain growth and magnetic alignment processes on sintering, anisotropic sintering shrinkage, microstructure development and texture in ZnO ceramics. Suspensions of 0–10 vol % ZnO template particles were slip cast in a 12 T rotating magnetic field. Sintering and texture characteristics were investigated via thermomechanical analysis and electron backscatter diffraction, respectively. Sintering as well as texture characteristics depend on template concentration. For the studied ZnO system, there is a critical template concentration (2 vol % in this study) above which densification is limited by the templates owing to constrained sintering. Below this limit, the densification is enhanced and the anisotropic shrinkage is reduced, which is attributed to densifying characteristics of the templates.     

Optimization of the Performance of Porous Low-Carbon Steels by Means of an Evolution Strategy

Possibilities for manufacturing cellular metallic materials are reviewed. However, this study primarily concerns the role of a cell-wall structure in influencing the mechanical behavior of metallic foams. A porous low-carbon steel with a controlled porous structure is processed from spark plasma sintering of ferromagnetic metal segments with a special, elongated shape. The ferromagnetic metal segments are filled into a die-block and their orientation is settled by a static magnetic field. The cell-wall structures of the porous low-carbon steel can be modified in order to improve its performance because differences in the cell-wall structure substantially affect the mechanisms of deformation and failure under different types of loading. The optimal shape of the structure following the required macroscopic mechanical response is established by means of the search scheme of an evolution strategy.     

Room Temperature Electrochemical Sintering of Zn Microparticles and Its Use in Printable Conducting Inks for Bioresorbable Electronics

This study describes a conductive ink formulation that exploits electrochemical sintering of Zn microparticles in aqueous solutions at room temperature. This material system has relevance to emerging classes of biologically and environmentally degradable electronic devices. The sintering process involves dissolution of a surface passivation layer of zinc oxide in CH₃COOH/H₂O and subsequent self‐exchange of Zn and Zn²⁺ at the Zn/H₂O interface. The chemical specificity associated with the Zn metal and the CH₃COOH/H₂O solution is critically important, as revealed by studies of other material combinations. The resulting electrochemistry establishes the basis for a remarkably simple procedure for printing highly conductive (3 × 10⁵ S m^?1) features in degradable materials at ambient conditions over large areas, with key advantages over strategies based on liquid phase (fusion) sintering that requires both oxide‐free metal surfaces and high temperature conditions. Demonstrations include printed magnetic loop antennas for near‐field communication devices.