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LI Zhihui XIONG Baiqing ZHANG Yong 'an ZHU Baohong WANG Feng LIU Hongwei 《稀有金属(英文版)》2007,26(3):193-199
The effects of the two-step ageing parameters (temperature and time) on the mechanical properties and electrical conductivity of 7B04 (A1-Zn-Mg-Cu) pre-stretched thick plates were studied. The results reveal that the initial T1 ageing contributes a major increase of the tensile strength, and the 0.2% proof stress value reaches 482 MPa after ageing for 7 h at 115℃. Behavioral differences in the tensile properties of the alloy after the two-step ageing treatment were less with the first-step ageing at 115~C for different time periods (7, 14, and 21 h). The effects of the second ageing parameters on the properties and microstructure of the 7B04 alloy were remarkable. TEM analysis of the samples aged at Temper I (7 h at 115℃ + 12 h at 160℃) and Temper II (7 h at 115℃ + 16 h at 165℃) indicates that two kinds of phases, i.e. 11' and 11 phases, precipitate from the matrix and efficiently improve the tensile strength of the alloy, and the grain boundary precipitates are coarse and discrete. There are obvious precipitate free zones (PFZs) along the grain boundary in the microstructure of the alloy after the two-step ageing treatment. 相似文献
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Solution and aging treatments are important approaches to improve mechanical properties and microstructure of aluminum-base alloys. In this research, a new type high strength AI-Cu-Si-Mn cast alloy was prepared. The effect of different solution and aging treatment temperatures on microstructure and mechanical properties of the AI-Cu-Si-Mn cast alloy were studied by means of microstructure observation and mechanical properties testing. Results showed that after solution treated at different temperatures for 12 h and aged at 175 ℃ for 12 h, with the increase of the solution temperature, both the tensile strength and the elongation of the alloy firstly increase and then decrease, and reach their peak values at 530 ℃. When the solution temperature is below 530 ℃, the microstructure of the alloy consists of a phase, undissolved e phase and T phase; while when it exceeds 530 ℃, the microstructure only consists of cr phase and T phase. After solution treated at 530 ℃ for 12 h and aged at different temperatures for 12 h, both the tensile strength and the elongation of the alloy firstly increase and then decrease with the increasing of temperature, and reach their peak values at 175 ℃. Therefore, the optimal heat treatment process for the alloy in this study is 12 h solution at 530 ℃ and 12 h aging at 175 ℃, and the corresponding tensile strength is 417 MPa, elongation is 4.0%. 相似文献
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Single-aging characteristics of 7055 aluminum alloy 总被引:3,自引:0,他引:3
The microstructures and properties of 7055 aluminum alloy were studied at different single-aging for up to 48 h using hardness test, tensile test, electrical conductivity measurement, XRD and TEM microstructure analysis. The results show that at the early stage of aging, the hardness and strength of the alloy increase rapidly, the peak hardness and strength are approached after 120 ℃ aging for 4 h, then maintained at a high level for a long time. The suitable single-aging treatment of 7055 alloy is 480 ℃, 1 h solution treatment and water quenching, then aging at 120 ℃ for 24 h. Under those condition, the tensile strength, yield strength, elongation and electrical conductivity of the studied alloy are 513 MPa, 462 MPa, 9.5% and 29%(IACS), respectively. During aging, the solid solution decomposes and precipitation occurs. At the early aging stage of 120 ℃, GP zones form and then grow up gradually with increasing ageing time. η′ phase forms after ageing for 4 h and η phase starts to occur after 24 h aging. 相似文献
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Continuing the effort to redesign IN718 alloy in order to provide microstructural and mechanical stability beyond 650 ℃, IN718 alloy was modified by increasing the Al, P and 13 contents, and the microstructure and mechanical properties of the modified alloy were compared with those of the conventional alloy by SEM and TEM. The precipitation of the grain boundaries of the two alloys is different. The Cr-rich phase, Laves phase and α-Cr phase are easily observed in the modified alloy. The γ" and γ' phases in the modified alloy are precipitated in a "compact form". The tensile strengths of the modified alloy at room temperature and 680 ℃ are obviously higher than those of the conventional one. The impact energy of the modified alloy is only about half of that of the conventional alloy. Ageing at 680 ℃ up to 1000 h lowers the tensile properties and impact energy of both the conventional and modified 718 alloys, except increasing the ductility at 680 ℃. It is concluded that the modified alloy is more stable than the conventional one. 相似文献
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The effect of stress on the microstructure and properties of an Al-Cu-Mg-Ag alloy under-aged at 165 ℃ for 2 h during thermal exposure at 200 ℃ was investigated. The tensile experimental results show that the remained tensile strength of both specimens at room temperature after being exposed at 200 ℃ with and without applying stress rises firstly, and then drops with the increasing of exposure time. The peak value of the remained strength reaches 439 MPa for non-stress-exposure for 10 h, and 454 MPa after being exposed with stress loaded for 20 h at 220 MPa. The elongation change is similar to that of strength. After being exposed for 100 h, specimen exposed at 220 MPa still remains a tensile strength of 401 MPa, larger than that exposed without applying stress. TEM shows that the microstructure of under-aged alloy is dominated by Ω phase mainly and a little θ′ phase. The θ′ and Ω phases are believed competitive with increasing exposure time. The width of precipitation free zone(PFZ) increases and the granular second phase precipitates at grain-boundary correspondingly. It is shown that the mechanical properties of alloy decrease slightly and present good thermal stability after thermal exposure at 200 ℃ and 220 MPa for 100 h. 相似文献
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The effect of stress on the microstructure and properties of an Al-Cu-Mg-Ag alloy under-aged at 165℃ for 2 h during thermal exposure at 200℃ was investigated. The tensile experimental results show that the remained tensile strength of both specimens at room temperature after being exposed at 200℃ with and without applying stress rises firstly, and then drops with the increasing of exposure time. The peak value of the remained strength reaches 439 MPa for non-stress-exposure for l0 h, and 454 MPa after being exposed with stress loaded for 20 h at 220 MPa. The elongation change is similar to that of strength. After being exposed for 100 h, specimen exposed at 220 MPa still remains a tensile strength of 401 MPa, larger than that exposed without applying stress. TEM shows that the microstructure of under-aged alloy is dominated by Ω phase mainly and a little θ' phase. The θ and Ω phases are believed competitive with increasing exposure time. The width of precipitation free zone(PFZ) increases and the granular second phase precipitates at grain-boundary correspondingly. It is shown that the mechanical properties of alloy decrease slightly and present good thermal stability after thermal exposure at 200 ℃ and 220 MPa for 100 h. 相似文献
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You Zhi-yong Jiang Ao-xue Duan Zhuang-zheng Qiao Gang-ping Gao Jing-lei Guo Ling-bing 《中国铸造》2020,17(3):219-226
Semi-solid AZ91D magnesium alloy billets were prepared by near-liquidus heat holding. Semi-solid squeeze casting was conducted at 575, 585 and 595 ℃, respectively, with 1 mm·s~(-1) squeeze speed. The semisolid squeeze casting AZ91D samples were heat treated by T4(solution at 415 ℃ for 24 h) and T6(solution at 415 ℃ for 24 h + 220 ℃ for 8 h) processes, respectively. The microstructure and mechanical properties of the alloy in different states were investigated by means of OM, SEM and tensile testing machine. The results show that compared to as-cast alloy, the grain size of the semi-solid squeezed AZ91D decreased significantly, and with the increase of semi-solid squeeze temperature, the grain size of AZ91D increased. The grains of the alloy were refined by T4 treatment, and further refined by T6 treatment. T6 treatment greatly improved the tensile strength, elongation, and hardness, but did not significantly improve yield strength. After 575 ℃ squeeze casting and T6 treatment, the ultimate tensile strength(UTS) reached 285 MPa, the elongation reached 13.36%, and the hardness also reached the maximum(106.8 HV), but the yield strength(YS) was only 180 MPa. During the process of semi-solid squeeze casting and heat treatment, the matrix grain was refined and a large number of precipitated and secondary precipitated phases of Mg_(17)Al_(12) appeared. Both the average size of matrix grain and secondary precipitated phase decreased, while the volume fraction of secondary precipitated phase increased. All these resulted in high tensile strength, elongation and hardness. 相似文献
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The effects of aging on mechanical properties,intergranular corrosion and exfoliation corrosion behaviors of a 2197 type A1-Li alloy were investigated,and the mechanisms were studied through microstructure observation and electrochemical measurement of simulated bulk phase.The main strengthening precipitates of the alloy aged at175 ℃ and 160 ℃ are δ' and T1.T1 precipitation in the alloy aged at 160 ℃ is delayed,which results in its slower age strengthening and over-aging behavior than the alloy aged at 175 ℃.Meanwhile,aging temperature of 160 ℃causes more uniform distribution and finer size of T1,resulting in its better strengthening effect.As aging time and aging temperature are increased,the size of T1 at grain boundaries and the width of PFZ along grain boundaries are increased,leading to an increase in the susceptibility to intergranular corrosion and exfoliation corrosion.It is suggested that better comprehensive properties can be obtained when the alloy is aged at 160 ℃. 相似文献
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ZHANG Ju-mei JIANG Bai-ling WANG Zhi-hu YUAN Sen NAN Hong-qiang LUO Hong-bin 《中国铸造》2007,4(4):296-299
The microstructure and mechanical properties of AZ80 magnesium alloy after solid solution and aging treatments were studied by using optical microscope (OM), X-ray diffraction (XRD), scanning electron microscopy(SEM) as well as tensile testing. The results indicated that β-Mg17Al12 phase was getting to distribute discontinuously along the grain boundary after treated at 395℃ ageing for 12 h followed by water-cooling, but it did not dissolve into α-Mg completely. The residual β-Mg17Al12 phase distributed along the grain boundary and had block-like or island shapes. The size of α-Mg was getting to be coarsening but not significantly. The β-Mg17Al12 precipitates appeared in discontinuous and continuous patterns from supersaturated α-Mg solid solution after aged at 200℃. The precipitation patterns were associated with the aging time essentially. The tensile strength and elongation of the alloy increased significantly but the hardness and yield strength decreased after solid solution treatment. However, with the prolonging of aging time, the hardness and strength of alloy increased while the ductility decreased. 相似文献
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《中国铸造》2015,(4)
The microstucture,mechanical properties and fracture behaviors of semi-continuous cast Mg-8Gd-3Y-0.5Zr(wt.%,GW83K) alloy after different heat treatments were investigated.Almost all the eutectic compounds were dissolved into the matrix and there was no evident grain growth after optimum solution treatment at 500 ℃for 4h.Further ageing at low temperatures led to significant precipitation hardening,which strengthened the alloy.Peak-aged at 200 ℃,the alloy had the highest ultimate tensile strength(UTS) and lowest elongation at 395 MPa and 2.8%,respectively.When aged at 225 ℃ for 15 h,the alloy exhibited prominent mechanical performance with UTS and elongation of 363 MPa and 5.8%,respectively.With regard to microstructure and tensile properties,the processes of 500 ℃,4h+225℃,15 h are selected as the optimal heat treatment conditions.The alloy under different conditions shows different fracture behaviors:in the as-cast alloy,a quasi-cleavage pattern is observed;after solution treatment,the alloy exhibits a trans-granular quasi-cleavage fracture;after being peak-aged at 200 ℃ and 225 ℃,the fracture mode is a mixed mode of trans-granular and intergranular fracture,in which the inter-granular mode is dominant in the alloy peak-aged at 200 ℃. 相似文献
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文化维度的大学师生关系论 总被引:3,自引:0,他引:3
大学师生关系在本质上是一种特殊的文化关系,从文化维度来考察大学师生关系不仅可以对大学师生关系的本质和规律有更清晰的认识,同时为建构和谐的现代大学师生关系提供了新的认识论和方法论基础.大学师生关系的和谐,有赖于大学师生文化价值体系的重建、教师文化霸权的自觉消解和学生正确"文化生态位"的确立. 相似文献
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Bioleaching: A microbial process of metal recovery; A review 总被引:1,自引:0,他引:1
Debaraj Mishra Dong-Jin Kim Jong-Gwan Ahn Young-Ha Rhee 《Metals and Materials International》2005,11(3):249-256
The present review describes the historical development and mechanisms of bioleaching. Recent development has shown commercial
application of the process and, concurrently, details pertaining to the key microorganisms involved in these processes have
been described. Bioleaching of metal sulfides is caused by diverse groups of bacteria. The dissolution biochemistry signifies
two types of pathways, which are specifically determined by the acid-solubility of the sulfides, the thiosulfate and polysulfate
pathways. This sulfide dissolution can be affected by ‘direct’ and ‘indirect’ mechanisms. In the ‘indirect’ mechanism bacteria
oxidize only dissolved iron (II) ions to iron (III) ions and the latter can then attack metal sulfides and then be reduced
to iron (II) ions. The ‘direct’ mechanism requires the attachment of bacteria to the sulfide surfaces. In the case of thiobacilli,
bacteria secrete exopolymer that facilitates attachment of the bacteria to a metal surface, thus enhancing the leaching rate.
In terms of eco-friendliness and process economics, within the field of biohydrometallurgy the technology is considered robust. 相似文献
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翟昕 《有色金属再生与利用》2008,(6):66-69
智利以铜著称,是中国铜业关注的地方。尽管北京与智利首都圣地亚哥的距离是全球各国首都之间最远的两个点,但还是有一批又一批的考察团远渡重洋来到这个神秘的国度。 相似文献
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