半固态触变成形AZ91D镁合金卫星角框件

通过对等径道角挤压处理后的AZ91D镁合金坯的触变成形试验，并借助于金相显微镜、Instron材料拉伸试验机等分析手段，对AZ91D镁合金卫星角框件的半固态触变成形工艺进行了研究。研究结果表明：当坯料加热温度为560℃，保温时间为20min，模具预热温度为400℃，保压时间为40s时，强度可达到292MPa，伸长率达到4．8％；触变成形对材料微观组织的影响主要表现为较明显的固液相分离现象，而对制件晶粒形状的影响比较小，在成形过程中，坯料的流动方式是以液相包裹球状固相颗粒的方式进行的；通过固溶处理和自然时效可以提高触变成形后的卫星角框件的强度；当固溶时间为6h，强度提高幅度在10％以上。     

金属半固态触变压铸工艺的探讨

结合金属半固态加工技术的特点,通过与传统液态压铸技术的比较,分析了半固态触变压铸的工艺过程、充型机理及工艺要素.同时对半固态压铸模具及压射系统的改进也进行了讨论,给出了选用半固态压铸机的一般流程.     

半固态AZ91D镁合金触变特性研究

在自行设计的Couette型同轴双桶流变仪上对半固态AZ91D镁合金浆料的触变性能进行了研究,结果表明半固态AZ91D浆料经等温静置后,表观粘度升高,然后在剪切作用下逐渐降低,最后达到一个稳态值,呈现出典型的剪切变稀特性;在相同剪切速率下,随静置时间的延长,半固态AZ91D合金浆料在随后的剪切作用下表观粘度达到稳态所用时间随之延长,同时稳态表观粘度也相应增大,这主要是由于静置过程中固相颗粒发生了合并;在剪切速率和静置时间相同时,随固相率的增加,半固态AZ91D合金浆料达到稳态所需时间也随之增加;在相同固相率和静置时间下,随剪切速率的增大,半固态AZ91D合金浆料的稳态表观粘度随之降低,同时达到稳态粘度所需时间也随之减小.     

时效处理对触变成形AZ91D镁合金组织和力学性能的影响

研究了固溶时效处理(T6)对触变成AZ91D合金组织演变的影响及组织与性能之间的关系。结果表明，触变成形AZ91D合金具有明显的时效硬化特征，分布在基体品界处的β相的数量、大小和形态与合金的力学性能有密切的关系。T6处理能明显提高合金抗托强度、屈服强度与硬度．T6处理后的合金的σb=212MPa，σ0.2=122MPa，硬度为83HV；并且热处理后的断口呈现明显的解理断裂特征。     

半固态镁合金触变成形数值模拟及试验验证

利用DEFORM-3D塑性有限元软件,对半固态AZ61触变成形过程进行了数值模拟,分析了半固态坯料与常规态坯料成形过程中的应力、应变分布和温度场,并对此两种坯料进行了触变锻造试验.结果表明,半固态镁合金材料具有变形抗力小,应力、应变分布均匀,通过对触变锻造试验和模拟结果的对比可知,二者拟合较为理想.     

镁合金半固态压铸触变成形技术的研究与进展

介绍了镁合金半固态触变成形技术中的三个关键技术：非枝晶组织半固态浆料的制备、坯料的二次加热、半固态触变压铸成形.并综述了镁合金半固态压铸触变成形技术的研究现状和发展前景.     

高固相率半固态镁合金触变成形数值模拟

对高固相率半固态镁合金触变成形过程进行数值模拟,分析了成形过程中的应力、应变分布和温度场,对比了半固态坯料与常规态坯料成形的特点.结果表明,半固态镁合金材料具有变形抗力小,应力、应变分布均匀的特点,材料流动性、充填性能优于常规坯料,能够一次成形复杂形状零件.数值模拟为半固态成形工艺参数的优化起到很好的参考作用.     

成形参数对AZ91D镁合金触变成形性与缺陷形成的影响

研究了不同成形工艺参数,如坯料加热温度、加热时间和模具预热温度(模具温度)对AZ91D镁合金触变成形性与缺陷形成的影响。结果表明:成形性、缺陷形成与加工参数紧密相关。合适的成形参数为:坯料加热温度在575～595℃,加热时间超过75min,模具预热温度超过275℃;主要有冷隔、液相偏析、缩松、裂纹和氧化夹杂5种缺陷。其中,裂纹和氧化夹杂是主要的缺陷。     

成形参数对AZ91D镁合金触变成形性与缺陷形成的影响

研究了不同成形工艺参数，如坯料加热温度、加热时间和模具预热温度（模具温度）对AZ91D镁合金触变成形性与缺陷形成的影响。结果表明：成形性、缺陷形成与加工参数紧密相关。合适的成形参数为：坯料加热温度在575～595℃，加热时间超过75min，模具预热温度超过275℃；主要有冷隔、液相偏析、缩松、裂纹和氧化夹杂5种缺陷。其中，裂纹和氧化夹杂是主要的缺陷。     

AZ91D镁合金的触变成形及其磨损性能的研究

研究了加热时间和模具预热温度对AZ91D镁合金触变成形性、组织和磨损性能的影响。结果表明，适合AZ91D镁合金触变成形的最佳加热时间为90min(在585℃)，模具预热温度为350℃；在此工艺条件下，初生相颗粒较圆整、粒度较小，组织最致密，相应地，其耐磨性也最好；与金属型铸造相比，触变成形显著地减少了缩松，因而，也明显地提高了耐磨性。     

Study on a semi-solid rheo-diecasting process with AZ91D alloy slurry

In this paper, a rheo-diecasting process of AZ91D alloy semi-solid slurry produced with a twin-screw stirring mixer was investigated. The results show that the tensile strength and elongation of the sample made by rheo-diecasting were 37% and 44% higher, respectively, than those produced by conventional liquid diecasting. The castings fabricated by rheo-diecasting possessed good density with low shrinkage and could be heat treated. It is a “near-net shape” production process.     

Thixotropic behavior of semi-solid AZ91D magnesium alloy

The thixotropie behavior of semi-solid AZ91D slurry was studied through a Couette type viseometer.The results show that the apparent viscosity of semi-solid AZ91D magnesium alloy slurry increases after being isothermally held, but the apparent viscosity quickly falls down to a steady state value after being stirred again and it takes on a sharp shear-thinning behavior. With the same shearing rate and the rest time increasing, the steady apparent viscosity increases because of the agglomeration of the solid particles, and the time required for the slurry to reach the steady state also becomes longer. If the solid fraction increases, it takes longer time for the slurry to reach the steady apparent viscosity with the same shearing rate and the same rest time. If the solid fraction and the rest time are the same, but the shearing rate rises, it takes shorter time for the slurry to reach the steady apparent viscosity and the final steady apparent viscosity also decreases.     

Microstructure of electromagnetic stirred semi-solid AZ91D alloy

The microstructures of semi-solid AZ91D alloy stirred by rotationally electromagnetic field were studied.The shape of primary α-Mg phase is dendrite under conventional solidification condition and the primary α-Mg grains are changed to the fine rosette-like or granular grains under electromagnetic stirring condition. If the electromagnetic stirring frequencies are low, there are a large amount of fine rosette-like primary α-Mg grains and the fine rosettelike primary α-Mg grain in two dimensions belongs to a single grain in three dimensions; there are also many spherical primary α-Mg grains, they may belong to a single grain in three dimensions and the orientation differences of the grains between them are very small. If the electromagnetic stirring frequencies are high, a lot of the fine rosette-like primary α-Mg grains disappear and are converted into granular grains, and moreover, most of these granular grains belong to different grains in three dimensions.     

半固态AZ91D镁合金压铸过程的数值模拟

采用机械搅拌方式研究了半固态AZ91D合金的流变特性,并根据实验数据,拟合出剪切速率为238s-1时,半固态AZ91D合金的固相体积分数和表观粘度之间的关系式。从流体力学的角度,采用数值技术对半固态AZ91D镁合金的压铸过程进行了研究。数值模拟结果表明,半固态浆料温度为550℃、模具温度为300℃、压铸速度为1m/s时,该文所设计的压铸件的压铸过程能很好地进行。同时,该研究工作能为分析压铸成形过程提供有益的信息。     

AZ91D镁合金半固态触变成形的数值模拟

采用商业有限元软件DEFORM3DTM对半固态镁合金AZ91D的触变成形过程进行了数值模拟,并利用自制的模具,在加热到570℃保温不同时间的情况下,对AZ91D镁合金半固态坯料进行触变成形试验。通过模拟分析的结果与试验的实际结果进行对比,得出了最佳触变成形工艺参数,同时,在一定程度上验证了数值模拟分析结果的可靠性。     

Numerical and experimental investigations of semi-solid AZ91D magnesium alloy in thixoforming process

Many complicated factors affect thixoforming fluidity in thixoforming process of semi-solid metal (SSM). So, it is important to forecast the flow property of SSM. Rigid visco-plastic constitutive model of semi-solid AZ91D Mg alloy was established at different strain rate. The thixoforming process of semi-solid AZ91D Mg alloy was simulated using commercial finite element software DEFORM-3D™. The fluid and effective stress–strain fields in the thixoforming process were obtained and the relationships among stress, strain rate and temperature also were analyzed. The thixoforming experiments were performed at 570 °C with different holding time. Finite element analysis results were compared with experimental ones, and experimental data has good agreements with the simulation results.     

半固态镁合金AZ91D变形行为研究

对应变诱发法制得的半固态镁合金AZ91D坯料进行了单向压缩实验,研究了不同工艺参数对半固态镁合金的压缩流变应力的影响。流变应力不仅是变形量和变形温度的函数,而且是应变速率的函数,由此采用回归分析法建立了能综合反映热力参数对流变应力影响的半固态AZ91D合金的粘塑性本构方程,为半固态触变成形的数值模拟奠定了理论基础。     

Reheating microstructure of refined AZ91D magnesium alloy in semi-solid state

By means of equal channel angular extrusion (ECAE) test, upsetting test and metalloseope, reheating mierostruetures of raw casting ingots, materials prepared by SIMA and materials extruded by ECAE in semi-solid state were investigated. The results show that compared with those of raw casting ingots and materials prepared by SIMA, reheating microstrueture of materials extruded by ECAE is the best and the final grain size is the finest. With increasing holding time, a growing phenomenon occurs in reheating microstrueture of materials extruded by ECAE, which can be described by Ostwald ripening law. The average grain size increases firstly, subsequently decreases and the shape factor of grains approaches to 1 as the reheating temperature increases. With increasing equivalent strain, the average grain size decreases. This demonstrates that reheating material extruded by ECAE technology is a good method to prepare AZ91D magnesium alloy semi-solid billets.     

Development of anodic film on Mg alloy AZ91D

At constant applied current, the evolution of morphology, structure and composition of anodic film on Mg alloy AZ91D with anodizing time was investigated using SEM, EDX and XRD. The development of anodic film on the Mg alloy was similar to that on high-purity Mg except that, attributed to alloying effect, hunch-like resultants replaced volcano-like ones to become predominant initial products at transitional stage of anodization. The black cicatrices at the anode surface were related with the inhomogeneous activation and dissolution under strong polarization conditions. The evolution of micropores in shape, size and number was associated with anodizing mechanism. The main elements in anodizing products were Mg, O, Al and Si, indicating that both alloy substrate and electrolyte solution were involved in anodization. Anodic film developed early was mainly comprised of periclase MgO and forsterite Mg₂SiO₄. However, amorphous compounds became dominant with treatment time increasing. In anodizing products, the element Al existed primarily in the form of amorphous compound.     

应变诱发AZ91D镁合金半固态组织形态及形成机理

采用应变诱发方法制备了AZ91D镁合金半固态材料。考察了变形率、温度、保温时间对固相体积分数、组织形态以及晶粒尺寸的影响。结果表明：在冷变形条件下.于570℃保温一定时间后。可制备出固相体积分数最小达55％的镁合金半固态材料。分析讨论了AZ91D镁合金半固态组织的形成机理。在热处理过程中，组织发生再结晶，而冷变形程度对再结晶的组织有显著影响。