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1.
SiC_p/Cu梯度复合材料热疲劳性能研究   总被引:1,自引:0,他引:1  
采用粉末冶金方法制备了4种SiC颗粒呈渐变分布的梯度复合材料,应用扫描电子显微镜、X射线衍射仪、自动显微硬度计等,研究了梯度复合材料的显微组织、硬度分布和热疲劳性能。结果表明,SiCp/Cu梯度复合材料基体连续,梯度层过渡均匀,显微组织及硬度呈梯度分布;梯度复合材料的SiC颗粒渐变过渡越均匀,梯度复合材料抗热疲劳性能越好。  相似文献   

2.
SiCP/Al复合材料的显微结构分析   总被引:2,自引:1,他引:1  
采用粉末冶金+热挤压工艺制备SiCp/Al复合材料,测定其力学性能。利用X射线衍射分析复合材料物相的组成,用金相显微镜、扫描电镜和透射电镜分析其微观组织结构。结果表明,SiC颗粒在铝基体中分布比较均匀,SiC颗粒与基体结合良好;基体主要是α-Al,强化相β-Mg2Si和弥散相(Fe,Mn,Cu)3Si2Al15(体心立方结构,晶格常数1.28nm);SiCp/Al界面则为Al和Mg元素扩散到SiC表面的SiO2层形成的20nm-30nm无定形层;复合材料的断裂机制主要是SiC颗粒断裂和SiCp/Al界面塑性撕裂:复合材料在变形过程中,SiC颗粒可阻止裂纹的扩展。  相似文献   

3.
SiC_P/Cu梯度复合材料的制备及性能研究   总被引:4,自引:4,他引:0  
采用粉末冶金方法制备了SiCP/Cu均质复合材料及梯度复合材料,并对复合材料的显微组织、硬度、导电率和耐磨性进行了研究。结果表明:均质复合材料中SiC颗粒含量越多,导电率越小,耐磨性越好;梯度复合材料基体连续,组织及硬度呈梯度分布且其耐磨性优于基体Cu材料;磨损机理是微切削磨损和磨粒磨损的复合作用。  相似文献   

4.
采用挤压铸造技术制备硅酸铝短纤维增强铝硅合金梯度复合材料,研究了这类材料的凝固组织和基本热物理性能。结果表明,在复合材料中,基体组织细小,纤维与基体结合良好,并呈梯度状无序分布;梯度复合材料的热物理性能优异。  相似文献   

5.
采用粉末冶金和喷射沉积方法制备了Al及Al/SiCp复合材料,测试了材料的力学性能,利用金相显微镜和扫描电镜观察了材料的断裂行为。结果表明,Al/SiCp复合材料的强度比基体材料的高,但塑性低。粉末冶金方法制备的Al/SiCp复合材料与喷射沉积方法制备的比较,前者组织更致密,强度更高,塑性更好,断裂是SiC颗粒开裂,裂纹的传递主要沿颗粒中形成的裂纹扩展;后者断裂主要表现为SiC颗粒从基体中拔出,裂纹的传递大多是SiC颗粒周围形成的裂纹在基体中扩展。  相似文献   

6.
李微  陈振华  陈鼎  滕杰 《金属学报》2011,47(1):102-108
采用紧凑拉伸试样进行恒载和降K控制的拉--拉疲劳实验, 研究了喷射沉积SiCp/Al-7Si复合材料及其基体的疲劳裂纹扩展行为. 通过金相显微镜和扫描电镜观察了复合材料及其基体的组织和疲劳裂纹扩展形貌, 研究了SiC颗粒对复合材料疲劳裂纹扩展机制的影响. 结果表明: 复合材料在任何相同的ΔK水平下其抗疲劳裂纹扩展能力优于基体材料, 并表现出较高的疲劳门槛值. 其原因是复合材料中裂纹裂尖遇到增强颗粒时, 裂纹发生偏转, 特别是SiC颗粒自身微裂纹萌生有效降低了裂纹尖端的应力强度因子, 复合材料的裂纹闭合效应也随之增大. 去除裂纹闭合效应的影响, 当有效应力因子ΔKeff作为裂纹扩展的驱动力时, 复合材料的裂纹扩展速率却高于基体.  相似文献   

7.
开展了粉末冶金法制备的20%SiC_p/2009Al复合材料坯锭的等温锻造实验,通过金相观察、扫描电镜(SEM)、拉伸和断裂韧性测试等方法研究了不同变形量对锻件微观组织和力学性能的影响。结果表明,随着等温锻造变形量的增大,SiC颗粒分布更加均匀,锻件的强度和塑性显著提高。通过SEM对材料断裂韧性裂纹扩展路径观察发现,主裂纹扩展发生在SiC颗粒偏聚区域的铝基体中。复合材料的断裂方式为以基体韧性断裂和增强体脆性断裂这2种方式为主。  相似文献   

8.
Al2O3sf/ZL109复合材料的热疲劳短裂纹的扩展行为   总被引:9,自引:0,他引:9  
在室温至280℃间热循环条件下,研究了体积百分含量18%的氧化铝短纤维增强ZL109铝-硅合金复合材料和基体ZL109铝-硅合金的热军短裂纹扩展行为,并且探讨和复皮劳裂纹的形成机制和扩展过程。研究结果显示,短裂纹扩展阶段,热疲劳裂纹与增强体纤维有明显的交互作用,但复合材料的皮劳短裂纹扩展速率比基体合金的大,加强基体与纤维的界面结合,提高纤维质量,可望提高复合材料的热疲劳裂纹扩展抗力。  相似文献   

9.
为了研究激光沉积TC4/TC11钛合金梯度材料的组织与疲劳性能,采用激光沉积制造技术制备两种不同过渡方式的TC4/TC11复合材料。观察不同过渡方式复合材料的显微组织,测试两种复合材料分别在550Mpa和800Mpa下的疲劳性能,并对疲劳断口进行分析。结果表明,相比直接过渡的复合材料,具有3层过渡层梯度材料的显微组织过渡界面不明显,过渡区组织结合紧密;具有3层过渡层的梯度材料在两种应力下的疲劳寿命均比直接过渡的高,低应力下相对提高了129.3%,高应力下相对提高了81.8%;直接过渡复合材料在裂纹扩展时沿着α片层集束开裂,滑移面较大,疲劳寿命较低;具有3层过渡层的梯度材料,裂纹扩展沿着单个α片层滑移开裂,滑移面小,裂纹扩展路径比较曲折,疲劳寿命高。  相似文献   

10.
梯度复合材料活塞的挤压铸造研究   总被引:1,自引:1,他引:0  
陶瓷梯度增强铝基复合材料是发动机活塞的理想增强材料。采用挤压铸造法制造出梯度复合材料活塞,对梯度 复合材料的层间结合的显微组织进行了观察,发现复合材料之间、复合材料与基体之间的结合情况非常令人满意。采用 ANSYS有限元分析软件,对梯度复合材料活塞的隔热效果进行了分析,分析结果显示隔热度提高了8.7%。  相似文献   

11.
Fatigue crack retardation with infiltrated SiC paste into a crack is examined in low carbon structural steel. Two different sizes of SiC powders, whose average diameters are 15 and 53 μm, are used. The SiC powder mixed with oil is infiltrated into a through thickness fatigue crack from the crack mouth. Fatigue crack growth retardation is examined by the ΔK increasing test of R = 0.1, comparing with the base plate property, where ΔK is stress intensity factor range and R is stress ratio. Crack growth is retarded just after infiltrating SiC paste into the crack mouth, and the deceleration of crack growth rate to 1/50 of the base plate appears in the maximum. It is revealed that this crack retardation behaviour results from the crack closure induced by the wedge effect of the SiC particle into a crack. The crack retardation effect is investigated with several combinations of SiC particle size and cyclic stress conditions. The crack growth rate, da/dn and stress intensity factor, Kcl for the crack closure depend on both the maximum stress intensity factor, Kmax, and the stress ratio, R. While the better retardation effect can appear in the higher Kmax and the higher R ratio, it disappears in the R ratio over 0.7. The SiC paste with 15 μm powder brings the crack retardation effect in the wider cyclic stress condition more stable than in the SiC paste with 53 μm powder.  相似文献   

12.
Pardo  A.  Merino  M.C.  López  M.D.  Escalera  M.D.  Viejo  F. 《Oxidation of Metals》2003,59(1-2):1-21
A study was made on the influence of the SiCp proportion and the matrix concentration of four composites (A360/SiC/10p, A360/SiC/20p, A380/SiC/10p, A380/SiC/20p) on their oxidation behavior. Gravimetric tests were used in a kinetics study of the corrosion process at different temperatures (350, 400, 450, and 500°C). The influence of corrosion on mechanical properties was evaluated by hardness measurements. The nature of corrosion products and the influence of the microstructure on the morphology and growth of the oxidation layer were analyzed by SEM and low-angle XRD. The extent of the damage due to oxidation for Al/SiCp composites increases with the SiCp concentration due to the increase of nucleation sites. One of these nucleation sites is in the interface region between the matrix and the particles. Oxidation was influenced more by the percentage of alloy elements in the matrix than by the proportion of SiCp reinforcement. The presence of Cu and Ni in the matrix favors the oxidation process through the formation of different intermetallic compounds.  相似文献   

13.
采用极性分散剂,在微米Al2O3基体中加入微米ZrO2和纳米SiC颗粒,用真空热压法制备出了Al2O3/SiC纳米复合陶瓷,并研究了微米ZrO2和纳米SiC的添加对Al2O3/SiC纳米复合陶瓷显微组织及其性能的影响.结果表明:与纯Al2O3比较,适量微米ZrO2和纳米SiC颗粒的加入阻碍了Al2O3晶粒的长大,使复合陶瓷的显微组织非常细小,纳米复合陶瓷烧结后的力学性能大大提高.  相似文献   

14.
The influence of silicon carbide (SiCp) proportion and matrix composition on four aluminium metal matrix composites (A360/SiC/10p, A360/SiC/20p, A380/SiC/10p, A380/SiC/20p) immersed in 1-3.5 wt% NaCl at 22 °C was investigated by potentiodynamic polarization. The kinetics of the corrosion process was studied on the basis of gravimetric measurements. The nature of corrosion products was analysed by scanning electron microscopy (SEM) and low angle X-ray diffraction (XRD). The corrosion damage in Al/SiCp composites was caused by pitting attack and by nucleation and growth of Al2O3 · 3H2O on the material surface. The main attack nucleation sites were the interface region between the matrix and the reinforcement particles. The corrosion process was influenced more by the concentration of alloy elements in the matrix than by the proportion of SiCp reinforcement and saline concentration.  相似文献   

15.
Al2O3/5%SiC nanocomposites were fabricated by pressureless sintering using MgO as a sintering aid and then post hot-isostatic pressed (HIP), which can subsequently break through the disadvantage of hot-pressing process. The MgO additive was able to promote the densification of the composites, but could not induce the grain growth of Al2O3 matrix due to the grain growth inhibition by nano-sized SiC particles. After HIP treatment, Al2O3/SiC nanocomposites achieved full densification and homogeneous distribution of nano-sized SiC particles. Moreover, the fracture morphology of HIP treated specimens was identical with that of the hot-pressed Al2O3/SiC nanocomposites showing complete transgranular fracture. Consequently, high fracture strength of 1 GPa was achieved for the Al2O3/5%SiC nanocomposites by pressureless sintering and post HIP process.  相似文献   

16.
Friction stir processing of AA6061-T4 alloy with SiC particles was successfully carried out.SiC particles were uniformly dispersed into an AA6061-T4 matrix.Also SiC particles promoted the grain refinement of the AA6061-T4 matrix by FSP.The mean grain size of the stir zone (SZ) with the SiC particles was obviously smaller than that of the stir zone without the SiC particles.The microhardness of the SZ with the SiC particles reached about HV80 due to the grain refinement and the distribution of the SiC particles.  相似文献   

17.
为制备基体相晶粒细小、增强相均匀分布的SiC/Al纳米复合涂层,以Al、SiC为原料,采用高能球磨法获得SiC颗粒弥散分布的纳米晶Al基复合材料粉末,利用冷喷涂技术低温成型制备了SiC/Al纳米复合涂层,分析了SiC含量对复合涂层相结构、晶粒尺寸、微观结构、硬度及磨损性能的影响规律。结果表明:冷喷涂可实现球磨纳米晶复合粉末结构的原位移植,所制备SiC/Al纳米复合涂层组织致密,微米及亚微米级SiC弥散分布在纳米晶Al(约80 nm)基体之上;SiC颗粒对Al基体有明显强化作用,冷喷涂SiC/Al纳米复合涂层的硬度随SiC体积分数的增加而显著增加,50% SiC/Al纳米复合涂层的硬度高达515 HV0.3,约为Al块材的13倍;冷喷涂SiC/Al纳米复合涂层的耐磨损性能随着SiC含量增加而显著提高,涂层磨损失效机制为磨粒对基体的切削犁沟变形。  相似文献   

18.
SiC颗粒增强铁基合金复合涂层的组织   总被引:1,自引:0,他引:1  
采用等离子堆焊—SiC后送粉技术制备了SiC颗粒增强铁基合金复合涂层,利用扫描电子显微镜(SEM)、X射线衍射仪(XRD)和能谱仪(EDS)对涂层的显微组织、相组成和元素分布进行了观察和测试。试验结果表明:SiC分布于马氏体基体上,原始形态保持完好,没有发生明显溶解,复合效果较好。SiC与基体界面层由预覆层、近基体区和絮状区构成。SiC边缘为CrSi2、CrSi3;近基体区耐腐蚀性相对基体较强,组织难以显示;絮状区由大量(Fe,Cr)7 C3、(Fe,Cr)23 C6碳化物和α-(Fe,Cr)固溶体组成。  相似文献   

19.
A SiC/2024 composite was made by semisolid casting.The wetting between SiC and Al matrix is improved by treating SiC particles at a high temperature,coating K2ZrF6,and adding Mg to the Al melt,An effective way to remove the gas around SiC particles was also found.Microstructures were observed under optical microscope(OM) and scanning electron microscopy(SEM).The results show that SiC particles and Al matrix are well bonded and no gaps or cavities around the particles are observed.SiC particles distribute homogeneously in the Al matrix.The existence of SiC particles results in the increase of wear resistance and strength.  相似文献   

20.
SiC纤维增强Ti基复合材料(SiCf/Ti)容易发生界面反应,从而影响其力学性能。开展界面反应和动力学的研究,对于SiCdTi复合材料的制备和服役具有指导意义。采用扫描电镜、透射电镜和X射线衍射分析了SICf/Ti-6Al—4V复合材料的界面反应及其动力学,发现SiC纤维的C涂层与Ti-6Al—4V反应形成粗晶粒的和细晶粒的TiC,长期高温热处理使得界面反应加剧,TiC层加厚,当C涂层完全消耗后,界面反应层中除了TiC外,还出现了Ti3SiC2。研究表明,界面反应层的加厚受元素扩散控制,服从抛物线规律,求出的动力学参数Q为268.8kJ/mol,k为0.0057m/s1/2。  相似文献   

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