GH2907合金热变形行为及热加工图

通过热模拟压缩实验研究了GH2907合金在变形温度为950~1100℃、应变速率为0.01~10s_^-1、变形量为60%条件下的热变形行为,流变应力随着变形温度的升高或应变速率的降低而显著降低；根据Arrhenius方程和Zener-Hollomon参数,计算了热变形激活能Q,建立了GH2907合金的热变形本构方程；根据动态材料模型,确定了GH2907合金在不同应变下的功率耗散图,功率耗散效率η较高的区域位于温度为1050~1100℃,应变速率为0.01~0.03s_^-1范围,在该变形区域内组织发生了明显的动态再结晶现象；基于Preased失稳判据,绘制了GH2907合金在不同应变下的热加工图,流变失稳区位于高温高应变速率区域,即温度为970~1100℃,应变速率为0.6~10s_^-1范围,在该变形区域内动态再结晶晶粒沿着绝热剪切带和局部流动分布。根据GH2907合金热加工图及微观组织分析得到适宜的加工区域是温度为1050~1100℃,应变速率为0.01~0.03s_^-1范围。     

Ti60合金的热变形行为及工艺参数优化

在变形温度600～950℃,应变速率0.001～10s_^-1条件下,采用Thermecmaster-Z型热加工模拟试验机对Ti60合金进行等温恒应变速率压缩实验。通过分析流动应力行为,计算应变速率敏感指数m和应变硬化指数n,并综合考虑加工图和变形微观组织来研究该合金的热变形行为,得到优化的工艺参数范围。研究结果表明,Ti60合金的流动应力-应变曲线在不同热力参数条件下分别呈现流动稳态型和流动软化型。应变速率敏感指数m随着变形温度升高和应变速率降低而增大。应变硬化指数n随着变形温度升高而减小；随着应变速率的增加在低应变速率(0.001～0.1s_^-1)区间增大,在高应变速率(1～10s_^-1)区间减小；随着应变的增加在高温段(800～950℃)的低应变速率(0.001～0.1s_^-1)区间较缓慢地减小,在高温段(800～950℃)的高应变速率(1～10s_^-1)区间以及低温段(600～750℃)的所有应变速率(0.001～10s_^-1)区间较明显地减小。Ti60合金存在两个功率耗散效率峰值区域,其对应的热力参数窗口分别为温度725～875℃,应变速率≤0.003s_^-1和温度875～938℃,应变速率≤0.04s_^-1。从流动应力行为、应变速率敏感指数m、应变硬化指数n以及加工图综合考虑,Ti60合金的最佳热加工工艺参数为：温度800～875℃,应变速率0.001～0.003s_^-1,或温度875～938℃,应变速率0.001～0.04s_^-1。     

低成本Ti-Al-V-Fe-O钛合金热变形行为及热加工图

通过真空非自耗熔炼炉制备了低成本Ti-6Al-2.5V-1.5Fe-0.15O合金,利用Gleeble-1500D热模拟机,研究了其热加工参数为：变形温度875℃-1100℃、应变速率0.001s_-1-1s_-1,变形量为70%时的热变形行为,建立了Ti-6Al-2.5V-1.5Fe-0.15O合金考虑应变量的Arrhenius本构方程,基于动态材料模型建立热加工图。研究结果表明：变形温度升高,应变速率降低,流变应力降低。通过本构方程计算可得两相区平均热激活能为398.824KJ/mol,远大于纯钛自激活能,表明热变形软化机制与动态再结晶有关。单相区热激活能为210.93KJ/mol,略大于纯钛自激活能,以动态回复为主。通过热加工图确定两个失稳区,中等变形温度(950℃-1070℃)高应变速率(0.31-0.1s_-1)易发生绝热剪切,结合热加工图确定适合的加工区间：应变速率为0.001-0.01s_-1,变形温度为875℃-925℃。     

Ti6242合金的热变形行为及加工图

利用Gleeble-3800对Ti6242合金进行热模拟压缩试验。研究了压缩量为60%、应变速率分别为0.01、0.1、1、10 s-1,变形温度分别是900、950、1000、1050、1100℃条件下试样的热变形行为。根据试验参数得出Ti6242合金本构方程,绘制Ti6242合金真应力-应变曲线,基于动态材料模型建立热加工图。结果表明,流变应力随着变形温度的升高而下降,随着应变速率的增加而升高,变形激活能Q=453.74 k J/mol,最佳热加工工艺为变形温度1000~1050℃应变速率0.1 s-1左右。     

基于MATLAB的Ti80合金热变形行为及热加工图

用热模拟试验机、光学显微镜、MATLAB软件研究了双态组织Ti80合金在变形温度860 ~ 1020 ℃、应变速率0.001 ~ 10 s_-1、最大变形量50%下的热变形和热加工特性。结果表明：Ti80合金为负温度敏感型、正应变速率敏感型材料,主要软化机制随温度的升高由动态再结晶转变为动态回复。利用MATLAB编程构建了应变补偿本构方程与热加工图,计算应力与试验应力的相关系数R=0.994、平均相对误差AARE=7.443%;合金最佳热加工工艺参数区间为：[980 ~ 1015 ℃]-[0.013 ~ 0.100 s_-1],该区峰值功率耗散系数h=64%。     

Cr微合金化低碳钢热变形行为

采用Gleeble-3500热模拟机对一种含微量合金元素Cr、Mn、Ti的低碳钢在变形温度700～1050℃.应变速率0.01～0.1s~(-1)条件下的热变形行为进行研究.结果表明:单相奥氏体区和铁索体区,峰值应力随变形温度的降低而升高,在两相区,峰值应力随着变形温度的降低而降低;在775～850℃与950～1050℃的温度区间,峰值应力的大小基本相当.建立了热加工图,并通过组织观察对其热加工图进行了解释.根据流变应力曲线,确定了试验低碳钢铁素体区的热变形激活能和热变形方程.     

变形态Ti40合金高温变形行为

在GLEEBLE热模拟试验机上对变形态Ti40合金进行热压缩实验,采用基于Prasad准则的加工图技术,研究变形态Ti40合金在变形温度950℃～1100℃、应变速率0.001s-1～1.0s-1范围内的微观变形机制和流变失稳现象,并优化该合金的高温变形参数。结果表明,失稳区出现在低温、高应变速率区,当变形温度为950℃～1010℃、应变速率0.13s-1～1.0s-1时,失稳区会出现局部流动,在实际热加工时应尽量避开这一参数范围;变形温度950℃～1100℃、应变速率0.001s-1～0.01s-1为较佳的变形参数范围,其变形机制以动态再结晶为主,伴随动态回复,最佳的变形参数位于温度1050℃、应变速率0.001s-1附近,该区域发生了完全动态再结晶;除失稳区和较佳变形区以外的区域,变形机制以动态回复为主,伴随动态再结晶,是可加工的区域。     

新型钛合金Ti-555热变形行为及热加工图研究

本文通过高温热压缩试验研究Ti-555钛合金热变形过程中变形温度、应变速率对流变应力的影响,采用Arrhenius双曲正弦函数模型推导出Ti-555本构方程,并依据动态材料模型建立了ε=0.6时的热加工图。结果表明,Ti-555钛合金流变应力对应变速率和变形温度较为敏感,热变形时随变形温度升高或应变速率降低,流变应力下降。根据热加工图确定了两个热加工安全区参数为(1)变形温度为850～950 ℃、应变速率为0.6～10 s_^-1;(2)变形温度为950～1150 ℃、应变速率为0.36～0.9 s_^-1。     

高强耐腐蚀Ti80合金的热变形行为及热轧板材的组织性能研究

通过热模拟实验研究Ti80合金热变形行为及组织演化规律,考察该合金的应力-应变曲线、加工硬化规律并建立该合金的热加工图。在此基础上,进行不同热轧工艺下的Ti80合金板材制备,研究其微观组织变化对力学性能的影响,探索Ti80合金具有最优力学性能的工艺条件。结果表明:Ti80合金的峰值应力和加工硬化率随着变形温度的升高以及变形速率的降低而减小,属于变形温度和应变速率敏感型合金。通过热加工图计算分析,温度在800～920℃、920～1050℃,应变速率在0.01～0.1 s-1范围内为最佳的稳定变形区。随着变形温度的升高,其微观组织经历由等轴组织、双态组织到层片组织的变化。同时,随着应变速率的升高,存在β转变组织形态的变化。对比分析Ti80合金不同热轧条件下的力学性能,初轧温度1060℃、终轧温度950℃时,显示为网篮组织+块状α相的混合组织形态,此时具有最优的强度和塑性性能,抗拉强度为881.6MPa,延伸率为11.27%,展现为韧性断裂。     

Ti1023合金锻造参数优化的基础研究

通过Ti1023合金等温压缩试验,得到不同高温变形条件下真应力-应变曲线和热加工图。通过加工硬化和动态软化效应分析了变形参数对Ti1023合金应力-应变曲线形态和峰值应力的影响。结果表明:在中低温区域和大应变速率条件下,变形参数对流动应力影响较大,高温区域和小应变速率对流动应力影响较小。通过对Ti1023合金热加工图的分析,发现合金的热变形能量分配主要受应变速率的影响。热加工图中主要存在两个变形失稳区和一个临界失稳区,失稳机制主要包括局部塑性流动和绝热剪切等。Ti1023钛合金的较优锻造区间为:变形温度760~780℃、应变速率5×10~(-4)~10~(-1)s~(-1)。     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

Three-Dimensional Growth of Coherent Ferrite in Austenite: A Molecular Dynamics Study

Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.     

Effect of Short-Time Aging on the Pitting Corrosion Behavior of a Novel Lean Duplex Stainless Steel 2002

The effect of short-time aging in the temperature range between 400 and 1000 °C on the pitting corrosion behavior and mechanical property of a novel lean duplex stainless steel(LDSS) 2002 was investigated through the potentiostatic critical pitting temperature(CPT) tests and the Charpy impact tests. Both the pitting corrosion resistance and the toughness of aged specimens degraded due to the precipitation of detrimental secondary phases and the most significant reduction of CPT and impact energy emerged at 650 °C concurrently. The CPT of LDSS 2002 specimen aged at 650 °C decreased by 28 °C, and the impact energy dropped from 69 to 29 J/cm~2 compared with the solution-annealed sample. Transmission electron microscopy characterization showed that the main precipitates in LDSS 2002 were Cr_2N and M_(23)C_6 along the ferrite–austenite grain boundaries.     

INTRODUCTION TO PATENTS

The invention provides a method of making a mold which can reduce SOx generation rate while preventing decrease in hardening rate in the case of using sulfuric acid for a hardener composition. The method has a mixture step in which fire-resistant particles, a hardener composition and a binder composition are mixed to obtain a composition for a mold. The hardener composition contains sulfuric acid. In the mixture step, sodium carbonate is added. A molar ratio of the sulfuric acid to the sodium carbonate is 0.5 or more and 4.0 or less.     

China Foundry Week 2014

China Foundry Week, hosted by the Foundry Institution of Chinese Mechanical Engineering Society （FICMES） each year, is a large academic event in China. It is one of the ten high-impact activities sponsored by the Chinese Mechanical Engineering Society.     

17th Conference of Hydrodynamic and Electromechanical Control Engineering Call for papers

正1.Contents In order to promote the academic exchanges and technical communication of the research in the field of fluid power transmission and control,fluid control engineering specialized committee of the Chinese Society of Theoretical and Applied Mechanics will hold the 17th Conference of Hydrodynamic and Electromechanical Control Engineering on July 27-29,2014 in Tibet,Lhasa city.     

Information for Contributors

正The Transactions of Nonferrous Metals Society of China,founded in 1991 and sponsored by The Nonferrous Metals Society of China,is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology,including mineral processing,extraction metallurgy,metallic materials and heat treatments,metal working,physical metallurgy,powder metallurgy,with the emphasis     

Preface

<正>We are pleased to present this Special Issue of Transactions of Nonferrous Metals Society of China containing selected papers from the First Asian Conference on Aluminum Alloys(ACAA-2013),held in Beijing,China,13–17 October 2013.This conference has been initiated,with approval of     

Information for Contributors

The Transactions of Nonferrous Metals Society of China, founded in 1991 and sponsored by The Nonferrous Metals Society of China, is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology, including mineral processing, extraction metallurgy, metallic materials and heat treatments, metal working, physical metallurgy, powder metallurgy, with the emphasis on fundamental science. It is the unique preeminent publication in English for scientists, engineers, under/post-graduates on the field of nonferrous metals industry. This journal is covered by many famous abstract/index systems and databases such as SCI Expanded, Ei Compendex Plus, 1NSPEC, CA, METADEX, AJ and JICST.     

Rheology Feature of Simple Metal Melt

The rheology feature of Sb, Bi melt and alloys was studied using coaxial cylinder high-temperature viscometer. The results showed that the curve of torsion-rotational speed for Sb melt presents a linear relation in all measured temperature ranges, whereas for the Bi melt, the curve presents obvious non-Newtonian feature within the low temperature range and at relative high shear stress. The rheology feature of Sb80Bi20 and Sb20Bi80 alloy melts was well correlated with that of Sb and Bi, respectively. It is considered that the rheology behavior of Sb melt plays a crucial role in Sb80Bi20 alloy and that of Bi melt plays a crucial role in Sb20Bi80 alloy.