Hamon 10 × 100 MΩ resistor based traceable source for calibration of picoammeters in the range 100 pA–100 nA

This paper describes a measurement method developed at National Institute of metrological Research (INRIM) to calibrate picoammeters in dc current from 100 pA to 100 nA. The current source is based on a traceable to the dc resistance national standard 10 × 100 MΩ Hamon resistor developed at INRIM and on a traceable to the dc voltage national standard high precision dc voltage calibrator. The expanded uncertainties of the method for the calibration of picoammeters span from 9.4 × 10⁻⁴ for the gain of a picoammeter at 100 pA to 4.0 × 10⁻⁴ for the gain at 100 nA. A detailed uncertainties budget at 10 nA level and the results of a comparison with a different technique are also reported.     

The influence of elastic strain on the early stages of decomposition in Cu–1.7 at% Fe

The initial stage of decomposition of homogenized Cu–1.7 at% Fe at 722 K was investigated by means of field ion microscopy (FIM), atom probe tomography (APT) and computer-assisted field ion image tomography (cFIIT). The agglomeration of atoms depending on time could be investigated and the growth of precipitates with a diameter of few nanometers was observed during ongoing nucleation.     

Construction of a standard force machine for the range of 100 μN–200 mN

A new force standard machine (FSM) for the range of 100 μN–100 mN has been developed [1]. The machine is based on the comparison of a force transducer with the indication of an electromagnetic compensated balance (ECB). Construction details as well as first measurements will be presented. To guarantee traceability to the established deadweight force machines, the new facility was compared with the PTB 200 N FSM.     

A traceable technique to calibrate dc current shunts and resistors in the range from 10 μΩ to 10 mΩ

A traceable to dc resistance and dc voltage National Standards measurement technique to calibrate dc current shunts and resistors in the range from 10 μΩ to 10 mΩ has been developed at National Institute of Metrological Research (INRIM) in addition to the primary reference system for low value resistors calibration. This technique is applicable in secondary and industrial metrological laboratories. It is based on a volt-amperometric method, to compare an unknown shunt with a standard one in 1:1 or 1:10 ratios. In the setup are involved: a dc current calibrator and a current generator to supply currents respectively up to 100 A and up to 1200 A, with a switch to reverse the current, two 7 1/2 digit nanovoltmeters (nVs) for the acquisition of the voltage on the standard and under calibration shunts and two Tinsley 100 μΩ and 1 mΩ standard shunts kept in mineral oil and with a cooling system. An optional variation in the procedure that can reduce the measurement uncertainties is discussed. The 2σ relative capabilities of the technique span from 6.0 × 10⁻⁶to 4.6 × 10⁻⁴. Compatibility results with the INRIM reference measurement system for low value resistors calibration are also given.     

Analysis of composition dependence of some thermal transport properties in glassy Se80−xTe20Snx (0 ⩽ x ⩽ 10) alloys using transient plane source measurements

In the present work, we have studied simultaneous measurements of thermal transport properties (effective thermal conductivity, diffusivity, specific heat per unit volume, thermal inertia I_T) of glassy Se_80−xTe₂₀Sn_x (0 ? x ? 10) system using their twin pellets. The glassy system is prepared under a load of 5 tons and measurements have been made at room temperature using Transient Plane Source (TPS) technique. The composition dependence of the thermal transport properties of given glassy system is also discussed.     

Computer simulation of a 1.0 GPa piston–cylinder assembly using finite element analysis (FEA)

The paper reports a preliminary study of the behavior of a high performance controlled-clearance piston gauge (CCPG) in the pressure range up to 1 GPa through finite elemental analysis (FEA). The details of the experimental characterization of this CCPG has already been published (Yadav et al., 2007 [1]). We have already pointed out that the use of Heydemann–Welch (HW) model for the characterization of any CCPG, has some limitation due to the fact that the linear extrapolation of the cube root of the fall rate versus jacket pressure (v^1/3–p_j) curve is assumed to be independent of the rheological properties of the pressure transmitting fluids. The FEA technique addresses this problem through simulation and optimization with a standard ANSYS program where the material properties of the piston and cylinder, pressure dependent density and viscosity of the pressure transmitting fluid etc. are to be used as the input parameters. Thus it provides characterization of a pressure balance in terms of effective area and distortion coefficient of the piston and cylinder. The present paper describes the results obtained on systematic studies carried out on the effect of gap profile between piston and cylinder of this controlled-clearance piston gauge, under the influence of applied pressure (p) from 100 MPa to 1000 MPa, on the pressure distortion coefficient (λ) of the assembly. The gap profile is also studied at different applied jacket pressure (p_j) such that p_j/p varied from 0.3, 0.4 and 0.5.     

Inter-laboratories comparison at 100 GΩ and 1 TΩ level to evaluate the traceability transfer from INRIM in the field of high dc resistance

A National inter-laboratories comparison of dc resistance at 100 GΩ and 1 TΩ among the National Institute of Metrological Research (INRIM) and eight Secondary Electrical Calibration Laboratories was carried out in 2010. All the involved Laboratories made their measurements with a method based on a Multifunction Calibrator (MFC) and on a digital multimeter (DMM), both used in their dc voltage function.These and other Secondary Electrical Laboratories are traceable to National Standards by means of the calibration at INRIM of a complete set of primary standards or, alternatively, by means of the calibration of a high accuracy DMM or of a Multifunction Transfer Standard (MTS) or of few primary standards. All the relative differences between each Laboratory’s value and its reference value obtained in the comparison were within their relative expanded uncertainties. This result showed that the traceability transfer methods from INRIM to Electrical Secondary Laboratories lead to satisfactory results in the field of high dc resistance.     

1–15,000 Pa Absolute mode comparisons between the NIST ultrasonic interferometer manometers and non-rotating force-balanced piston gauges

The National Institute of Standards and Technology (NIST) Low Pressure Manometry Project maintains and operates primary standard ultrasonic interferometer manometers (UIMs) over the pressure range of 1 mPa to 360 kPa. Over the past decade a new type of customer gauge, the non-rotating force-balanced piston gauge or FPG (model 8601, DH Instruments, a Fluke Company¹) has been introduced to the standards community that covers the range of ≈1–15,000 Pa and is capable of both absolute and differential measurement modes. Since 2002, NIST customers² have requested that four different FPG units be compared to the NIST primary pressure ultrasonic interferometer manometer standards (UIMs). The results of the comparisons were that all four FPG units were within manufacturers stated uncertainty (0.008 Pa + 30 × 10⁻⁶ × P for absolute mode) when compared against the NIST UIMs at pressures between 10 Pa and 15,000 Pa (absolute mode). At pressures between 5 Pa and 10 Pa, the results were generally within manufacturer’s specifications. Below 5 Pa some of the FPG units were outside of manufacturer’s uncertainty specifications. The use of an isolating capacitance diaphragm gauge (CDG) was necessary during the comparisons to prevent humidified gas from the FPG from entering the NIST 160 kPa mercury UIM primary pressure standard. The results of these four different comparison tests will be discussed in detail, along with test conditions, equipment set-up, and test uncertainty analysis.     

Drilling of microholes down to 10 μm in diameter using ultrasonic grinding

Drilling by grinding is useful for fabricating holes in hard and brittle materials with high dimensional accuracy and low machining cost. However, its application to microholes has been limited to those with a diameter on the submillimeter order. The drilling of microholes less than 0.1 mm in diameter by grinding was therefore attempted on crown glass. Cemented tungsten carbide micropins were fabricated by electrical discharge machining and used as micro-grinding tools. They can be employed because the convex parts of discharge craters formed on the tool surfaces serve as cutting edges of abrasive grains of grinding wheels. In order to reduce grinding force and thus prevent tool breakage, ultrasonic grinding was employed with the workpieces ultrasonically oscillated. As a result, microholes down to 10 μm in diameter were successfully drilled. They are the smallest-diameter holes drilled by grinding, to the best of our knowledge. The effect of helical feeding, in which the tool not only rotates around its axis but also moves in planetary motion, on drilling properties was also investigated.     

云计算助力制造业管理走向2·0时代

业界曾有人将云计算的影响力比喻成为是从古老的单台发电机向发电厂集中供电模式的一大转变。它意味着计算能力可以作为一种商品进行自由流通与交易，就像煤气和水电一样，取用方便，价格低廉。     

Environmental Effects on the Tribology and Microstructure of MoS<Subscript>2</Subscript>–Sb<Subscript>2</Subscript>O<Subscript>3</Subscript>–C Films

The tribology of molybdenum disulfide (MoS₂)–Sb₂O₃–C films was tested under a variety of environmental conditions (ambient 50% RH, 10⁻⁷ Torr vacuum, 150 Torr oxygen, and 8 Torr water) and correlated with the composition of the surface composition expressed while sliding. High friction and low friction modes of behavior were detected. The lowest coefficient of friction, 0.06, was achieved under vacuum, while sliding in 8 Torr water and ambient conditions both yielded the highest value of 0.15. Water vapor was determined to be the environmental species responsible for high friction performance. XPS evaluations revealed a preferential expression of MoS₂ at the surface of wear tracks produced under vacuum and an increase in Sb₂O₃ concentration in wear tracks produced in ambient air (50% RH). In addition, wear tracks produced by sliding in vacuum exhibited the lowest surface roughness as compared to those produced in other environments, consistent with the picture of low friction originating from well-ordered MoS₂ layers produced through sliding in vacuum.     

Fabrication In Situ TiB<Subscript>2</Subscript>–TiC–Al<Subscript>2</Subscript>O<Subscript>3</Subscript> Multiple Ceramic Particles Reinforced Fe-Based Composite Coatings by Gas Tungsten Arc Welding

A Fe-based composite coating reinforced by multiple TiB₂–TiC–Al₂O₃ ceramic particles was developed by gas tungsten arc welding (GTAW) melting process. Mixture of aluminum (Al), boron carbide (B₄C), and titanium dioxide (TiO₂) powders was used as precursors, and as a consequence TiB₂–TiC–Al₂O₃ multiple ceramic particles were in situ synthesized during GTAW melting process. Microstructural investigations showed that TiB₂ particles exhibit a blocky morphology, TiC particles are of flower-like shape, and the Al₂O₃ particles exist as small black dots and located in the core of reinforced particles. The hardness and wear resistance of the coatings increased drastically in comparison with that of the substrate.     

阿特拉斯&#183;科普柯的PET吹瓶压缩机首次通过Class0认证

2008年9月15日,阿特拉斯&#183;科普柯宣布该公司旗下的ZD高压压缩机成为世界上首台可为PET包装生产提供安全性通过100％无油空气认证和Class0认证的压缩机。该款压缩机具有下列特点：1提供100％无油空气。油污染是所有装瓶设备和无菌环境中的隐形敌人。阿特拉斯&#183;科普柯的40barZD压缩机凭借其独特的设计,完全消除了因油污染而引发的风险。     

Tribological Properties of Organic Functionalized ZrB<Subscript>2</Subscript>–Al<Subscript>2</Subscript>O<Subscript>3</Subscript>/Epoxy Composites

The tribological behaviors of epoxy composites filled with organic functionalized ZrB₂–Al₂O₃ were environmentally investigated and compared with those with as-received fillers under both dry and oil sliding conditions in this work. The worn surfaces and the transfer films on the counterparts were characterized by scanning electronic microscope (SEM), and the frictional temperature rising was investigated by infrared thermometer. The results demonstrated that the coefficient of friction (CoF), the wear rate, as well as the frictional temperature rise of the epoxy composites were all decreased due to the introduction of ZrB₂–Al₂O₃ fillers. And with the increase in filler content, similar variation tendencies of CoF and wear rate of epoxy composites were observed under the different sliding conditions. Besides, the organic functionalization of ZrB₂–Al₂O₃ fillers, which made the epoxy composites exhibit lower CoF and wear rate than those with as-received fillers, lowered the frictional temperature as well. In comparison, the epoxy composites filled with 5 vol% modified fillers presented better tribological properties, suggesting a stronger interfacial bonding between modified fillers and epoxy matrix. The dominant wear mechanisms of filled composites under dry and oil sliding conditions could be inferred as the combination of adhesive wear and abrasive wear and the fatigue wear, respectively, on the basis of SEM images of worn surfaces.     

Effects of Silicon Content on the Mechanical Properties and Lubricated Wear Behaviour of Al–40Zn–3Cu–(0–5)Si Alloys

In this work, one ternary Al–40Zn–3Cu and seven quaternary Al–40Zn–3Cu–(0.25–5)Si alloys were synthesized by permanent mould casting. Their microstructure, mechanical and lubricated wear properties were investigated using appropriate test apparatus and techniques. As the silicon content increased the hardness of the alloys increased, but their elongation to fracture decreased. Tensile strength of the alloys decreased with increasing silicon content following a sharp decrease and a slight increase. Among the silicon-containing quaternary alloys the highest and the lowest tensile strength values (348 and 305 MPa) were obtained with the Al–40Zn–3Cu–2Si and Al–40Zn–3Cu–5Si alloys, respectively, while the base alloy (Al–40Zn–3Cu) exhibited a tensile strength of 390 MPa. However, the volume loss due to wear of the alloys increased with increasing silicon content after showing an initial increase and a sharp decrease. The lowest wear loss was obtained with the alloy containing approximately 2% Si which has the highest tensile strength among the quaternary alloys containing more than 0.25% Si. Wear surfaces of the alloys were characterized mainly by smearing indicating that adhesion is the dominant wear mechanism for the experimental alloys.     

Dry Sliding Friction and Wear Properties of Al–25Zn–3Cu–(0–5)Si Alloys in the As-Cast and Heat-Treated Conditions

Dry sliding friction and wear properties of ternary Al–25Zn–3Cu and quaternary Al–25Zn–3Cu–(1–5)Si alloys were investigated using a pin-on-disc test machine after examining their microstructures and mechanical properties. An alloy (Al–25Zn–3Cu–3Si), which exhibited the highest tensile and compressive strengths, was subjected to T7 heat treatment. Surface and subsurface of the wear samples were investigated using scanning electron microscopy (SEM). The hardness and both tensile and compressive strengths of the alloys increased with increasing silicon content, but the trend reversed for the latter ones above 3% Si. It was observed that T7 heat treatment reduced the hardness and both tensile and compressive strengths of the Al–25Zn–3Cu–3Si alloy, but increased its elongation to fracture greatly. Three distinct regions were observed underneath the surface of the wear samples of the Al–25Zn–3Cu–3Si alloy. The formation of these regions was related to the heavy deformation of surface material and mixing, oxidation and smearing of wear material. Al–25Zn-based ternary and quaternary alloys in both as-cast and heat-treated conditions were found to be superior to SAE 660 bronze as far as their mechanical and dry sliding wear properties are concerned.     

Microstructural and Tribological Properties of A356 Al–Si Alloy Reinforced with Al<Subscript>2</Subscript>O<Subscript>3</Subscript> Particles

In the present study, the effect of the Al₂O₃ particles (average size of 12 μm, 3 and 10 wt.%) reinforcement on the microstructure and tribological properties of Al–Si alloy (A356) was investigated. Composites were produced by applying compocasting process. Tribological properties of unreinforced alloy and composites were studied, using pin-on-disc tribometer, under dry sliding conditions at different specific loads and sliding speed of 1 m/s. Microhardness measurements, optical microscope and scanning electron microscope were used for microstructural characterization and investigation of worn surfaces and wear debris. During compocasting of A356 alloy, a transformation from a typical dendritic primary α phase to a non-dendritic rosette-like structure occurred. Composites exhibited better wear resistance compared with unreinforced alloy. Presence of 3 wt.% Al₂O₃ particles in the composite material affected the wear resistance only at specific loads up to 1 MPa. The wear rate of composite with 10 wt.% Al₂O₃ particles was nearly two order of the magnitude lower than the wear rate of the matrix alloy. Dominant wear mechanism for all materials was adhesion, with others mechanisms: oxidation, abrasion and delamination as minor ones.     

齐齐哈尔二机床CK61250&#215;1O0／80数控重型卧式车床

机床的用途：本机床适用于高速钢、硬质合金及陶瓷刀具，对黑色金属、有色金属及部分非金属零件的粗、精加工。可车削圆柱面、圆锥面、端面、切槽、螺纹及回转曲面。     

Sliding Wear of Electrically Conductive ZrO<Subscript>2</Subscript>−WC Composites Against WC–Co Cemented Carbide

ZrO₂-based composites with WC addition can be successfully machined by electrical discharge machining (EDM) in demineralised water. ZrO₂ composites with 40 vol.% WC were produced from nanocrystalline and micrometre sized WC starting powders in order to compare their tribological behaviour. Friction and wear data are obtained on wire-EDM’ed ZrO₂–WC composite flats sliding against a WC–Co cemented carbide pin using a small-scale pin-on-plate testing rig. Correlations between wear volume, wear rate and friction coefficient on the one hand and material properties and test conditions on the other hand were elucidated. The experimental results revealed that the grain size of the electro-conductive WC-phase exhibits a strong influence on the friction and wear behaviour of the ZrO₂-based composite.