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排序方式: 共有742条查询结果,搜索用时 31 毫秒
1.
Chunliang Li Theo Veldhuis Bart Reuvers Rafaël J Sablong Cor E Koning 《Polymer International》2020,69(1):24-30
Limonene‐derived polycarbonate‐based alkyd resins (ARs) have been prepared by copolymerization of limonene dioxide with CO2, catalysed by a β‐diiminate zinc–bis(trimethylsilyl)amido complex, and subsequent chemical modification with soybean oil fatty acids using triphenylethylphosphonium bromide as the catalyst. This quantitative partial modification was realized via epoxy–carboxylic acid chemistry, affording ARs with higher oil lengths, lower polydispersities and higher glass transition temperatures (Tg) in comparison to a conventional polyester AR based on phthalic acid, multifunctional polyol pentaerythritol and soybean fatty acid. The novel limonene polycarbonate AR and the conventional polyester AR were evaluated as coatings and both the physical drying (without the presence of the oxidative drying accelerator Borchi® Oxy Coat) and chemical curing (with Borchi® Oxy Coat) processes of these coatings were monitored by measuring the König hardness and complex modulus development with time. A better performance was obtained for the alkyd paint containing polycarbonates modified with fatty acids (FA‐PCs), which showed a faster chemical drying, a higher König hardness and a higher Tg in coating evaluation, demonstrating that the fully renewable FA‐PCs are promising resins for alkyd paint applications. © 2019 Society of Chemical Industry 相似文献
2.
Iris Bakker Theo van der Voordt Peter Vink Jan de Boon Conne Bazley 《Color research and application》2015,40(1):62-71
Studies on color preferences are dependent on the topic and the relationships with personal characteristics, particularly personality, but these are seldom studied in one population. Therefore a questionnaire was collected from 1095 Dutch people asking for color preferences about different topics and relating them to personal characteristics. Color preferences regarding different topics show different patterns and significant differences were found between gender, age, education and personality such as being technical, being emotional or being a team player. Also, different colors were mentioned when asked for colors that stimulate to be quiet, energetic, and able to focus or creative. Probably, due to unconsciousness of contexts, many people had no color preference, a result that in the literature seldom is mentioned. Blue was the overall favorite color; however, most males chose for blue (25%) while most females had no color preference (18%). Black was the overall favorite color for clothing, mainly chosen by females (40%), while males primarily chose blue (27%). For building interiors subjects preferred white. For moods, subjects preferred white for being quiet or being able to focus, red for being energetic and had no color preference for being creative. It is concluded that color preferences are dependent upon the topic, and personal characteristics. The findings are important for architects, interior designers, fashion designers and product designers to have a basic idea of preferred colors for different objects by different types of people. © 2013 Wiley Periodicals, Inc. Col Res Appl, 40, 62–71, 2015 相似文献
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Terasa Kubala Baldev Gambhir S. Ian Borst 《Drug development and industrial pharmacy》1993,19(7):749-757
A high performance liquid chromatography method is described for the determination of diclofenac sodium, its related compounds and degradation products in commercial sources of raw materials and solid dosage forms. This method is specific, accurate and stability indicating. The method employs a reverse-phase octylsilane (C18) column with a mobile phase composed of acetonitrile/methanol/pic B-6 (25:25:50) and detection at 229 nm. The method resolves six principal related compounds with quantitation in the range 0.3-1.5%. Assay recoveries by spiking commercial formulations with diclofenac sodium were 99.64 ± 1.30%. Drug content in several commercial formulations are reported. Accelerated stability tests were conducted on raw materials and drug products and 1-(2,6-dichlorophenyl)-2-indolin-2-one was identified for the first time as a degradation product in solid dosage forms which are stressed under humidity and heat. 相似文献
6.
Alain B. Kounga Njiwa Theo Fett Doru C. Lupascu Jürgen Rödel 《Journal of the American Ceramic Society》2003,86(11):1973-1975
Crack–opening displacement (COD) measurements were performed on a commercial lead zirconate titanate (PZT). The intrinsic fracture toughness (or crack–tip toughness) of this material was determined using a new evaluation procedure, which takes into account the near–tip CODs and complete crack profile CODs. The crack–tip toughness K I0 was determined from an extrapolation of COD data obtained at various loading stages, thus avoiding the complications caused by subcritical crack growth in PZT. Results for plane strain and plane stress condition are presented. 相似文献
7.
Keshun Liu Susan Seegers Wenming Cao Janitha Wanasundara Juxing Chen Alessandro Esteves da Silva Kristopher Ross Alexandra Lozano Franco Theo Vrijenhoek Pankaj Bhowmik Yonghui Li Xin Wu Scott Bloomer 《Journal of the American Oil Chemists' Society》2021,98(4):375-390
For determining trypsin inhibitor activity (TIA) in soy products, the American Oil Chemists' Society (AOCS) Method Ba 12-75 has been used. It measures differences in absorbance at 410 nm of bovine trypsin activity toward a synthetic substrate (Nα-benzoyl-DL-arginine-p-nitroanilide) in the absence and presence of an inhibitor. Recently, a significantly improved method was developed (JAOCS, 2019, 96:635–645), featuring 5 mL of total assay volume, enzyme-last sequence, and single inhibitor level in duplicate. It is proposed as the AOCS Method Ba 12a-2020. As a part of the AOCS method approval process, a collaborative study involving 12 international laboratories was conducted to evaluate the performance of the proposed method. The study involved measuring TIA in 10 selected test samples plus a blind duplicate. They included soybeans, pulses, cereals, and their processed products (flours, concentrates, and isolates). After rigorous statistical treatment of the data, only three outliers were removed from the data of two samples. Repeatability relative standard deviations (RSDr) for the 11 samples ranged from 0.99% to 5.52%. Reproducibility RSD (RSDR) ranged from 7.07% to 22.92%, with seven samples having RSDR around 10% or less. The remaining four samples had very low TIA, and their RSDR values ranged from 13.34% to 22.92%. The study has demonstrated reliable performance of the proposed AOCS method. Several collaborators carried out additional experiments addressing some aspects of the method, leading to further refinements. The proposed method is undergoing evaluation by the AOCS Uniform Methods Committee for adoption as an Official Method for measuring TIA in various legume and grain products. 相似文献
8.
Takeo Uchida Keita Abe Yuma Endo Shosei Ichiseki Satoru Akita Shiyun Liu Sho Aradachi Masataka Saito Akihiko Fukuchi Taiyo Kikkawa Theo Dammaretz Ibuki Kawamata Yuki Suzuki Shin‐ichiro M. Nomura Satoshi Murata 《Small (Weinheim an der Bergstrasse, Germany)》2017,13(41)
A new kind of the Vernier mechanism that is able to control the size of linear assembly of DNA origami nanostructures is proposed. The mechanism is realized by mechanical design of DNA origami, which consists of a hollow cylinder and a rotatable shaft in it connected through the same scaffold. This nanostructure stacks with each other by the shape complementarity at its top and bottom surfaces of the cylinder, while the number of stacking is limited by twisting angle of the shaft. Experiments have shown that the size distribution of multimeric assembly of the origami depends on the twisting angle of the shaft; the average lengths of the multimer are decamer, hexamer, and tetramer for 0°, 10°, and 20° twist, respectively. In summary, it is possible to affect the number of polymerization by adjusting the precise shape and movability of a molecular structure. 相似文献
9.
J. Vignollet S. May R. de Borst 《International journal for numerical methods in engineering》2016,108(9):990-1006
An isogeometric model is developed for the analysis of fluid transport in pre‐existing faults or cracks that are embedded in a fluid‐saturated deformable porous medium. Flow of the interstitial fluid in the porous medium and fluid transport in the discontinuities are accounted for and are coupled. The modelling of a fluid‐saturated porous medium in general requires the interpolation of the displacements of the solid to be one order higher than that of the pressure of the interstitial fluid. Using order elevation and Bézier projection, a consistent procedure has been developed to accomplish this in an isogeometric framework. Particular attention has also been given to the spatial integration along the isogeometric interface element in order to suppress traction oscillations that can arise for certain integration rules when a relatively high dummy stiffness is used in a poromechanical model. © 2016 The Authors. International Journal for Numerical Methods in Engineering Published by John Wiley & Sons Ltd. 相似文献
10.
Powell–Sabin B‐splines and unstructured standard T‐splines for the solution of the Kirchhoff–Love plate theory exploiting Bézier extraction
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Stefan May Julien Vignollet René de Borst 《International journal for numerical methods in engineering》2016,107(3):205-233
The equations that govern Kirchhoff–Love plate theory are solved using quadratic Powell–Sabin B‐splines and unstructured standard T‐splines. Bézier extraction is exploited to make the formulation computationally efficient. Because quadratic Powell–Sabin B‐splines result in ‐continuous shape functions, they are of sufficiently high continuity to capture Kirchhoff–Love plate theory when cast in a weak form. Unlike non‐uniform rational B‐splines (NURBS), which are commonly used in isogeometric analysis, Powell–Sabin B‐splines do not necessarily capture the geometry exactly. However, the fact that they are defined on triangles instead of on quadrilaterals increases their flexibility in meshing and can make them competitive with respect to NURBS, as no bending strip method for joined NURBS patches is needed. This paper further illustrates how unstructured T‐splines can be modified such that they are ‐continuous around extraordinary points, and that the blending functions fulfil the partition of unity property. The performance of quadratic NURBS, unstructured T‐splines, Powell–Sabin B‐splines and NURBS‐to‐NURPS (non‐uniform rational Powell–Sabin B‐splines, which are obtained by a transformation from a NURBS patch) is compared in a study of a circular plate. Copyright © 2015 John Wiley & Sons, Ltd. 相似文献