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ABSTRACT: Physical aging of amorphous anhydrous fructose at temperature 5 °C and at 22 °C was studied using differential scanning calorimetry (DSC). The dynamic glass transition temperature, Tg0 for unaged samples was 16 °C and 13.3 °C for heating rate of 10 °C/min and 1 °C/min, respectively. The fictive temperature, Tf0 for unaged samples calculated by Richardson and Savill method was 12 °C, which is close to the dynamic value obtained from the lower DSC heating rate. The fictive temperature Tf of the aged fructose glasses at temperatures both below and above the transition region was fitted well by a non-exponential decay function (Williams-Watts form). Aging above the transition region (22 °C) for 18 d increased both the dynamic glass transition temperature Tg and the fictive temperature Tf . However, aging below the transition region (5 °C) for 1 d increased the dynamic glass transition temperature Tg but decreased the fictive temperature Tf . 相似文献
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提出用高效液相色谱法( H P L C), Bondapak N H2 柱为分析柱,乙腈—水(3∶1, V/ V)为流动相,示差折 光仪为检测器,一次进样能同时测定低聚果糖样品中的果糖、蔗糖、蔗果三糖( G F2 )、蔗果四糖( G F3 )、蔗果五糖( G F4 )、蔗果六糖( G F5 )等。本法测定了样品“博爱生命素”和“火麻仁内清液”,所得结果良好,变异系数为 09 % ~15 % ,线性相关系数 r 为 09990~09999。 相似文献
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Ozan Tas Ulku Ertugrul Mecit Halil Oztop Bekir Gokcen Mazi 《International Journal of Food Science & Technology》2021,56(11):5461-5470
Modification of food proteins to have improved functional properties is of great importance. In this study, modification of soy protein isolate (SPI) was achieved through glycation. SPI was glycated in a spray dryer (SD) and an incubator followed by freeze drying (FD). d -Allulose, an important rare sugar, was used in SPI glycation as the carbohydrate source, and results were compared with fructose. In addition to the sugar type, two different SPI powder: sugar ratios (1:1 and 5:1) were investigated. For the glycated samples, emulsification activity, free amino groups, protein solubility, Fourier-transform infrared spectroscopy analysis, antioxidant activity experiments and time-domain NMR relaxometry measurements for hydration were conducted. According to the results, the solubility of SPI that is limited in native form has shown a significant improvement after glycation through both FD and SD methods. Besides, glycation through the FD method was found to be more favourable due to its milder conditions than the SD method. Considering the physicochemical properties, the best combination for the highest glycation degree was found to be the samples prepared at the 1:1 ratio with d -Allulose in the FD method. Overall, it was concluded that glycation of SPI enhanced its functional properties such as antioxidant and emulsification activities. 相似文献
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为了降低传统脲醛树脂中甲醛的危害,采用了果糖代替甲醛与尿素合成了环保型果糖/尿素树脂,并用合成出的树脂与芦苇纤维复合制备了芦苇纤维板,考察了树脂合成过程中果糖/尿素物质的量之比、反应温度、反应时间、催化剂种类等工艺参数对树脂及芦苇纤维板性能的影响,得到了果糖/尿素树脂的最佳合成工艺,即果糖/尿素/催化剂盐酸的物质的量之比为2.5/1/0.13、反应温度为91℃、反应时间为3 h。在此最佳合成工艺下合成的树脂固含量为65.57%、黏度为73 m Pa·s,由此树脂制备的芦苇纤维板的静曲强度为26.19 MPa,弹性模量为6.13 GPa,完全满足国家标准GB/T 11718–2009的要求。 相似文献
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Messias Miranda Júnior Margareth Batistote José Roberto Ernandes 《Journal of the Institute of Brewing》2008,114(3):199-204
Glucose and fructose fermentations by industrial yeasts strains are strongly affected by both the structural complexity of the nitrogen source and the availability of oxygen. In this study two Saccharomyces cerevisiae industrial wine strains were grown, under shaken and static conditions, in a media containing either a) 20% (w/v) glucose, or b) 10% (w/v) fructose and 10% (w/v) glucose or c) 20% (w/v) fructose, all supplemented with nitrogen sources varying from a single ammonium salt (ammonium sulfate) to free amino acids (casamino acids) and peptides (peptone). Data suggest that a complex structured nitrogen source is not submitted to the same control mechanisms as those involved in the utilization of simpler structured nitrogen sources, and mutual interaction between carbon and nitrogen sources, including the mechanisms involved in the regulation of aerobic/anaerobic metabolism, may play an important role in defining yeast fermentation performance and the differing response to the structural complexity of the nitrogen source, with a strong impact on fermentation performance. 相似文献
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John E Bradshaw D Wynne Griffiths 《Journal of the science of food and agriculture》1990,50(2):167-172
The sugar content was determined of 19 cultivars of swede (Brassica napus ssp rapifera L) grown in rows 50 and 75 cm apart. Sugar concentration ranged from 54.3 to 78.7 g kg?1 fresh weight and was positively correlated with dry matter content which ranged from 90.4 to 138.7 g kg?1 fresh weight. The average concentration of fructose, glucose and sucrose in the dry matter was 225.0, 328.4 and 34.5 g kg?1 DM, respectively. The high-dry-matter cultivars tended to have less fructose and more sucrose than the low-dry-matter ones, but total sugar concentration in the dry matter was not associated with dry-matter content. Row width had little effect on sugar content compared with the differences between cultivars. The implications for the feeding value of swedes are discussed. 相似文献