排序方式: 共有18条查询结果,搜索用时 31 毫秒
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丙溴磷,杀螨隆,氟铃脲等防治小菜蛾及菜青虫试验 总被引:2,自引:0,他引:2
试验结果表明,丙溴磷、杀螨隆、氟铃脲等对小菜蛾均有效,且持效期长,丙溴磷具有速效性及对菜青虫高效。 相似文献
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采用气相色时测定溴丙磷原药及制剂的含量,选用5%OV-101/Gas Chrom Q色谱柱,以邻苯二甲酸二丁酯为内标物,三氯甲烷为溶剂,用氢火焰离子化检测器测定,其回收率在98.6 ̄100.4%,原油和乳油的变异系数分别为0.42%和0.48%。 相似文献
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1993、1994年用40%丙溴磷乳油进行了防治棉铃虫药效试验,两年的试验结果表明,亩用该药60、80、100毫升,在药后7 天远达到了80%以上的防效,亩施100毫升,防效均达到93.7%以上,明显高于2.5%三氟氯氰菊酯乳油亩施30毫升的防效77.0%。该药是一种防治抗性棉铃虫的优良杀虫剂,建议棉田用量为亩施80 ̄100毫升为宜。 相似文献
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利用高效液相色谱法对丙溴磷进行了分析测定。本实验选择μBondapak C18色谱柱、甲醇:水以动相和UV-280纳米检测等色谱条件,使丙溴磷得到了较好地分离。本方法定量测定的回收率为98.82%,变异系数为3.12%,。实验结果表明,本方法是一种快速,简便,灵敏度高,重现性较好的测定方法。 相似文献
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44%丙溴磷·氯氰菊酯水乳剂的配方研究 总被引:5,自引:1,他引:4
根据水乳剂形成的机理,选用合适的表面活性剂、助溶剂等,制备出44%丙溴磷.氯氰菊酯水乳剂,并对其进行了性能测定和田间药效试验。结果表明,44%丙溴磷.氯氰菊酯水乳剂与44%丙溴磷.氯氰菊酯乳油药效相当。 相似文献
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S. M. Dogheim El M. M. Ashraf S. A. G. Alla M. A. Khorshid S. M. Fahmy 《Food Additives & Contaminants》2004,21(4):323-330
A total of 835 samples of leafy vegetables and some aromatic medicinal plants were collected from five different areas of Egypt during 1999. Ninety-seven per cent of the leafy vegetables were contaminated with heavy metals with 39% exceeding the maximum limits for each element. Cadmium was detected in 78 of 116 samples of leafy vegetable, although without any exceeding the maximum limits. However, lead was detected in 99 samples, of which 39 exceeded the maximum limits (0.3 mg kg-1) and 56 medicinal plant samples of 70 had lead levels above 0.5 mg kg-1. Copper was detected in 69 medicinal plant samples, of which 58 samples contained levels higher than 10 mg kg-1. However, cadmium was only found in 43% of samples with only two of 70 samples above the maximum limit. Seventy-three per cent of the samples of medicinal plants were contaminated with pesticide residues, of which 44% contained amounts that exceeded maximum residue limits. Malathion was the most frequently found pesticide residue, being detected in 203 of 391 (52%.) samples, followed by profenofos, which was detected in 131 of 391 (33%) samples. 相似文献
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韩曦莹 《食品安全质量检测学报》2020,11(10):3301-3305
目的建立气相色谱法测定陈皮中丙溴磷残留量的分析方法。方法样品经乙腈提取,经过滤,QuECHERS净化,浓缩后,用丙酮定容,采用气相色谱法测定、外标法定量。结果丙溴磷在0.005~1.000μg/mL范围内线性良好,相关系数r~2达到0.999;方法检出限为0.008 mg/kg;平均回收率为89.9%~110.8%,相对标准偏差(relative standard deviation,RSD)为2.2%~3.3%(n=6)。结论本方法操作简便、灵敏度高、准确度好,适用于陈皮中丙溴磷残留量测定。 相似文献