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1.
《International Journal of Hydrogen Energy》2022,47(25):12726-12738
The use of a Pt-based catalyst was evaluated for autocatalytic hydrogen recombination. The Pt was supported on a mixture of Ce-, Zr- and Y-oxides (CZY) to yield nanosized Pt particles. The Pt/CZY/AAO catalyst was then prepared by the spray-deposition of the Pt/CZY intermediate onto an anodized aluminium oxide (AAO) layer on a metallic aluminum core. The Pt/CZY/AAO catalyst (3 × 1 cm) was evaluated for hydrogen combustion (1–8 vol% hydrogen in the air) in a recombiner section testing station. The thermal distribution throughout the catalyst surface was investigated using an infrared camera. The maximum temperature gradient (ΔT) for the examined hydrogen concentrations did not exceed 36 °C. The Pt/CZY/AAO catalyst was also evaluated for prolonged hydrogen combustion duration to assess its durability. An average combustion temperature of 239.0 ± 10.0 °C was maintained for 53 days of catalytic hydrogen combustion, suggesting that there was limited, or no, catalyst deactivation. Finally, a Pt/CZY/AAO catalytic plate (14.0 × 4.5 cm) was prepared to investigate the thermal distribution. An average surface temperature of 212.5 °C and a maximum ΔT of 5.4 °C was obtained throughout the catalyst surface at a 3 vol% hydrogen concentration. 相似文献
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B. Van de Moortéle 《材料科学技术学报》2003,19(6)
The homogeneous plastic flow of fully amorphous and partially crystallized Zr(41.2)Ti(13.8)Cu(12.5)Ni(10)Be(22.5) bulk metallic glass (Vitl) has been investigated by compression tests at high temperatures in supercooled liquid region. Experimental results show that at sufficiently low strain rates, the supercooled liquid of the fully amorphous alloy reveals Newtonian flow with a linear relationship between the flow stress and strain rate. As the strain rate is increased, a transition from linear Newtonian to nonlinear flow is detected, which can be explained by the transition state theory. Over the entire strain rate interval investigated, however, only nonlinear flow is present in the partially crystallized alloy, and the flow stress for each strain rate is much higher. It is found that the strain rate-stress relationship for the partially crystaltized alloy at the given temperature of 646 K also obeys the sinh law derived from the transition state theory, similar to that of the initial homogeneous amo 相似文献
4.
The influence of Zr addition on magnetic properties and temperature coefficient for nanocomposite Nd10Fe78.5-xCO5ZrxB6.5 (x=0~4) bonded magnets was investigated. It was found that the room-temperature magnetic properties were remarkably improved with Zr addition due to the grain refinement and increasing volume fraction of the hard magnetic phase. The optimal magnetic properties of Jr=0.689T, iHc=769.4kA·m-1 and (BH)max=84kJ·m-3 were obtained for 2.5% Zr addition. The temperature coefficient of remanence (α) increases slightly and the temperature coefficient of coercivity (β) decreases obviously with increasing Zr content for nanocomposite Nd10Fe78.5-xCo5ZrxB6.5 (x=0~4) bonded magnets. 相似文献
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《Calphad》2021
Accurate Young's modulus is the necessity for the design of biomedical Ti alloys. A combinatorial method of the diffusion couple, nanoindentation, electron probe microanalysis (EPMA), and CALculation of PHAse Diagrams (CALPHAD) techniques has been utilized to construct the Young's modulus database of Ti alloys with various compositions in the present work. Two groups of body-centered cubic (bcc) Ti–Nb–Zr–Mo quaternary diffusion couples annealed at 1273 K for 25 h were experimentally prepared. Subsequently, the composition-dependent mechanical properties in the wide compositional range of Ti-based alloys were obtained by using EPMA and nanoindentation probes. Finally, on the basis of the measured Young's moduli in the present and previous work and the modeling parameters of Young's modulus of Ti–Nb–Zr system, the Young's modulus database of bcc Ti–Nb–Zr–Mo system was established through the CALPHAD approach. The CALPHAD-type database of bcc Ti–Nb–Zr–Mo system can provide the accurate Young's moduli of Ti alloys with wide compositions. 相似文献
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锆及锆合金中微量铝的测定 总被引:1,自引:0,他引:1
陈学源 《稀有金属材料与工程》1992,21(6):65-68
本文介绍在硫酸介质中,先用钽试剂-氯仿萃取分离除去锆以及钛、铁、铪等;再在pH=8.5左右,用苯萃取铝-钽试剂配合物,用稀盐酸反萃取;最后在pH=5.5—6时用铬天青S比色以测定铝的方法,确定了其测定条件。本方法准确性好,灵敏度高,测定范围为0.0025%—0.035%。 相似文献
9.
用弯曲法和拉伸法测定Ti-22Nb-6Zr(at%)合金的超弹性和形状记忆效应,研究固溶处理温度对Ti-22Nb-6Zr合金组织结构及性能的影响。结果表明:固溶处理后Ti-22Nb-6Zr合金的室温组织为单一的β相,晶粒尺寸随固溶处理温度升高而增大;合金的静态弹性模量小于30GPa;Ti-22Nb-6Zr合金具有良好的超弹性和一定的形状记忆效应。室温下变形,合金的超弹性和形状记忆效应随固溶处理温度升高而提高。900℃固溶处理后的合金在室温下拉伸变形,应变为5%时,总的最大回复应变达4.12%,其中超弹性回复应变为3.91%,记忆回复应变为0.21%。 相似文献
10.
Zr对Cu—Zn—Al形状记忆合金相变的影响 总被引:2,自引:0,他引:2
采用示差扫描热分析(DSC)、X射线衍射及透射电镜,研究了Zr对Cu-Zn-Al合金高温相变、马氏体正逆转变以及形状记忆效应的影响。结果表明,添加Zr0.35wt-%时,能有效地抑制α,γ相析出,促进β_2→DO_3→18RM转变。(M_s-M_f)及(A_s-A_f)温度区间较窄,马氏体相变激活能最低,马氏体变体间界面的可动性好,形状记忆效应最佳。 相似文献