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81.
E. Papadopoulou D. Delimaris A. Denis A. Machocki T. Ioannides 《International Journal of Hydrogen Energy》2012
Co–MnO catalysts have been prepared by pyrolytic decomposition of the corresponding fumarate or gluconate salts and examined in the reactions of methanol and ethanol reforming. The synthesis parameters were the type of organic salt, the Co:Mn ratio and the temperature of decomposition. The decomposition pathway depends on the type of carboxylate, with the fumarate group being more stable than the gluconate. In-situ XRD measurements of salt decomposition showed that the reducing atmosphere prevailing during thermal treatment, as well as the presence of solid carbon, facilitates reduction of cobalt oxides towards metallic cobalt at temperatures above ∼500 °C. Thus, the reduced form of the catalyst, consisting mainly of metallic cobalt and MnO dispersed in a carbonaceous matrix can be prepared in a single step. It was found that reforming of both methanol and ethanol proceeds under comparable reaction conditions and hydrogen yield is maximized at temperatures of 400–450 °C. The activity of catalysts prepared under an inert atmosphere was considerably higher than the one of catalysts prepared through oxidative pre-treatment. 相似文献
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Andrey N. Agafonov Boris O. Volodkin Denis G. Kachalov Boris A. Knyazev Grigory I. Kropotov Konstantin N. Tukmakov 《Journal of Modern Optics》2013,60(11):1051-1054
AbstractWe demonstrate results of studies of a silicon binary diffractive optical element (DOE) focusing a terahertz laser Gaussian beam into a paraxial segment. The characteristics of the DOE were examined on a Novosibirsk Free Electron Laser beam of 141-μm wavelength. 相似文献
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Emmanuel Bernuau Andrey Polyakov Denis Efimov Wilfrid Perruquetti 《Systems & Control Letters》2013,62(12):1159-1167
Several conditions are proposed to check different robustness properties (ISS, iISS, IOSS and OSS) for generic nonlinear systems applying the weighted homogeneity concept (global or local). The advantages of this result are that, under some mild conditions, the system robustness can be established as a function of the degree of homogeneity. 相似文献
87.
Joelle Al Hage Maan E. El Najjar Denis Pomorski 《Journal of Intelligent and Robotic Systems》2017,87(3-4):661-681
Multi-robot system attracted attention in various applications in order to replace the human operators. To achieve the intended goal, one of the main challenges of this system is to ensure the integrity of localization by adding a sensor fault diagnosis step to the localization task. In this paper, we present a framework able, in addition of localizing a group of robots, to detect and exclude the faulty sensors from the group with an optimized thresholding method. The estimator has the informational form of the Kalman Filter (KF) namely Information Filter (IF). A residual test based on the Kullback-Leibler divergence (KLD) between the predicted and the corrected distributions of the IF is developed. It is generated from two tests: the first acts on the means and the second deals with the covariance matrices. Thresholding using entropy based criterion and Receiver Operating Characteristics (ROC) curve are discussed. Finally, the validation of this framework is studied on real experimental data from a group of robots. 相似文献
88.
Complex structural contribution of the morphotropic phase boundary in Na0.5Bi0.5TiO3 - CaTiO3 system
Roy Roukos Sara Abou Dargham Jimmy Romanos Fatima Barakat Denis Chaumont 《Ceramics International》2019,45(4):4467-4473
The correlation between structure and dielectric properties of lead-free (1-x)Na0.5Bi0.5TiO3 - xCaTiO3 ((1-x)NBT - xCT) polycrystalline ceramics was investigated systematically by X-ray diffraction, combined with impedance spectroscopy for dielectric characterizations. The system shows high miscibility in the entire composition range. A morphotropic phase boundary (MPB), at 0.09?≤?x?<?0.15 was identified where rhombohedral and orthorhombic symmetries coexist at room temperature. The fraction of orthorhombic phase increases gradually with x in the MPB region. Dielectric measurements reveal that the relative permittivity increase with addition of Ca2+. This behavior is unusual with this kind of doping. A thermal hysteresis occurred only in the MPB composition which varies in a non-monotonically manner with x, detected by dielectric properties. This phenomenon is related to the crystalline microstructure by a linear relationship between the fraction of each phase and dielectric properties, and, more precisely, to the strong interaction between rhombohedral and orthorhombic phases. 相似文献
89.
Gunka Volodymyr Shved Mariia Prysiazhnyi Yuriy Pyshyev Serhiy Miroshnichenko Denis 《国际煤炭科学技术学报(英文)》2019,6(1):63-73
International Journal of Coal Science & Technology - The study reviews the process of oxidative desulphurization of high-sulphur Ukrainian lignite, which was performed by coal treatment using... 相似文献
90.