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91.
Betül Sen Sultan Kuzu Enes Demir Tuğba Onal Okyay Fatih Sen 《International Journal of Hydrogen Energy》2017,42(36):23299-23306
Addressed herein, we reported the fabrication of the graphene oxide (GO) supported monodispersed ruthenium–platinum–nickel (RuPtNi) nanomaterials (3.40 ± 0.32 nm) to be utilized as a catalyst in the process of dimethylamine borane (DMAB) dehydrogenation. The nanoparticles were fabricated through the ultrasonication method by co-reducing the Ru3+, Pt2+ and Ni2+ cations and then the nanomaterials were characterized by X-ray diffraction (XRD), Raman spectroscopy, transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), electron energy loss spectroscopy (EELS), inductively coupled plasma optical emission spectrometry (ICP-OES), and X-ray photoelectron spectroscopy (XPS). The fabricated nanomaterials showed outstanding efficiency and remarkable reusability in addition to their record catalytic activity at low temperatures and with extreme low concentrations. They had a significantly high turnover frequency (TOF) (727 h?1) and low activation energy (Ea) (49.43 ± 2 kJ mol?1) for DMAB dehydrocoupling. To the best of our knowledge, RuPtNi@GO NPs become a very promising candidate as the best catalyst ever. 相似文献
92.
Marek Choratzy ;Marta Majcher ;Katarzyna Fedyszyn Urbanowicz ;Jedrzej Gtasek ;Maciej Gawlikowicz ;Tomasz Duniec 《材料科学与工程:中英文B版...》2014,(12):376-384
The authors compared their earlier results of the tumor biopsies performed under computer tomography (CT) guidance against the results of their recently modified-combined method of visualization and measurement of lung tumor parameters by CT imaging followed by US guided biopsy. In 238 (6.36%) of 3,745 patients in CT examination, the lung tumor was located peripherally, and obtaining histopathological confirmation was crucial to start the proper treatment. The patients were divided into two groups, the division was based on the biopsy method. Within the first group in I 18 patients, parietal lung tumor was confirmed and CT guided biopsy was performed. Within the second group, parietal lung tumor was confirmed in 120 patients and combined method of CT pre- biopsy planning and US guided biopsy were used. Pre-biopsy planning was performed using CT, measurements such as depth and distance of the tumor were made, obtained data were then saved on CT image and patient's skin was marked. Then obtained results were analyzed using test for two proportions. The analysis of the results confirmed the higher efficacy of the combined method taking into account the number of complications (p 〈 0.01) and diagnostic histopathological results (P 〈 0.001). Suggested innovative method, involving both CT pre-biopsy planning and US guided biopsy, allows to analyze simultaneously static CT and dynamic US images and it is considered to be an easy and effective method comparing to relying on static in nature CT images only. Our method is related to a lower complication risk rate. 相似文献
93.
Ákos Zarándy Csaba Rekeczky 《International Journal of Circuit Theory and Applications》2011,39(10):983-1005
Topographic and non‐topographic image processing architectures and chips, developed within the CNN community recently, are analyzed and compared. It is achieved on a way that the 2D operators are collected to classes according to their implementation methods on the different architectures, and the main implementation parameters of the different operator classes are compared. Based on the results, an efficient architecture selection methodology is formalized. Copyright © 2010 John Wiley & Sons, Ltd. 相似文献
94.
Multiscale approach to the morphology,structure, and segmental dynamics of complex degradable aliphatic polyurethanes 下载免费PDF全文
Milena Špírková Luďka Machová Libor Kobera Jiří Brus Rafał Poręba Magdalena Serkis Alexander Zhigunov 《应用聚合物科学杂志》2015,132(10)
A multiscale approach spanning from the segmental (subnanometer) up to micrometer level was applied for detailed study of the self‐assembly of aliphatic block polyurethane (PU) elastomers. To understand the principles of the self‐organization of hard and soft segments in the complex multi‐component systems, several two‐component model PU samples, that is, the products of 1,6‐diisocyanatohexane (HDI) with three diols differing in the length and constitution were also prepared, characterized, and investigated: (i) polycarbonate‐based macrodiol (MD), (ii) biodegradable oligomeric diol (DL‐L; product of butane‐1,4‐diol and D,L‐lactide), and (iii) butane‐1,4‐diol (BD). The study (particularly 13C‐1H PILGRIM NMR spectra) reveals complex internal organization and interesting (application appealing) behavior of multi‐component PUs. Hard segments (HDI+BD products) feature self‐assembled and significantly folded chain conformations with interdomain spacing 15–22 nm (small‐angle X‐ray scattering analysis). The small domains are hierarchically assembled in various structural formations of µm size (spherulites) depending on PU composition, as detected by transmission electron microscopy and atomic force microscopy. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015 , 132, 41590. 相似文献
95.
Effect of the structure of polymer inclusion membranes on zn(II) transport from chloride aqueous solutions 下载免费PDF全文
This article presents application of polymer inclusion membranes (PIM) containing polymer matrices: cellulose triacetate (CTA) or poly(vinyl) chloride (PVC), o‐nitrophenyloctyl ether (NPOE) as a plasticizer and phosphonium ionic liquids, i.e., trihexyltetradecylphosphonium chloride (Cyphos IL 101), bis(2,4,4‐trimethylpentyl)phosphinate (Cyphos IL 104) and tributyltetradecylphosphonium chloride (Cyphos IL 167), as carriers for Zn(II) transport from chloride medium. Cyphos IL167 application as an ion carrier in PIMs is reported for the first time. The membrane composition is found to affect Zn(II) transport significantly. SEM and AFM images show the differences in the surface morphology of PVC and CTA based membranes. Better transport abilities of CTA membranes (Zn(II) recovery factors exceed 80%) compared with those of PVC, indicate that the structural differences between the two polymers play a crucial role for the membrane permeability. The best initial flux and permeability coefficient are obtained for the membranes with Cyphos IL 101 and Cyphos IL 104 as carriers. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015 , 132, 42319. 相似文献
96.
97.
Emina?AlickovicEmail author Abdulhamit?Subasi 《Circuits, Systems, and Signal Processing》2015,34(2):513-533
Current trends in clinical applications demand automation in electrocardiogram (ECG) signal processing and heart beat classification. This paper examines the design of an effective recognition method to diagnose heart diseases. The proposed method consists of three main modules: de-noising module, feature extraction module, and classifier module. In the de-noising module, multiscale principal component analysis (MSPCA) is used for noise reduction of the ECG signals. In the feature extraction module, autoregressive (AR) modeling is used for extracting features. In the classifier module, different classifiers are examined such as simple logistic, k-nearest neighbor, multilayer perceptron, radial basis function networks, and support vector machines. Different experiments are carried out using the MIT-BIH arrhythmia database to classify different ECG heart beats and the performance of the proposed method is evaluated in terms of several standard metrics. The experimental results show that the proposed method is able to reduce noise from the noisy ECG signals more accurately in comparison to previous methods. The numerical results indicated that the proposed algorithm achieved 99.93 % of the classification accuracy using MSPCA de-noising and AR modeling. 相似文献
98.
99.
Krzysztof Marycz Monika Marędziak Jakub Grzesiak Ryszard Fryczkowski Jadwiga Laska 《Polymer-Plastics Technology and Engineering》2016,55(18):1897-1907
Articular cartilage dysfunctions are major cause of pain and disability and lead to serious health complications. Cell-based therapies are proposed as treatment methods for cartilage regeneration. In this study, we proposed polyurethane/poly(L-lactide-co-D, L-lactide)-based electrospun nonwovens as carriers for the delivery of human adipose-derived stromal stem cells. We found that 6:4 and 8:2 polyurethane/poly(L-lactide-co-D, L-lactide) initially enhance proliferative rate of human adipose-derived stromal stem cells, shorten their population doubling time, promote creation of functional chondrogenic nodules during chondrogenic differentiation, improve the collagen-2-to-collagen-1 protein ratio, and upregulate the expression of collagen-2 and aggrecan genes. 相似文献
100.
The purpose of the study was to obtain a composite material with the self‐reinforced structure, which processing provide increased mechanical properties. The composites used in presented work were prepared from the two types of fiber mixtures, both were based on polypropylene fibers, the difference was in used cellulose or wood flour filler. Composites were prepared using the hot compaction method. The presented research describes the effect of the composite composition and processing conditions. The results include the static tension measurements, tensile impact tests and thermal analysis, including: DSC and DMTA. The structure has been studies using the SEM observations. Results of presented studies confirm the self‐reinforcing effect in obtained hybrid composites. It provides in the comparison to the standard wood polymer composites to the higher level of material reinforcement with lower amount of natural filler. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016 , 133, 43283. 相似文献