磷酸盐激光玻璃中铂颗粒密度与氧化还原平衡关系的研究

用吸收光谱法研究了Ｒ２Ｏ—ＢａＯ—Ｐ２Ｏ５系统磷酸盐激光玻璃中铂颗粒密度与铭的氧化还原平衡的关系。结果表明，玻璃中铂颗粒密度随平衡向右移动而减小；玻璃中平衡随熔炼气氛中氧分压增大、熔炼温度升高而向右移动，当足够大时，铂颗粒不能形成。     

用小尺寸R－CT试样研究核压力容器钢断裂韧性及与Charpy试样的比较

提出了一种用双边带深侧槽的小尺寸圆形紧凑拉伸试样评定核压力容器（ＲＰＶ）钢断裂韧性的单试作试验方法，给出了用该方法测定的两个厂家生产的核压力容器用Ａ５０８ＣＬ３钢的断裂韧性参数，还与Ｃｈａｒｐｙ试样的试验结果及大尺寸标准试样的试验结果进行了比较。研究结果表明：用双边带深侧槽的小尺寸Ｒ－ＣＴ试样测得的断裂韧性值比相同恻槽深度预制疲劳裂纹Ｃｈａｒｐｙ试样的测试值更接近有效断裂韧性值，所以，用于核压力容器断裂韧性的监测是可行的。     

A unified model for dislocation nucleation, dislocation emission and dislocation free zone

In this paper, a unified model for dislocation nucleation, emission and dislocation free zone is proposed based on the Peierls framework. Three regions are identified ahead of the crack tip. The emitted dislocations, located away from the crack tip in the form of an inverse pileup, define the plastic zone. Between that zone and the cohesive zone immediately ahead of the crack tip, there is a dislocation free zone. With the stress field and the dislocation density field in the cohesive zone and plastic zone being, respectively, expressed in the first and second Chebyshev polynomial series, and the opening and slip displacements in trigonometric series, a set of nonlinear algebraic equations can be obtained and solved with the Newton-Raphson Method. The results of calculations for pure shearing and combined tension and shear loading after dislocation emission are given in detail. An approximate treatment of the dynamic effects of the dislocation emission is also developed in this paper, and the calculation results are in good agreement with those of molecular dynamics simulations.Presented at the Far East Fracture Group (FEFG) International Symposium on Fracture and Strength of Solids, 4–7 July 1994 in Xi'an, China.     

邻重氮萘醌改性酚醛树脂碱溶解特性的定量评价

本文提出了一种利用紫外—可见光分光光度仪定量评价高分子膜溶解速度的方法。并着重考查了邻重氮萘醌改性后的酚醛树脂在碱溶液中的溶解特性。实验表明,曝光后的树脂在碱溶液中首先溶胀,然后才开始溶解,即存在溶解滞后现象。溶解滞后和溶解速度与溶液的碱度有关,与树脂膜厚无关。     

应用音平化渣图象分析和指导转炉造渣操作

利用音平化渣图象可以清晰地看出在转炉造渣过程中何时发生喷溅，何时发生炉渣返干和何时化渣正常。应用音平化渣图象和炉渣三元相图，可以正确地分析发生喷溅和返干的原因，从而找到避免突发性喷溅和严重返干的方法。正确的枪位和炉渣碱度控制是实现平稳吹炼的保证，而音平化渣图象能帮助操作工实现这一目标。     

多级脉冲深穿透射孔技术

目前国内较先进的射孔工艺是增效射孔和三相流射孔,这2种射孔工艺均存在射孔深度和造缝深度浅的问题,尤其是对低渗油藏和纵向渗透率远大于横向渗透率的油藏,此造缝深度并不能满足油田生产的需要.介绍了一种新型的射孔技术,它是一种能进行深度射孔造缝的多级射孔技术,利用三级推进剂燃爆时产生峰值不连续的高温、高压气流,形成多级脉冲,多次冲击射孔孔眼前沿的裂缝,使其有效延伸至地层深处,从而较单独的射孔更能有效地增加油气产量.通过地面水泥靶的试验,证明了该射孔器的延缝功能和安全性;通过塘32等井的现场试验,证明该射孔技术对污染地层解堵有显著效果,可明显地降低地层破裂压力.     

Thermodynamic properties of 1-nutyl-3-methylimidazolium chloride (C<Subscript>4</Subscript>mim[Cl]) ionic liquid

Thermodynamic properties of 1-butyl-3-methylimidazolium chloride (C₄mim[Cl]) ionic liquid were determined using thermogravimetric (TG) differential thermal analysis (DTA). A new method called DTA mass-difference baseline, was used to measure the heat capacity and enthalpy change of phase transformation of ionic liquid from DTA curves. Based on this, the changes in standard enthalpy, entropy, and Gibbs energy were determined. The results show that standard enthalpy and entropy changes of C₄mim[Cl] increase nonlinearly with increasing temperature, while the standard Gibbs energy change decreases nonlinearly with increasing temperature within the temperature range studied (298–453 K). The standard enthalpy of melting and enthalpy of vaporization were determined to be 0.93 and 11.07 kJ/mol, respectively.     

Fast acquisition clock and data recovery circuit with low jitter

This paper presents a half-rate clock and data recovery circuit (CDR)that combines the fast acquisition of a phase selection (PS) delay-locked loop (DLL) with the low jitter of a phase-locked loop (PLL). The PLL acquisition time improves considerably with use of a phase frequency magnitude detector(PFMD) that feeds back an estimate of the magnitude of the frequency difference in addition to the sign. Measurements in 0.5/spl mu/m CMOS technology show operation up to 700 Mb/s, a 7% acquisition range, an initial acquisition time of 8 bit times with jitter of 30% bit time, and jitter of 16 ps after the PLL acquires lock. With a phase frequency detector (PFD), the PLL locks in about 700 ns from an initial frequency difference of 7%. Measurements using a PFMD show the 700 ns PLL acquisition time is reduced on average by about a factor of 5 to 140 ns from an initial 7% frequency difference. The power dissipation is 300mW.     

木质装饰材料干缩湿胀性对家具拼口的影响

随着装饰业、家具制造业的强劲发展,对于木质材料干缩湿胀性研究尤为重要,企业渴望得到解决木质材料干缩湿胀性的技术。本文在分析了大量文献的基础上,简述了国内外木质材料干缩湿胀性的研究成果,并提出了一些对家具制造具有实用价值的措施。     

以质量管理体系为基础建立实施整合型QHSE管理体系

通过体系整合的必要性和可行性分析,介绍运用管理的系统方法,以质量管理体系为基础,策划、推进及实施整合型QHSE管理体系的做法,并对各阶段体系建立的方法与措施进行阐述。