连续油管技术与装备发展综述

自世界上第一台连续油管作业机问世至今,连续油管作业技术与装备已经过了40多年的发展历程,以其占地面积小、作业成本低、搬迁安装方便、保护油层、增加油井产量和使用范围广等诸多不可比拟的优势,得到迅速发展,并广泛应用于钻井、完井、试油、采油、修井和集输等各个作业领域。实践表明,连续油管作业技术与装备是一项具有巨大潜力和生命力的实用性技术。目前,该项技术的应用日趋活跃,备受关注。在总结连续油管作业技术与装备的发展现状和展示其发展趋势的基础上,客观地分析了国内连续油管技术与装备的应用与研究现状,提出相应的发展对策。     

X80焊管H_2S环境应力腐蚀开裂行为研究

采用三点弯曲加载法和微电极扫描测试技术,研究了X80高强度级管线钢及其焊缝区的抗H2S环境应力腐蚀开裂(SSCC)行为。测定了焊接接头的显微硬度分布,分析了显微组织结构、力学性能及抗腐蚀性能之间的相关性。研究表明,热影响区(HAZ)对应力腐蚀开裂最为敏感,母材的纵向和横向取样对应力腐蚀敏感性影响不显著,薄壁管材比厚壁管材有较好的抗H2S环境应力腐蚀性能。HAZ晶粒粗大、硬度高,局部腐蚀倾向大,由此导致该区SSCC敏感性高。     

琼东南盆地深水区储层分布规律

琼东南盆地深水区经历了断陷、断拗和拗陷3大构造演化和沉积充填阶段,主要发育4种沉积体系,相应地形成了4类主要储层:1)陵三段扇三角洲或滨海相砂岩储层;2)三亚、梅山组滨浅海相砂岩储层;3)三亚—莺黄组低位体储层;4)梅山组台地边缘礁滩灰岩储层。平面上,储层发育具有明显的分带性,可划分为:北部浅水陆架滨岸砂岩、三角洲砂岩储层发育带;中央坳陷低位体储层发育带;南部永乐隆起区碳酸盐岩储层发育带。深水区主要位于后2个带,每个带储层发育的控制因素不同,可以进一步划分为多个储层发育区。每个储层发育区存在多套储盖组合,每套储盖组合在多个储层区中发育。其中台地灰岩储层可能成为南部隆起区具有重要意义的勘探层系。      

井下电视检测系统在水井施工中的应用

简要介绍了井下电视在大港油田水源井水井结构检测、井管故障检测、指导落物打捞、水源井验收、地层结构检测及水源井地层受力分析等方面的应用情况，及应用井下电视检测所取得的经济效益和社会效益。     

Breaking a remote user authentication scheme for multi-server architecture

Lin et al., (2003) proposed a remote user authentication scheme for multi-server architecture. In this paper, we breaks this scheme by giving an attack. Our attack allows an adversary to impersonate any user in the system, as long as a single authentication message of that user is observed.     

用AFM导电探针在n-Si(111)表面进行纳米加工的机理研究

本文介绍了在AFM针尖与氢钝化硅表面之间施加电场作用对硅表面进行修饰的纳米加工方法，重点讨论了加工机理。实验考虑了样品的表面状态，周围大气状况，所加电压的极性、大小和加压方式等影响纳米加工的因素。对机理的研究表明，针尖和样品之间发生的是场致电子发射而非热电子发射，电流热效应增强粒子的扩散能力，提高了电化学反应速度。最后给出了电场诱导阳极氧化扩散增强的加工机理。     

Flash器件中氧化硅/氮化硅/氧化硅的特性

对普遍采用的氧化硅/氮化硅/氧化硅( ONO)三层复合结构介质层的制备工艺及特性进行了研究分析,研究了ONO的漏电特性以及顶氧( top oxide)和底氧( bottom oxide)的厚度对ONO层漏电的影响.结果表明,采用较薄的底氧和较厚的顶氧,既能保证较高的临界电场强度,又能获得较薄的等效氧化层厚度,提高耦合率,降低编程电压.     

Estimating crystallinity in high density polyethylene fibers using online Raman spectroscopy

Online Raman spectra, obtained at different points along the spin line during pilot‐scale nonisothermal melt spinning of high density polyethylene (HDPE) fibers, are presented for the first time. The fraction of the crystalline phase corresponding to each spectrum was determined from the normalized integrated intensity of the 1418 cm^?1 Raman band. It is well established that this band represents the orthorhombic crystalline phase in polyethylene. The estimates of percent crystallinity obtained from decomposition of the Raman spectrum were compared with the percent crystallinity from differential scanning calorimetry (DSC) measurements. It is concluded that online Raman spectroscopy can be successfully used to monitor the development of crystallinity in HDPE fibers as a function of distance from the spinneret. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 545–549, 2003     

Magnetic Properties of Fe-Doped Rutile

Ball-milling method was applied to dissolve Fe into titanium dioxide (TiO₂). X-ray diffraction indicated the starting anatase changed to a rutile-type structure with oxygen deficiency after ball milling. Transmission electron microscopy and X-ray absorption experiments were conducted to examine the possible existence of magnetic impurities in the ball-milled powders after they were leached in HCl solutions. Temperature dependence of the resistivity shows semiconducting behavior and the magnetic hysteresis loops at 5 and 300 K exhibit ferromagnetic characteristics. Fe-doped TiO₂ films were also prepared by pulsed laser deposition. The magnetic properties of the films are discussed.     

复合固体超强酸SO42-/Fe2O3-γ-Al2O3催化合成丁酸丁酯

采用沉淀硫酸化法制备了复合固体超强酸催化剂SO2-4/Fe2O3-γ-Al2O3,确定了其最佳制备工艺条件:硫酸浸渍浓度为0.6 mol/L,浸渍时间4 h;焙烧温度550℃,焙烧时间3 h.并采用该催化剂合成丁酸丁酯,考察了物料配比、催化剂用量和反应时间对酯化反应的影响,确定了丁酸丁酯的最佳合成条件:丁醇与丁酸摩尔比为1.4:1,催化剂用量0.9%(以反应物质量计),回流条件下反应3.0 h,在此最佳合成条件下,酯化率可达95.6%.