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121.
Xiangrong Ma Rui Dang Ning Yang Xiao Li Ya zhang Ying Gong Zhipan Liu Wei Guo Yuanyuan Zhang Chunyan Li 《International Journal of Hydrogen Energy》2021,46(44):22842-22851
The high cost of noble metal catalysts has been a great bottleneck for the catalyst industry. Using the noble metal at a single-atom level for catalytic applications could dramatically decrease the cost. The impacts of single Pt atoms on the photocatalytic performance of Ag3VO4 have been investigated and reported. In this report, single Pt atoms were anchored on the surface of Ag3VO4 (AVO) as a cocatalyst, and the resultant composite photocatalyst has been studied for photocatalytic H2 production from water driven by visible light. The as-prepared AVO particles are hollow nanospheres in the monoclinic phase with a bandgap of 2.20 eV. The light absorption edge of AVO/Pt is slightly red-shifted compared to that of the pristine AVO, indicating more visible light absorption of AVO/Pt. The XPS peaks of Ag, V, and Pt exhibit a significant shift after AVO and Pt get into contact, suggesting the strong interaction between the surface Ag and V atoms, and single Pt atoms. After 3-h illumination, the photocatalytic H2 evolution amount from AVO/Pt is improved up to 1400 μmol, which is 2.8 times that on the bare AVO. Such efficient photocatalytic H2 evolution on AVO/Pt is still maintained after five reaction cycles. The better photocatalytic performance of AVO/Pt has been attributed to the more efficient visible light utilization and the lower interfacial charge transfer resistance, as demonstrated in the DRS and EIS spectra. The presence of the surface Pt atoms also leads to a higher amount of reactive radicals, which could efficiently promote the surface redox reactions. 相似文献
122.
Graded evolution of anisotropic microstructure during sintering from crystal-oriented powder compact
Shoko Baba Alexandre Maître Nicolas Pradeilles Guy Antou Nobuo Saito Satoshi Tanaka 《International Journal of Applied Ceramic Technology》2020,17(2):677-684
Anisotropic sintering, including shrinkage and grain growth, was examined for c-axis-oriented (Sr,Ca)2NaNb5O15 (SCNN) ceramics, which were prepared by colloidal processing under a magnetic field. In the c-axis-oriented SCNN powder compact, shrinkage and grain growth along the c-axis were higher than those along the a-axis. The anisotropic microstructural development was clearly associated with anisotropic sintering shrinkage. X-ray diffraction, scanning electron microscopy, and energy back scattering diffraction showed that the grain growth of oriented particles by including random grains contribute to the development of the oriented microstructure. Finally, the highly crystal-oriented SCNN ceramics with a densified microstructure were obtained through anisotropic sintering. These results clearly showed the potential to develop a well-defined anisotropic microstructure during sintering by designing and controlling the particle packing structure in a powder compact. 相似文献
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刘家山排土场为民采排弃形成,已经出现大规模滑坡。为了保证上下游生产生活设施的安全,依据现场实际情况,结合现场调查,提出了削坡处理的方案。经过治理后,刘家山排土场平稳地渡过了雨季,目前处于稳定状态,达到了治理目的。 相似文献
125.
Xiaoqin Zhang Shugang Ma Ang Shen Jin Zhu Zhisen Shen Jinggang Wang Xiaoqing Liu 《应用聚合物科学杂志》2020,137(44):49365
Poly(butylene terephthalate-co-butylene 2,5-furandicarboxylate) copolyesters (PBTFs) were synthesized from 1,4-butanediol, dimethyl terephthalate (DMT), and 2,5-furandicarboxylic acid (FDCA) by a two-step polymerization method. Their chemical structures were confirmed by Fourier-transform infrared spectroscopy, proton nuclear magnetic resonance spectroscopy, and carbon nuclear magnetic resonance before thermal properties were explored with differential scanning calorimeter and thermogravimetric analyzer. Results showed that PBTFs changed from semi-crystalline to completely amorphous when the content of FDCA unit was increased to 45 mol% at first, and then became crystallographic again with the further increment of FDCA unit to 75 mol%. For their mechanical properties, the tensile modulus and strength showed the similar trend, decreasing firstly and then increasing later. Their barrier to carbon dioxide and oxygen became better with the increasing of furan content due to the rigidity and higher polarity of furan ring. The performance of PBTFs copolyesters was investigated clearly, and the relative content of FDCA and DMT can be adjusted to satisfy different performance requirements. 相似文献
126.
文章中主要采用有机溶剂萃取法(OSE)对高浓度石油污染土壤进行修复,经过精馏操作,有效回收原油,建立脱附等温曲线,研究了石油污染物在土壤-有机溶剂两相间的迁移规律。 相似文献
127.
现有的基于电磁感应理论的接地网故障诊断方法需要大量的磁场测量数据,为了解决该问题,笔者提出了一种基于支路影响系数分析的分层诊断方法.首先定义了支路影响系数,并根据影响系数建立了支路诊断难易程度的评价体系.在该评价体系的指导下,分层诊断方法的测量点选取更具针对性,并以分层递进的方式实现了高精确度的腐蚀诊断.在诊断模型求解方面,运用改进的鲸鱼优化算法,保证了分层诊断的准确性.最后,进行了分层诊断与普通磁场反演诊断的对比实验.实验结果表明:分层诊断方法可以在保证诊断准确率的情况下大幅减少测量点数量(可做到接地网支路数50%以下),并且能够缩小测量点的分布范围,因此该方法可以减少现场测量工作量,提高接地网故障诊断效率. 相似文献
128.
随钻扩眼工具及技术研究 总被引:1,自引:0,他引:1
基于随钻扩眼技术优势的分析,研究了机械式、液压式和偏心式随钻扩眼工具执行机构和扩眼总成的机构原理,并介绍了国内所开展的相关研究。文章提出应加强现有工具的适应性和匹配性研究,发掘各类工具的优势。优化执行机构、扩眼总成和水力机构、重视底部钻具组合力学特性的分析是今后发展和完善随钻扩眼工具及技术的几个重要内容。实践表明,随钻扩眼技术在处理井下复杂情况、降低钻井综合成本、提高钻井速度、提高建井质量和安全性等方面具有显著的优势,随钻扩眼工具也正逐渐成为一种重要的石油钻井配套工具。 相似文献
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130.
Effendi Rusli Timothy O. Drews David L. Ma Richard C. Alkire Richard D. Braatz 《Journal of Process Control》2006,16(4):409-417
Robust nonlinear feedforward–feedback controllers are designed for a multiscale system that dynamically couples kinetic Monte Carlo (KMC) and finite difference (FD) simulation codes. The coupled codes simulate the copper electrodeposition process for manufacturing on-chip copper interconnects in electronic devices. The control objective is to regulate the current density subject to the condition that the steady-state fluctuation of the overpotential remains bounded within ±0.01 V. The controller designs incorporate a low-order stochastic model that captures the input–output behavior of the coupled KMC–FD code. The controllers achieve the objectives and the closed-loop responses implemented on the low-order model and the coupled KMC–FD code match well within stochastic variations. The nonlinear feedforward control reduces the rise time of the controller response while the feedback control ensures robustness in the presence of model uncertainty. 相似文献