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11.
Marija Prekajski Đorđević Jelena Maletaškić Nadežda Stanković Biljana Babić Katsumi Yoshida Toyohiko Yano Branko Matović 《Ceramics International》2018,44(2):1771-1777
Hydroxyapatite was used as the inert matrix for in-situ immobilization of strontium (Sr) radioactive isotopes at room temperature. A nano-emulsification method was applied to synthesize Sr-substituted calcium hydroxyapatite (Ca1?xSrx)10(PO4)6(OH)2. The concentration of incorporated Sr was in the range of 0 ≤ x ≤ 1. Immobilization of Sr was evaluated using a stable isotope instead of radioactive isotope. The effect of strontium concentration on the crystal structure was studied and the results have showed that in the whole concentration range, Sr forms solid solutions with the host hydroxyapatite crystal structure. Powders comprised of nanometre sized particles were obtained and their properties, such as crystallite and particle size, changes in lattice parameters as function of dopant content and thermal stability, were further examined. It was found that the crystal structure of obtained powders is thermally stable at high temperatures. No secondary phases were formed in as-prepared powders or during calcination. The results in this study showed that nano-emulsion strategy provides a simple pathway for synthesis of a single-phase Sr-substituted hydroxyapatite, which can be used for immobilization of Sr radioactive isotopes. 相似文献
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Simultaneous B-M-mode scanning method for real-time full-range Fourier domain optical coherence tomography 总被引:1,自引:0,他引:1
High-speed complex full-range Fourier domain optical coherence tomography (FD-OCT) is demonstrated. In this FD-OCT, the phase modulation of a reference beam (M scan) and transversal scanning (B scan) are simultaneously performed. The Fourier transform method is applied along the direction of the B scan to reconstruct complex spectra, and the complex spectra comprise a full-range OCT image. Because of this simultaneous B-M-mode scan, the FD-OCT requires only a single A scan for each single transversal position to obtain a full-range FD-OCT image. A simple but slow version of the FD-OCT visualizes the cross section of a plastic plate. A modified fast version of this FD-OCT investigates a sweat duct in a finger pad in vivo and visualizes it with an acquisition time of 27 ms. 相似文献
14.
We report on the alloying of epitaxial Co/Pt core-shell nanoparticles using transmission electron microscopy (TEM) and electron diffraction. In as-deposited nanoparticles followed by in situ annealing at 823 K for 10.8 ks, high-angle annular dark-field (HAADF) imaging by scanning TEM (STEM) clearly revealed formation of Co-shell/Pt-core structures due to the large atomic number (Z) difference between Co (Z = 27) and Pt (Z = 78). We identified a formation of locally ordered areas of the L10 ordered phase at the core of the nanoparticles. After ex situ annealing at 873 K for 0.6 ks, some of the ordered areas showed complicated contrasts in the HAADF-STEM images. Based on image simulations, we found that these atypical contrasts arise from the stacking of two orthogonal variants of the L10 phase in the electron beam direction. Furthermore, the simulation showed that image contrast strongly reflects the structure of the variant located closer to the beam entrance rather than to the bottom side. Solid solution phase was formed by further annealing at 873 K for 3.6 ks, while high-density {111} stacking faults were observed inside the Co-Pt alloy nanoparticles. Magnetic coercivity remained at values as low as ~ 15.9 kA/m at 300 K, irrespective of the formation of local L10 ordered areas and/or a high-density stacking faults. 相似文献
15.
Kenta Aoyagi Yumiko Kodama Takanori Kiguchi Yoshitaka Ehara Hiroshi Funakubo Toyohiko J. Konno 《Materials Science and Engineering: B》2012,177(7):528-531
The microstructure of an epitaxial PbTiO3 thick film, grown on a SrRuO3/SrTiO3 substrate at 600 °C by pulsed-MOCVD method, was investigated by using transmission electron microscopy. A number of extrinsic or intrinsic stacking faults were observed in the epitaxial PbTiO3 thick film and they were parallel to the (0 0 1) plane of the PbTiO3. We also investigated the size distribution of these stacking faults. The width of these stacking faults along the [1 0 0] axis of the PbTiO3 was very small, ranging from 2 to 13 nm. It was also revealed that the size distribution of stacking faults depends on the position in the film: near the surface, near the substrate, near threading dislocations, and near 90° domain boundaries. 相似文献
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Saori Umehara Masao Nomura Shin Okumura Toyohiko Yano Tadafumi Kishimoto 《Journal of Nuclear Science and Technology》2013,50(12):1473-1480
To develop the 48Ca enrichment process, a feasibility study on a band chromatography was made using 9 M HCl solution and crown ether resin synthesized in porous silica beads. Prior to the chromatographic experiments, distribution coefficients, Kd, of Ca2+ and Sr2+ were measured at different concentrations of these ionic species. The frontal boundary of the chromatography was made by a usual manner of the breakthrough mode of calcium feeding, and the rear boundary was made by introducing strontium as a following ion on the basis of the observed Kd values. It was confirmed that the heavy isotope 48Ca was depleted in the rear boundary region, while 48Ca was enriched in the front boundary region. The values of separation coefficient ε (= α – 1) in three chromatographic operations at different temperatures were observed as 2 × 10?3 ~ 3 × 10?3. The separation coefficients observed in the front boundary regions, where 48Ca was enriched, agreed with those observed in the rear boundary regions, where 40Ca was enriched. 相似文献
18.
Simultaneous depth determination of multiple objects by focus analysis in digital holography 总被引:2,自引:0,他引:2
Focus analysis techniques from computer vision are applied to digital holography to determine the depth (range) of multiple objects and their surfaces from a single hologram capture. With this method the depths of objects can be determined from a single hologram capture without the need for manual focusing and without prior information on object location. Variance and the Laplacian of Gaussian are analyzed as focus measures, and techniques are proposed for focus plane determination from the focus measure curves. The algorithm is described in detail and demonstrated through simulation and optical experiment. 相似文献
19.
The crystallinity, solubility, degree of swelling, and hygroscopicity of the blends of syndiotactic-rich (st-PVA) and atactic poly(vinyl alcohols) (at-PVA) were studied. The crystallinity of the blends increased with increasing annealing temperature and that of the blends annealed at 200°C was larger than that of at-PVA. In the 200°C annealed blends containing st-PVA about 50%, the insoluble fraction in boiling water was larger than the fraction of st-PVA in each blend. The soluble fraction for the blend containing 75% st-PVA was 1.7%. The moisture regain of the blends was less than that of at-PVA. 相似文献
20.
Toyohiko Yano Masanori Ikari Takayoshi Iseki Eugene H. Farnum Frank W. Clinard Jr. T. E. Mitchell 《Journal of the American Ceramic Society》1995,78(6):1469-1474
MgO·3Al2 O3 single crystals were irradiated with neutron fluences of 8.3 × 1022 n/m2 at 100°C and 2.4 × 1024 n/m2 at 470°C ( E > 1.0 MeV) in the Japan Materials Testing Reactor. The Knoop microhardness of several orientations on the (100) plane of both the irradiated and unirradiated crystals were measured with different indentation loads. The change in hardness profile of the crystals was almost the same after the two irradiation conditions. The hardness increased by 4–15% because of the irradiations depending on the crystallographic orientation, the larger change being observed at orientations between the (001) and (011) directions. While both the {111} and {110} slip systems are simultaneously active in the unirradiated MgO·3Al2 O3 , the {111} system may be the dominant slip system in the neutron-irradiated crystals. It is concluded that the restriction of the {110} slip system is caused by irradiation-induced interstitial ions. 相似文献