旋风分离器结构改进的研究

根据旋风分离器的工作原理及应用特点 ,分析了影响旋风分离器分离效率的因素及结构存在的问题 ,并提出了改进措施 ,即内管外壁增设螺旋翼片 ,扩散形锥体改为悬挂挡板。通过实验观察 ,改进结构的旋风分离器分离效率比常规旋风分离器高。实践证明 ,对于密度差异较小的非均相物系的分离 ,只要对旋风分离器作适当改进 ,仍能取得令人满意的效果 ,这大大拓宽了旋风分离器的应用领域     

十二酰胺丙基二甲基羟乙基氯化铵与十二烷基硫酸钠水溶液的表面吸附和胶束形成

利用十二酰胺丙基二甲胺和氯乙醇反应 ,合成了十二酰胺丙基二甲基羟乙基氯化铵 (DDHA)阳离子表面活性剂 ,将其与十二烷基硫酸钠 (SDS)以不同摩尔比进行混合 ,测定了混合系统的表面张力 ,计算了单一系统和混合系统的饱和吸附量、分子最小截面积 ,表面层和胶束中 DDHA的摩尔分率及分子间相互作用参数 ,目视观察了混合系统的浑浊情况。结果表明 :在降低γcmc和 cmc方面 ,DDHA SDS混合系统有协同效应 ,表面层和胶束的组成与二组分配比有关 ,但是非对称的 ,等物质的量混合物中 ,DDHA在胶束和表面层中具有较大的摩尔分数。DDHA与 SDS在实验测定的各混合系统中都不出现混浊     

中国珠宝销售的可持续发展

通过对改革开放20多年来中国珠宝业发展的回顾与分析, 认为在激烈的市场竞争中, 珠宝业要达到可持续发展必须具备6个要素: (1)敬业精神; (2)信用意识; (3)创新意识和创新能力; (4)激励机制和团队精神; (5)资本营运和资源整合能力; (6)关系营销技巧.     

宽带线性调频信号产主技术研究

本文介绍了采用数字基带产生结合倍频链扩展带宽的方法设计与实现了大带宽线性调频信号产生系统。详细分析研究了实现系统的三项关键技术，给出并分析了相应环节的输出信号。对系统进行了预失真补偿处理，成功实现了ＶＨＦ／ＵＨＦ波段、带宽达３００ＭＨｚ线性调频信号的产生。经脉冲压缩处理，主瓣旁瓣比（ＰＳ１Ｒ）在－３７ｄＢ以下。     

Set－up of a Pure Electron Plasma Device

An electron Penning-Malmberg trap,which can confine an electron column and provide a good platform to investigate the cross-filed transportation of strongly magnetized electron plasma ,has been set up.With the device,an electron plasma with a density of 10^7 cm^-3 can be confined for a relatively long time.The structure of the trap,electron source,as well as the way how th measure electron plasma density profile and velocity distrbustion are introduced in detail.     

Top-Seeded Melt-Growth of YBa2Cus3Ox Crystals for Neutron Diffraction Studies

We have grown cubic centimeter-size crystals of YBa₂Cu₃O _x suitable for neutron studies, by a top-seeded melt-growth technique. Growth conditions were optimized with an eye toward maximizing phase purity. It was found that the addition of 2% Y₂BaCuO₅ and 0.5% Pt (by mass) were required to prevent melt loss and to obtain the highest crystallinity. A neutron diffraction study on a mosaic of six such crystals found that the final Y₂BaCuO₅ concentration was 5%, while other impurity phases comprised less than 1% by volume. The oxygen content was set to x = 6.5, the crystals were detwinned, and then carefully annealed to give the well-ordered ortho-II phase. The neutron study determined that 70% of the mosaic's volume was in the majority orthorhomic domain. The neutron (006) and (110) rocking curve widths were ～1° per crystal and ～2.2° for the mosaic, and the oxygen chain correlation lengths were >100 Å in the a- and b-directions and ～50 Å in the c-direction.     

纳米β-NiOOH的固相合成及其性能

首次利用固相氧化法制备了 β NiOOH纳米粉体样品 ,经X射线衍射和透射电镜测试结果表明所得样品 β NiOOH粒子呈球形 ,粒径大小在 2 0～ 40nm之间。热重与差热分析结果表明当温度超过 10 0℃ ,样品开始不可逆地分解为NiO。运用恒流充放电、循环伏安以及Tafel极化等电化学测试对样品的电化学性能进行了初步研究。结果表明 :β NiOOH的交换电流密度高于 β Ni(OH) 2 的交换电流密度约一个数量级 ,具有较好的电极可逆性、较高的质量比容量以及优良的容量保持率 ,适于作为Zn/NiOOH类型镍电池的正极活性材料     

多级机站通风新模式和矿井通风技术的新进展

文中详细论述了我国“九五”期间金属矿山在多级机站通风系统改造中涌现出的先进技术 ,反映了我国矿山通风技术的发展现状。同时 ,探讨了矿井通风技术的发展方向 ,对矿井通风系统的改造研究具有一定意义     

两段式热脱焦油煤气炉在环形加热炉上的开发应用

介绍了两段式煤气发生炉热脱焦油煤气在无缝钢管环形加热炉上的开发与应用 ,以及两段式煤气发生炉热脱焦油煤气站的设计和采用热脱焦油煤气代替重油所产生的经济效益     

Determination of molecular weight distributions of tert-octylphenol ethoxylate surfactant polymers by laser desorption Fourier transform ion cyclotron resonance mass spectrometry and high-performance liquid chromatography

Triton polymers are commercial surfactants whose molecular weight distributions are conventionally determined by means of high-performance liquid chromatography (HPLC). However, in the case of the important octylphenol ethoxylates [p-C8H17-C6H4-O-(CH2CH2O)n-H], HPLC cannot resolve individual oligomers of high molecular weight Triton surfactants (e.g., greater than 2000 u or so; u = unified atomic mass unit). In this paper, we show that laser desorption Fourier transform ion cyclotron resonance mass spectrometry (LD/FT/ICR/MS) provides a simple and accurate measure of such Triton surfactant molecular weight distributions up to at least 3500 u, based on a single-shot laser pulse measurement of a few seconds duration. Comparison of LD/FT/ICR/MS and HPLC molecular weight distributions of low molecular weight surfactants shows that laser desorption/ionization produces minimal fragmentation and thus offers an accurate measure of the relative abundances of the neutral oligomers, without the need for prior chromatographic separation of the components. Moreover, for all Triton polymer molecular weight distributions (700-3000 u), LD/FT/ICR/MS provides much more highly resolved profiles of oligomer relative abundances. Finally, LD/FT/ICR/MS reveals the presence of poly(ethylene oxide) side products of the polymerization process, which are not observed by HPLC with conventional ultraviolet absorption detection.