Ozonation of CI Reactive Black 5 using rotating packed bed and stirred tank reactor

This study investigates the ozonation of CI Reactive Black 5 (RB5) by using the rotating packed bed (RPB) and completely stirred tank reactor (CSTR) as ozone contactors. The RPB, which provides high gravitational force by adjusting the rotational speed, was employed as a novel ozone contactor. The same ozone dosage was separately introduced into either the RPB or the CSTR for the investigation, while the experimental solution was continuously circulated within the apparatus consisting of the RPB and CSTR. The decolorization and mineralization efficiencies of RB5 in the course of ozonation are compared for these two methods. Moreover, the dissolved and off‐gas ozone concentrations were simultaneously monitored for the further analysis. As a result, the ozone mass transfer rate per unit volume of the RPB was significantly higher because of its higher mass transfer coefficient and gas–liquid concentration driving force. Furthermore, ozonation kinetics was found to be independent of the gravitational magnitude of an ozone gas–liquid contactor. Therefore, the results suggest employing RPBs as ozone‐contacting devices with the advantage of volume reduction. The experimental results, which can be used for further modeling of the ozonation process in the RPB, also show the requirement of correct design for the RPB. Consequently, the present study is useful for the understanding of practical application of RPBs. Copyright © 2004 Society of Chemical Industry     

微滤膜清洗的研究

用次氯酸钠溶液、氢氧化钠溶液和盐酸溶液对小型微滤膜进行化学清洗试验,比较试验结果认为,用次氯酸钠溶液对受污染的微滤膜清洗更为有效,从而为鄂尔多斯羊绒集团污水处理厂中的大型连续微滤化学清洗提供依据.     

掺钛蓝宝石激光晶体中夹杂物的分析

本文用大视场光学显微镜、电子探针观察和分析了掺钛蓝宝石激光晶体中夹杂物的形状、尺寸大小及元素组成，并提出消除和减少这些夹杂物的方法．     

综述老油田改善开发效果及提高采收率技术

中国陆上老油田已进入高含水后期开发，随着开采程度加深，地下油水关系越来越复杂，剩余油分散，给油田稳产和调整挖潜带来的难度越来越大。但目前老油田储量和产量的比例，仍占陆上总开发储量和产量的７０％以上，是生产上的主力，其潜力也最大，仍然是今后调整挖潜的主要对象。鉴于中国陆上油田绝大多数为陆相储层，构造复杂，非均质严重，原油粘度偏高，石油地质特点决定了水驱油的不均匀性及剩余油分布的复杂性，潜力就存在于这种复杂之中。根据中国陆上石油地质特点和老油田开发现状，围绕改善开发效果及提高采收率着重阐述了四个方面的配套技术：即认识油藏的配套技术，主要包括油藏动态监测技术、油藏精细描述技术、油藏数值模拟技术；完善注水开发配套技术，主要包括注水结构调整、产液结构及含水结构调整、钻取高效调整井、改造“双低”单元、配套工艺技术等；热力采油配套技术；化学驱采油配套技术。经过多年来的努力，我国陆上油田提高采收率技术有了明显进步，针对不同类型油藏潜力分布特点，采用各种有效方法及其配套技术，为挖潜增储、增产提供了很大的余地。     

红外化学遥感数字信号处理算法的研究进展

介绍了几种为远距离红外蒸汽信号监测开发的分类器设计，频域数字滤波，时域数字滤波等数字信号处理技术。对线性分类器，分段线性分类器和神经网络分类器等在红外化学遥感系统中的应用做了初步的探讨。对背景扣除技术，频域数字滤波技术，数字滤波的切趾方法等做了简要的描述。阐述了时域滤波技术的基本原理及实际应用。展望了红外化学遥感数字信号处理算法的研究前景。     

丙烯酸2-乙基己酯与醋酸乙烯酯共聚合成高吸油性树脂的研究

以丙烯酸2－乙基己酯与醋酸乙烯酯为单体，采用悬浮聚合法，以单体自交联制得高吸油性树脂。对影响其吸油性能的多种因素，如单体配比、引发剂、油水相比的用量等，进行了系统的研究，得到的高吸油性树脂吸苯最高达16．1g/g，吸甲苯为14．8g/g，吸环己烷为13．3g/g，吸煤油为12．5g/g，可用于河面、海洋浮油的回收及工厂废水处理等领域.     

Sensitizing Mechanism and Adsorption Properties of Dye—Sensitized TiO2 Thin Films

The dye-sensitized TiO2 complex films were prepared by the dye coat onto TiO2 surfaces,and the sensitizing mechanism and adsorption properties of the dye-sensitized TiO2 complex films were inverstigated.The influence of the application conditions of dye adsorbed on TiO2 films on the amount of dye adsorption was discussed.Experimental results show that the concentration,the temperature of dye solutions and the dipping time of TiO2 films in the dye solutions have a significant influence on the amount of dye adsorption.Cell test indicates that the conversion efficiency of light to electricity increases with the amount of dye adsorption.     

划分IC缺陷团的聚类算法

大量实验表明了在集成电路（IC）制造过程中形成中的缺陷团之间具有很强的相关性，然而现用于划分缺陷团的方法均忽略了缺陷之间的相关性。因此，得到了缺陷分布规律不能有效地反映缺陷在圆片上的分布，为了提高IC成品率和可靠性仿真和设计的精度，提高缺陷分布模型的准确性，该文提出了划分缺陷团的聚类算法，该方法依据缺陷形成的动力学基础，充分考虑了缺陷团之间的相关性，实验证明该算法用于划分IC的缺陷团是十分有效的。     

国外钻井液和完井液用聚合物

９０年代以来，国外钻井液和完井液用聚合物添加剂的发展取得长足进步。本文介绍了国外目前用于钻井液和完井液的聚合物添加剂的类型及作用。     

布里奇曼法生长碲镉汞晶体的缺陷及其展望

简单介绍了布里奇曼法生长碲镉汞晶体的主要缺陷以及缺陷的控制原理，回顾了国内进行磅镉汞晶体生长的布里奇曼法及加速坩埚旋转技术的布里奇曼法（ＡＣＲＴ－Ｂ）研究的情况，并提出了进一步研究的问题。